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fantasy2047木虫 (正式写手)
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[求助]
求助微谱
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1 打谱溶剂吡啶 17.3,17.3,17.5,17.6,17.8,18.8,22.3,23.2,25.8,26.7,27.8,30.8,31.0,32.2,36.1,39.4,39.7,40.0,41.2,46.0,49.1,49.6,51.4,51.7,60.9,62.9,63.1,69.5,70.2,71.7,72.3,72.4,72.6,74.2,74.6,75.2,78.2,78.3,78.4,78.7,79.2,79.4,83.3,101.9,126.0,130.9 1 打谱溶剂 16.5,17.4,17.5,17.6,17.6,22.6,22.8,25.8,26.7,28.2,32.0,39.4,40.4,43.3,47.6,48.9,50.1,50.7,61.8,67.7,70.9,78.4,130.8 |
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wq0616
铁杆木虫 (正式写手)
- 应助: 323 (大学生)
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- 虫号: 2001721
- 注册: 2012-09-14
- 性别: MM
- 专业: 中药炮制
【答案】应助回帖
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感谢参与，应助指数 +1
jiangchunyong: 金币+1, 谢谢 2013-03-01 13:29:35
感谢参与，应助指数 +1
jiangchunyong: 金币+1, 谢谢 2013-03-01 13:29:35
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化合物1： 1 . ginsenoside-Re 相似度:95.8% Chemical & Pharmaceutical Bulletin 1986 34 4368-4372 Saponins of Plants of Panax Species Collected in Central Nepal and Their Chemotaxonomical Significance. II TOSHINOBU MORITA,YUN-CHEUNG KONG,PAUL PUI-HAY BUT,KAM-HUNG NG,TAI-TUNG YIP,RYOJI KASAI and OSAMU TANAKA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . compound 5 相似度:95.8% Acta Pharmaceutica Sinica 1989 Vol 24 633-636 FURTHER STUDY ON DAMMARANE SAPONINS OF LEAVES OF PANAX JAPONICUS VAR.MAJOR COLLECTED IN QINLING M OUNTAINS CHINA DQ Wang; BS Feng; XB Wang; CR Yang and J Zhou Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . Ginsenoside Re 相似度:95.8% Natural Product Sciences 2008 14 171-176 Ginsenosides from the Roots of Korean Cultivated-Wild Ginseng Yang, Min-Cheol; Seo, Dong-Sang; Hong, Jong-Ki; Hong, Sung-Hyun; Kim, Young-Choong; Lee, Kang-Ro Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . ginsenoside-Re 相似度:95.8% Phytochemistry 1989 28 1855-1858 Dammarane and oleanane saponins from callus tissue of Panax japonicus Naomi Fujioka,Hiroshi Kohda,Kazuo Yamasaki,Ryoji Kasai,Yukihiro Shoyama,Itsuo Nishioka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . ginsenoside-Re 相似度:95.8% Phytochemistry 1989 28 1855-1858 Dammarane and oleanane saponins from callus tissue of Panax japonicus Naomi Fujioka,Hiroshi Kohda,Kazuo Yamasaki,Ryoji Kasai,Yukihiro Shoyama,Itsuo Nishioka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . ginsenoside-Re 相似度:95.8% Phytochemistry 1978 17 1353-1358 Dammarane saponins of leaves of Panax pseudo-ginseng subsp. himalaicus Osamu Tanaka, Shoji Yahara Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . ginsenoside Rg1 C42H72O14 相似度:95.8% Chinese Traditional and Herbal Drugs 2010 41 1060-1065 Chemical components of active fractions from Qili Qiangxin Capsula LIU Yi-xun; YU He-shui; KANG Li-ping; ZOU Peng; JIA Ji-ming; WANG Hong-tao ZHENG Ya-jie; TIAN Shu-yan; WU Yi-ling; MA Bai-ping Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . ginsenoside Re 相似度:95.8% Chinese Pharmaceutical Journal 2008 43 412-415 Study on Isolation and Structural Elucidation of Ginsenosides from Transgenic Crown Gall of Panax quinquefolium ZHU Jian-hua YU Rong-min YAN Chun-yan SONG Li-yan ZHAO Yu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . ginsenoside Re 相似度:95.8% Natural Product Research and Development 2006 18 549-554 A Further Investigation on the Chemical Constituents from the Leaves of Panax notoginseng LI Hai-zhou; ZHANG Ying-jun; YANG Chong-ren* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . ginsenoside-Re 相似度:93.7% China Journal of Chinese Materia Medica 1992 17 96-98 A sttudy on the