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菲你莫属

铁杆木虫 (正式写手)

[求助] 求助微谱数据查询结果,感谢

12.2, 12.2, 17.3, 19.0, 21.0, 21.2, 21.4, 25.4, 26.4, 29.0, 31.2, 31.9, 36.3, 38.3, 38.6, 40.2, 41.8, 43.0, 45.4, 50.0, 50.0, 51.2, 54.7, 70.5, 126.1, 129.5, 138.1, 165.1, 202.2
溶剂是氘代氯仿。
谢谢!
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菲你莫属

铁杆木虫 (正式写手)

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2楼: Originally posted by wq0616 at 2013-03-12 13:04:45
1 .     3β-hydroxystigmast-5,22-dien-7-one
    相似度:93.1%
China Journal of Chinese Materia Medica          2009          34          1809-1811
Steroids from Monascus purpureus metabolite
SHA ...

谢啦
3楼2013-03-12 18:41:00
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wq0616

铁杆木虫 (正式写手)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
菲你莫属: 金币+20, ★★★★★最佳答案 2013-03-12 18:39:58
1 .     3β-hydroxystigmast-5,22-dien-7-one
    相似度:93.1%
China Journal of Chinese Materia Medica          2009          34          1809-1811
Steroids from Monascus purpureus metabolite
SHANG Xiaoya, WANG Ruolan, YI N Suqin, LI Jinjie, JIN Zonglian
Structure      13C NMR   碳谱模拟图
2 .     stigmasta-5,22-dien-3β-ol-7-one
    相似度:93.1%
China Journal of Chinese Materia Medica          2011          Vol 36,Issue 7          891-895
Chemical constituents from petroleum ether portion of Abelmoschus esculentus
JIA Lu, GUO M ingm ing, LI Dong, JING Lin lin
Structure      13C NMR   碳谱模拟图
3 .     3β-hydroxystigmasta-5,22-dien-7-one
C29H46O2     相似度:93.1%
Chinese Journal of Marine Drugs          2007          26(6)          5-9
Studies on chemical constituents in ethanol ic extract from A-ca nt hus ilici f olius as a pharmaceutic mangrove
ZHANG Liang-liang, WANG Zhan-chang, CHEN Jun-de, LIN Peng, YANG Zhi-wei, LIN Yi-ming
Structure      13C NMR   碳谱模拟图
4 .     stigmasta-5,22-dien-3β-hydroxy-7-one
    相似度:93.1%
China Journal of Chinese Materia Medica          2010          35          1137-1141
Ethyl acetate-soluble chemical constituents from whole plants of Senecio chrysanthemoides
LIN Sheng; ZHANF Zhongxiao; SHEN Yunheng; LI Huiliang; SHAN Lei; LIU Runhui; XU Xike; ZHANF Weidong
Structure      13C NMR   碳谱模拟图
5 .     3β-hydroxy-stigmast-5,22-dien-7-one
C29H46O2     相似度:93.1%
Chinese Traditional and Herbal Drugs          2007          38          340-342
Chemical constituents from stems of Clematis armandii (Ⅰ)
YAN Li-hua; XU Li-zhen; ZOU Zhong-mei; YANG Shi-lin
Structure      13C NMR   碳谱模拟图
6 .     3β-hydroxystigmasta-5,22-dien-7-one
    相似度:93.1%
Chinese Traditional and Herbal Drugs          2005          36          328-332
Chemical constituents of Schefflera venulosa and their antitumor activities
LIU Rui; GU Qian-qun; CUI Cheng-bin; HAN Bing; CAI Bing; LIU Hong-bing
Structure      13C NMR   碳谱模拟图
7 .     7β-hydroxy-4,22-stigmastadien-3-one
C29H46O2     相似度:93.1%
Pharmazie          2002          57          212-214
A new cytotoxic stigmastane steroid from Pistia stratiotes
S. N. Ayyad
Structure      13C NMR   碳谱模拟图
8 .     7β-hydroxy-4,22-stigmastadien-3-one
C29H46O2     相似度:93.1%
Pharmazie          2002          57          212-214
A new cytotoxic stigmastane steroid from Pistia stratiotes
S. N. Ayyad
Structure      13C NMR   碳谱模拟图
9 .     (20R)-3β-hydroxystigmasta-5,22-dien-7-one
C29H46O2     相似度:93.1%
Chinese Journal of Natural Medicines          2013          11          74-76
A new guaiane-type sesquiterpene lactone from the Chinese liverwort Porella acutifolia subsp. tosana
LI Rui-Juan, GUO Dong-Xiao, LOU Hong-Xiang*
Structure      13C NMR   碳谱模拟图
10 .     3β-hydroxy-stigmast-5,22-dien-7-one
    相似度:93.1%
Chinese Traditional and Herbal Drugs          2011          42          251-254
Chemical constituents of Omphalia lapidescens
XU Ming-feng, SHEN Lian-qing, WANG Kui-wu
Structure      13C NMR   碳谱模拟图
11 .     3β-Hydroxystigmasta-5,22-dien-7-one
