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picasso18: ½ð±Ò+100, ·ÒëEPI+1, Ïȸø100°É~×îºóÄãÒªÊǾõµÃÉÙ ÎÒ¿ÉÒÔÔÙ×·¼Ó½±Àø¡£ 2013-03-28 18:50:06
| heat and mass transfer of High viscosity pseudoplastic fluids in stirred tank reactor are very complicated.Current theories are difficult to reveal the nature of two processes.so far,with regard to heat transfer,dimensionless number equation are most derived by regression of a great quantity of experimental data.But calculated values differ greatly from experimental values,and the regression equation is not applicable to all fluids. ÏÈÖ§¸¶150½ð±Ò |

3Â¥2013-03-28 18:31:16
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- ×¢²á: 2013-04-07
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Powders of Ba1−xBixSc0.1Co0.9O3−ı and BaBixSc0.1Co0.9−xO3−ı (x = 0¨C0.3) were prepared by a combined EDTA¨Ccitrate complexing sol¨Cgel process. Ba(NO3)2 (99%, Ajax Finechem Australia), Bi(NO3)3¡¤5H2O (99.99+%, Sigma¨CAldrich), Sc(NO3)3 (99.9%, Metall Rare Earth Limited, China) and Co(NO3)2¡¤6H2O (98.0+%, Sigma¨CAldrich) were used as the raw materials for metal sources. Stoichiometric quantities of these metal nitrates were added to the EDTA (99.4+%, Ajax Finechem Australia) and NH3 aqueous solution (28%, Ajax Finechem Australia) (to control the pH at 6) under heating and stirring followed by the addition of anhydrous citric acid (99.5%, Fluka) resulting in violet transparent aqueous solution. The molar ratio of all metal nitrates:EDTA:citric acid is kept at 1:1.1:2. After evaporation of water, a dark purple gel was recovered. The gel was pretreated on the furnace at 700 ◦C for 8 h to form a solid precursor. The solid precursor was then ground onto powder and calcined at 700 ◦C for 8 h. As calcined powders were ball milled with ethanol (Analytical Reagent, Repack) in a planetary mill (Pulverisette 5, Fritsch) at 500rpm for 1.5 h and heated at 80 ◦C afterwards to evaporate the ethanol. The powders were subsequently pressed under a 5 tons force hydraulic press onto disks with diameter of 15mm. These green disks were finally sintered between 950 and 1100 ◦C for 8 h. Ç×ÃÇ£¬°ïæ·ÒëÒ»Ï塃 ¸Ð¼¤ |
4Â¥2013-04-07 22:57:13













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