Saponisns in Fruits Pedicels of Panax notoginseng (Burk.)F.H.Chen Wei Junxian and Cao Shuming Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . ginsenoside-Re 相似度:93.7% Magnetic Resonance in Chemistry 2002 40 483-488 Complete assignment of 1H and 13C NMR data for nine protopanaxatriol glycosides Rongwei Teng, Haizhou Li, Jiangtao Chen, Dezu Wang, Yineng He and Chongren Yang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . compound 8a 相似度:89.7% Tetrahedron Letters 2003 44 5661-5664 Regioselective acylation of ginsenosides by Novozyme 435 Rongwei Teng, Chingseng Ang, David McManus, David Armstrong, Shaiolim Mau, Antony Bacic Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . notoginsenoside M C48H82O19 相似度:89.5% Chemical & Pharmaceutical Bulletin 2001 49(11) 1452-1456 Bioactive Saponins and Glycosides. XIX.1) Notoginseng (3):Immunological Adjuvant Activity of Notoginsenosides and Related Saponins: Structures of Notoginsenosides-L, -M, and -N from the Roots of Panax notoginseng (BURK.) F. H. CHEN. Masayuki YOSHIKAWA,Toshio MORIKAWA, Kenichi YASHIRO, Toshiyuki MURAKAMI, and Hisashi MATSUDA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . Ginsenoside Re1 C48H82O19 相似度:89.5% Journal of Agricultural and Food Chemistry 2011 59 200-205 Protopanaxatriol-Type Ginsenosides from the Root of Panax ginseng Guo-Yuan Zhu, Ying-Wei Li, Desmond Kwok-Po Hau, Zhi-Hong Jiang, Zhi-Ling Yu, and Wang-Fun Fong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . ginsenoside-Rg2 相似度:89.1% Planta Medica 1990 56 298-300 A New Minor Saponin from the Leaves of Panax ginseng ShaolinZhang,Tadahiro Takeda, TinruZhu, Yingjie Chen, Xinsheng Yao, Osamu Tanaka, and Yukio Ogihara Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . compound 8b 相似度:89.1% Tetrahedron Letters 2003 44 5661-5664 Regioselective acylation of ginsenosides by Novozyme 435 Rongwei Teng, Chingseng Ang, David McManus, David Armstrong, Shaiolim Mau, Antony Bacic Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . pseudoginsenoside-RS1 相似度:88% Chemical & Pharmaceutical Bulletin 1986 34 4368-4372 Saponins of Plants of Panax Species Collected in Central Nepal and Their Chemotaxonomical Significance. II TOSHINOBU MORITA,YUN-CHEUNG KONG,PAUL PUI-HAY BUT,KAM-HUNG NG,TAI-TUNG YIP,RYOJI KASAI and OSAMU TANAKA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . floralginsenoside I C48H82O20 相似度:87.5% Heterocycles 2007 71 577-588 Structures of Dammarane-Type Triterpene Triglycosides from the Flower Buds of Panax ginseng Seikou Nakamura, Sachiko Sugimoto, Hisashi Matsuda, and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . floralginsenoside J C48H82O20 相似度:87.5% Heterocycles 2007 71 577-588 Structures of Dammarane-Type Triterpene Triglycosides from the Flower Buds of Panax ginseng Seikou Nakamura, Sachiko Sugimoto, Hisashi Matsuda, and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . Ginsenoside Re2 C48H82O19 相似度:87.5% Journal of Agricultural and Food Chemistry 2011 59 200-205 Protopanaxatriol-Type Ginsenosides from the Root of Panax ginseng Guo-Yuan Zhu, Ying-Wei Li, Desmond Kwok-Po Hau, Zhi-Hong Jiang, Zhi-Ling Yu, and Wang-Fun Fong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . notoginsenoside FP1 C47H80O18 相似度:87.2% Helvetica Chimica Acta 2008 Vol. 91 60 Two New Dammarane-Type Bisdesmosides from the Fruit Pedicels of Panax notoginseng Xian-You Wang, Dong Wang, Xiao-Xia Ma, Ying-Jun Zhang, and Chong-Ren Yang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . notoginsenoside-R1 相似度:87.2% China Journal of Chinese Materia Medica 1992 17 96-98 A sttudy on the Saponisns in Fruits Pedicels of Panax notoginseng (Burk.)F.H.Chen Wei Junxian and Cao Shuming Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . floralginsenoside La C48H82O19 相似度:87.2% Heterocycles 2007 71 577-588 Structures of Dammarane-Type Triterpene Triglycosides from the Flower Buds of Panax ginseng Seikou Nakamura, Sachiko Sugimoto, Hisashi Matsuda, and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 化合物2： 1 . (3S,4R,5S,9S,10S,11S)-3-S-(1,2-Dimercaptoethyl)morelian-1,7-dione 1-ethylenedithioketal C19H30OS4 相似度:60.8% Journal of Natural Products 2004 67 189-193 Preparation of Moreliane-Derived Volatile Sesquiterpenes Carlos M. Cerda-Garca-Rojas, Mara A. Bucio, Luisa U. Romn, Juan D. Hernndez, and Pedro Joseph-Nathan Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . 3β-hydroxyetio-17β-dammaranic acid C23H38O3 相似度:60.8% Chinese Chemical Letters 2011 22 1461-1464 Two new dammarane-type sapogenins from Gynostemma pentaphyllum Xia Li,Jia Qing Cao,Lin Shi,Yu Qing Zhao Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . compound 1a 相似度:60.8% Acta Chimica Sinica 1989 47 258-261 Studies on the Novel Diterpenoic Constituents of TU-JIN-PI IV. Isolation and Identification of Pseudolaric Acid D and Pseudolaric Acid E Li Zhu-Lian; Chen Ke; Pan De-Ji; Xu Gnang-Yi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . 3β-hydroxy-4,4,14α-trimethyl-5α-pregna-7,9(11)-diene-20S-carboxylic acid C25H38O3 相似度:57.6% Journal of the Chemical Society, Perkin Transactions 1 1984 1219-1221 New metabolic products of Verticillium lecanii. Part 2. 3β,12β,-Dihydroxy-4,4,14α-trimethyl-5α-pregna-7,9(11)-diene-20S-carboxylic acid and 4,4,14α-trimethyl-3-oxo-5α-pregna-7,9(11)-diene-20S-carboxylic acid John Frederick Grove Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . 3β-hydroxy-20,20-(ethylenedioxy)-22,23,24,25,26,27-hexanordammarane C29H48O3 相似度:57.6% The Journal of Organic Chemistry 1999 64 9587-9595 The Fluorine Atom as a Cation-Stabilizing Auxiliary in Biomimetic Polyene Cyclizations: Total Synthesis of dl-Dammarenediol1 William S. Johnson, William R. Bartlett, Boris A. Czeskis, Arnaud Gautier, Cheol H. Lee, Rémy Lemoine, Eric J. Leopold, Gregory R. Luedtke, and Katherine J. Bancroft Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . scutellaric acid 相似度:57.6% Lishizhen Medicine and Materia Medica Research 2005 16 620-621 Studies on the Chemical Constituents of Scutellaria barbata TAO Shu-hong; WU Feng-e Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . Ocotillol-II C30H52O3 相似度:57.1% Phytochemistry 1993 32 472-474 Lup-20(29)-en-3β,15α-diol and ocotillol-II from the stem bark of Phyllanthus flexuosus Reiko Tanaka, Kimiyo Masuda, Shunyo Matsunaga Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 19α-Hydroxyasiatic acid C30H50O4 相似度:57.1% Natural Product Research and Development 2012 24 757-760 Chemical Constituents from Stems of Rhododendron delavayi Franch. XU Jin-jin; WANG Yue-hu; WANG Hong-sheng; WANG Huan; HUANG Qiao-qin; LONG Chun-lin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . ent-(16S)-1α,14α-Diacetoxy-7β-hydroxy-17-methoxykauran-15-one C25H38O7 相似度:56.5% Chemical & Pharmaceutical Bulletin 2005 53(3) 296-300 Cytotoxic Diterpenoids from Vietnamese Medicinal Plant Croton tonkinensis GAGNEP. Phan Minh GIANG,Phan Tong SON,Yumi HAMADA,and Hideaki OTSUKA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . caldaphnidine Q C23H37NO3 相似度:56.5% Journal of Natural Products 2008 71(10) 1663-1668 Alkaloids from the Twigs of Daphniphyllum calycinum Chuan-Rui Zhang, Sheng-Ping Yang, and Jian-Min Yue Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . (+)-17-oxocycloprotobuxine C23H37NO 相似度:56.5% Journal of Natural Products 