C29H46O2     相似度:92.8%
Steroids          2002          67          291-304
The synthesis of spermine analogs of the shark aminosterol squalamine
Youheng Shu, Stephen R. Jones, William A. Kinney, Barry S. Selinsky
Structure      13C NMR   碳谱模拟图
12 .     3β-hydroxystigmast-5-en-7-one
C29H46O2     相似度:89.6%
China Journal of Chinese Materia Medica          2006          31          1072-1075
Chemical constituents from herb of Alternanthera philoxeroides
FANG Jinbo, DUNG Hongquan, ZHANG Yanwen, Yoshihisa Takaishi
Structure      13C NMR   碳谱模拟图
13 .     3β-hydroxystigmast-5-en-7-one
    相似度:82.7%
Chinese Pharmaceutical Journal          2008          43          897-899
Study on Steroids from the Stem of Croton caudatus Geisel.var.tomentosus Hook
WANG Yuan, ZOU Zhong-mei
Structure      13C NMR   碳谱模拟图
14 .     stigmasta-5,22,25-trien-7-on-3β-ol
C29H44O2     相似度:82.7%
Chemistry of Natural Compounds          2012          48          594-596
A novel C29 sterol from Clerodendrum cyrtophyllum
Peng Wang, Fujiang Guo, Junjie Tan, Cheng Huang and Guangyin Wang, et al.
Structure      13C NMR   碳谱模拟图
15 .     (22E)-3β-hydroxy-26,27-bisnorcholesta-5,22-diene-7,24-dione
    相似度:81.4%
Journal of Natural Products          1993          Vol 56          282
Marine Sterols. Side-Chain-Oxygenated Sterols, Possibly of Abiotic Origin, from the New Caledonian Sponge Stelodoryx chlorophylla
Francesco de Riccardis, Luigi Minale, Maria Iorizzi, Cécil Debitus, Claude Lévi
Structure      13C NMR   碳谱模拟图
16 .     ergosta-5,24(28)-dien-7-one,3β-hydroxy
    相似度:81.4%
Chinese Pharmaceutical Journal          2010          45          420-422
Chemical Constituents of Gorgonian Coral Paraplexaura sp. from South China Sea
LI Ting, LIAO Xiao-jian, XU Shi-hai
Structure      13C NMR   碳谱模拟图
17 .     (22E,24S)-7α-hydroperoxystigmasta-5,22-dien-3β-ol
C29H48O3     相似度:79.3%
Planta Medica          2003          69          757-764
Anti-Platelet Aggregation and Chemical Constituents from the Rhizome of Gynura japonica
Wei-Yu Lin,Yueh-Hsiung Kuo,Ya-Ling Chang, Che-Ming Teng,Eng-Chi Wang, Tsutomu Ishikawa,Ih-Sheng Chen
Structure      13C NMR   碳谱模拟图
18 .     (7Z)-Hydroximino-24-ethylcholest-5,22-dien-3-ol
    相似度:79.3%
Steroids          2009          74          62-72
Synthesis and evaluation of some steroidal oximes as cytotoxic agents: Structure/activity studies (I)
Jian-Guo Cui, Lei Fan, Li-Liang Huang, Hong-Li Liu, Ai-Min Zhou
Structure      13C NMR   碳谱模拟图
19 .     stigmasta-5,22-dien-7-one
    相似度:79.3%
China Journal of Chinese Materia Medica          2010          35          1137-1141
Ethyl acetate-soluble chemical constituents from whole plants of Senecio chrysanthemoides
LIN Sheng; ZHANF Zhongxiao; SHEN Yunheng; LI Huiliang; SHAN Lei; LIU Runhui; XU Xike; ZHANF Weidong
Structure      13C NMR   碳谱模拟图
20 .     (22E,24R)-ergosta-5,22-dien-3β-hydroxyl-7-one
    相似度:78.5%
Natural Product Research and Development          2007          19          605-609
Study on the Chemical Constitutes of Hydnellum concrescens
YANG Xiao-long;WANG Fei; SHAO Hong-jun; DONG Ze-jun; DING Zhi-hui; YANG Wan-qiu; LIU Ji-kai
Structure      13C NMR   碳谱模拟图
21 .     gelliusterol C
C27H40O2     相似度:77.7%
Journal of Natural Products          2001          64          741-744
Gelliusterols A-D, New Acetylenic Sterols from a Sponge, Gellius Species
Winklet A. Gallimore, Michelle Kelly, and Paul J. Scheuer
Structure      13C NMR   碳谱模拟图
22 .     polasterol A
C30H48O2     相似度:76.6%
Journal of Natural Products          2000          63          1175-1177
New 24-Isopropylcholesterol and 24-Isopropenylcholesterol Sulfate from the Marine Sponge Epipolasis Species
Akemi Umeyama, Kanako Adachi, Seiichi Ito, and Shigenobu Arihara
Structure      13C NMR   碳谱模拟图
艰难困苦,玉汝于成。
2楼2013-03-12 13:04:45
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