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willwang

银虫 (小有名气)

[求助] 求助微谱数据

C-NMR(CDCl3):15.65, 18.58, 18.84, 21.41, 23.36, 23.48, 26.43, 26.45, 26.54, 28.79, 31.05, 32.15, 32.39, 33.03, 34.33, 34.45, 36.52, 36.73, 39.79, 43.54, 45.26, 45.31, 47.69, 47.75, 55.48, 61.04, 128.04, 128.49, 130.12, 170.99, 199.44, 217.12

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wq0616

铁杆木虫 (正式写手)

【答案】应助回帖

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感谢参与,应助指数 +1
willwang: 金币+15, ★★★★★最佳答案 2013-03-26 14:43:36
1 .     齐墩果-12-烯-3,11-二酮
C30H46O2     相似度:93.7%
Chinese Traditional and Herbal Drugs          2003          34          590-592
Chemical constituents of Ailanthus triphysa
QI Shu hua; WU Da gang; MA Yun bao; LUO Xiao dong
Structure      13C NMR   碳谱模拟图
2 .     3,11-dioxo-olean-12-ene
    相似度:87.5%
Acta Botanica Sinica          1994          36          153-158
Studies On Triterpenod Constituents Isolated from The Roots of Sabia schumanniana
Yuan Xiao, Wang Guo-liang and Gong Fu-jun
Structure      13C NMR   碳谱模拟图
3 .     3,11-dioxoolean-12-en-28-yl acetate
C32H48O4     相似度:84.3%
Journal of Natural Products          1997          60          1174-1177
Partial Synthesis of Krukovines A and B, Triterpene Ketones Isolated from the Brazilian Medicinal Plant Maytenus krukovii
Tadashi Honda, Heather J. Finlay, and Gordon W. Gribble
Structure      13C NMR   碳谱模拟图
4 .     krukovine A
C30H46O3     相似度:84.3%
Journal of Natural Products          1997          60          1174-1177
Partial Synthesis of Krukovines A and B, Triterpene Ketones Isolated from the Brazilian Medicinal Plant Maytenus krukovii
Tadashi Honda, Heather J. Finlay, and Gordon W. Gribble
Structure      13C NMR   碳谱模拟图
5 .     12-oleanen-3,11-dione
    相似度:84.3%
China Journal of Chinese Materia Medica          2010          35          2708-2711
Chemical constituents of Indigofera pseudotinctoria
WEN Erya; LIANG Hong
Structure      13C NMR   碳谱模拟图
6 .     (18β,20β)-N-hydroxy-N-methyl-3,11-dioxo-olean-12-en-29-amide
    相似度:81.2%
Bioorganic & Medicinal Chemistry          2010          18          7522-7541
Synthesis of novel 3-amino and 29-hydroxamic acid derivatives of glycyrrhetinic acid as selective 11β-hydroxysteroid dehydrogenase 2 inhibitors
Christian Stanetty, Laszlo Czollner, Iris Koller, Priti Shah, Rawindra Gaware, Thierry Da Cunha, Alex Odermatt, Ulrich Jordis, Paul Kosma, Dirk Claßen-Houben
Structure      13C NMR   碳谱模拟图
7 .     12-en-3β-Hydroxy-olean-11-one
    相似度:81.2%
Chemistry of Natural Compounds          2012          48          344-345
Chemical constituents from Saussurea oligantha
Xue-Hu Li, Jian-Ping Liang, Xi-Hong Lu and Lei Tao
Structure      13C NMR   碳谱模拟图
8 .     3,11-dioxoolean-12-en-28-oic acid
    相似度:78.1%
Journal of Natural Products          2006          69          142-144
Lupane and Oleanane Triterpenoids from the Cones of Liquidamber styraciflua
Yuko Fukuda, Takeshi Yamada, Shun-ich Wada, Kuniyoshi Sakai, Shunyo Matsunaga, and Reiko Tanaka
Structure      13C NMR   碳谱模拟图
9 .     krukovine A
C30H46O3     相似度:78.1%
Journal of Natural Products          1996          59          1072-1075
Triterpenes from Brazilian Medicinal Plant “Chuchuhuasi” (Maytenus krukovii)
Osamu Shirota, Toshihiko Tamemura, Hiroshi Morita, Koichi Takeya, and Hideji Itokawa
Structure      13C NMR   碳谱模拟图
10 .     3,11-dioxo-18β-olean-12-en-28-oic acid
    相似度:78.1%
Chemistry of Natural Compounds          1992          28          1-23
13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES
A. I. Kalinovskii
Structure      13C NMR   碳谱模拟图
11 .     3β-acetoxyolean-12-en-11-one
    相似度:78.1%
Natural Product Sciences          1998          4          253-256