1999 62 665-669 New Steroidal Alkaloids from the Roots of Buxus sempervirens Atta-ur-Rahman, Athar Ata, Samina Naz, M. Iqbal Choudhary, Bilge Sener, and Songul Turkoz Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . di-6-epi-3-anhydroophiobolin B 相似度:56.5% Journal of Natural Products 1999 62 895-897 Characterization of 6-epi-3-Anhydroophiobolin B from Cochliobolus heterostrophus Xiaoyu Shen, Stuart B. Krasnoff, Shun-Wen Lu, Chuck D. Dunbar, James O’Neal, B. Gillan Turgeon, Olen C. Yoder, Donna M. Gibson, and Mark T. Hamann Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 16,17-dihydro-12b,16b-epoxyna-pelline C22H33NO3 相似度:56.5% Planta Medica 2005 71 1073-1076 Three New Diterpene Alkaloids from the Roots of Aconitum nagarum var.lasiandrum Fan Zhang , Shu-Lin Peng , Xun Liao , Kai-Bai Yu , Li-Sheng Ding Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . isopropylidenkirenol C23H38O4 相似度:56.5% Planta Medica 1991 57 396-396 Diterpene aus Siegesbeckia glabrescens Diterpenes from Siegesbeckia glabrescens K Liu and E. Roder Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . lepenine C22H33NO 相似度:56.5% Chemistry of Natural Compounds 1996 32 596-675 ALKALOIDS. PLANTS, STRUCTURES, PROPERTIES" Chapter 2, continued R. Shakirov, M. V. Telezhenetskaya, I. A. Bessonova,S. F. Aripova, I. A. Israilov, M. N. Sultankhodzhaev,V. I. Vinogradova, V. I.Akhmedzhanova, T. S. Tulyaganov,B. T. Salimov, and V. A. Tel'nov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . Lepenine C22H33N03 相似度:56.5% Chemistry of Natural Compounds 1992 28 388-389 ALKALOIDS OF THE MONGOLIAN FLORA I. ALKALOIDS OF THE EPIGEAL PART OF Aconitum barbatum N. Batbayar, D. Batsuren, and M. N. Sultankhodzhaev Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . ent-7α-15β,16β-epoxykaurane C22H32O2 相似度:56.5% Natural Product Research 2002 16 33-37 Diterpenes from Sideritis Trojana Gülaçti Topçu; Ahmet Gören; Turgut Kılİç; Y. Kemal YıLdız; Gülendam Tümen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . compound 1a C22H34O3 相似度:56.5% Natural Product Research 2007 21 135-140 New diterpenoids from Calceolaria polifolia Juan A. Garbarino; Marisa Piovano; M. Cristina Chamy; Luis Espinoza Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . strophanthidin C23H32O6 相似度:56.5% Journal of Natural Products 2010 73 338-345 Occurrence of Progesterone and Related Animal Steroids in Two Higher Plants' Guido F. Pauli, J. Brent Friesen, Tanja Gödecke, Norman R. Farnsworth and Bernhard Glodny Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . GA14 dimethyl ester 16α,17-epoxide 相似度:56.5% Phytochemistry 1992 31 1869-1877 Gibberellins A82 and A83 in seed of Lupinus albus Paul Gaskin, Gordon V. Hoad, Jake Macmillan, Ian K. Makinson, Jo E. Readman Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . ent-labdan-8β,18β-diol-15-al 相似度:56.5% Phytochemistry 1992 31 3274-3276 Diterpenoids from Baccharis neaei Francesca Faini, Cecilia Labbe, M.Inés Polanco Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . (10a'S)-2',3',5',6',7',10'-Hexahydro-10a'H-spiro[1,3-dithiolane-2,1'-pyrrolo[1,2-a]azocine]-10a'-carboxylic acid menthyl ester C23H37NOS2 相似度:56.5% Heterocycles 2006 68 47-58 Concise Highly Enantioselective Cascade Synthesis of Azacyclooctene Alkaloids with a Quaternary Stereocenter Daniele Muroni, Antonio Saba,* and Nicola Culeddu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . mansumbinol C22H36O 相似度:56.5% Phytochemistry 1986 25 917-922 The mansumbinanes: Octanordammaranes from the resin of Commiphora incisa Gordon J. Provan, Peter G. Waterman Structure 13C NMR 碳谱模拟图 |
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