Oleanane Triterpenoids from Gordonia ceylanica
Herath, H.M.T.B.; Athukoralage, P.S.
Structure      13C NMR   碳谱模拟图
12 .     3β-hydroxyolean-12-en-11-one
    相似度:78.1%
Natural Product Sciences          1998          4          253-256
Oleanane Triterpenoids from Gordonia ceylanica
Herath, H.M.T.B.; Athukoralage, P.S.
Structure      13C NMR   碳谱模拟图
13 .     3-Oxo-18β-glycyrrhetinic acid
C30H44O6     相似度:78.1%
Phytochemistry          2010          71          262-270
Bioactive microbial metabolites from glycyrrhetinic acid
Galal T. Maatooq, Amani M. Marzouk, Alexander I. Gray, John P. Rosazza
Structure      13C NMR   碳谱模拟图
14 .     3β-hidroxyolean-12-en-11-one
    相似度:78.1%
Natural Product Research          2010          24          767-774
Rearrangement and oxidation of β-amyrin promoted by growing cells of Lecanicillium muscarinium
Leonardo Ribeiro Martins; Jacqueline Aparecida Takahashi
Structure      13C NMR   碳谱模拟图
15 .     3,11-dioxo-olean-12-ene
    相似度:78.1%
Chinese Pharmaceutical Journal          2005          40          900-902
Studies on chemical constituents of Sabia schumanniana
LIANG Guang-yi, ZHOU Ying, CAO Pei-xue, XU Bi-xue
Structure      13C NMR   碳谱模拟图
16 .     11-oxo-3β-hydroxy-olean-12-ene
    相似度:78.1%
Chinese Pharmaceutical Journal          2005          40          900-902
Studies on chemical constituents of Sabia schumanniana
LIANG Guang-yi, ZHOU Ying, CAO Pei-xue, XU Bi-xue
Structure      13C NMR   碳谱模拟图
17 .     3,11-Dioxo-olean-12-en-30-oic acid
    相似度:78.1%
Zeitschrift für Naturforschung B          2011          66          521-532
Synthesis and Antitumor Activity of Ring A-modified Glycyrrhetinic Acid Derivatives
R. Csuk, S. Schwarz, B. Siewert, R. Kluge, and D. Ströhl
Structure      13C NMR   碳谱模拟图
18 .     (18β,20β)-3,11-dioxo-olean-12-en-29-oic acid methylester
    相似度:78.1%
Bioorganic & Medicinal Chemistry          2010          18          433-454
Synthesis of glycyrrhetinic acid derivatives for the treatment of metabolic diseases
Igor Beseda, Laszlo Czollner, Priti S. Shah, Rupesh Khunt, Rawindra Gaware, Paul Kosma, Christian Stanetty, Maria Carmen del Ruiz-Ruiz, Hassan Amer, Kurt Mereiter, Thierry Da Cunha, Alex Odermatt, Dirk Claßen-Houben, Ulrich Jordis
Structure      13C NMR   碳谱模拟图
19 .     (18β,20β)-N-hydroxy-3,11-dioxo-olean-12-en-29-amide
    相似度:78.1%
Bioorganic & Medicinal Chemistry          2010          18          7522-7541
Synthesis of novel 3-amino and 29-hydroxamic acid derivatives of glycyrrhetinic acid as selective 11β-hydroxysteroid dehydrogenase 2 inhibitors
Christian Stanetty, Laszlo Czollner, Iris Koller, Priti Shah, Rawindra Gaware, Thierry Da Cunha, Alex Odermatt, Ulrich Jordis, Paul Kosma, Dirk Claßen-Houben
Structure      13C NMR   碳谱模拟图
20 .     3β-乙酰氧基-齐墩果-12-烯-11-酮
    相似度:78.1%
Lishizhen Medicine and Materia Medica Research          2011          22          2208-2209
马棘石油醚部分化学成分研究
胡泽华; 周静; 田力; 张鹏; 吴继洲
Structure      13C NMR   碳谱模拟图
21 .     (18β,20β)-N-benzyloxy-3,11-dioxo-olean-12-en-29-amide
    相似度:77.1%
Bioorganic & Medicinal Chemistry          2010          18          7522-7541
Synthesis of novel 3-amino and 29-hydroxamic acid derivatives of glycyrrhetinic acid as selective 11β-hydroxysteroid dehydrogenase 2 inhibitors
Christian Stanetty, Laszlo Czollner, Iris Koller, Priti Shah, Rawindra Gaware, Thierry Da Cunha, Alex Odermatt, Ulrich Jordis, Paul Kosma, Dirk Claßen-Houben
Structure      13C NMR   碳谱模拟图
22 .     compound 62
    相似度:75%
Chemistry of Natural Compounds          1992          28          1-23
13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES
A. I. Kalinovskii
Structure      13C NMR   碳谱模拟图
艰难困苦,玉汝于成。
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