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谈判陶荣誉版主 (文坛精英)
如切如磋，如琢如磨
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化合物1： 208.07,165.20,145.70,143.95,142.44,125.40,113.15,113.04,82.09,42.81,41.55,29.68,28.34,27.33,26.41,24.08,22.47,22.34,18.1 化合物2： 208.97,165.27,153.25,148.93,148.89,148.77,131.56,130.87,128.82,123.50,123.45,122.57,119.95,119.04,112.24,111.13,110.31,110.15,107.02,104.37,78.04,76.30,65.54,60.78,56.27,56.19,56.04,56.00,55.95,55.86,52.94，52.50,30.57,29.66,28.49,13.69,13.64,12.82 化合物3： 209.39,164.96,153.42,153.03,133.61,130.88,128.85,124.88,107.11,104.47,78.62,65.55,60.91,60.80,56.31,56.23,52.50,30.6,28.49,19.19,13.69 打谱溶剂均为氘代氯仿 多谢各位了！ |
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2楼2013-01-25 16:57:05
谈判陶
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化合物1： 18.1,22.34,22.47,24.08,26.41,27.33,28.34,29.68,41.55,42.81,82.09 ,113.04,113.15,125.40,142.44,143.95,145.70,165.20,208.07 化合物2： 12.82,13.64,13.69,28.49,29.66,30.57,52.50,52.94,55.86,55.95,56.00 ,56.04,56.19,56.27,60.78,65.54,76.30,78.04,104.37,107.02,110.15,110.31,111.13,112.24,119.04,119.95,122.57,123.45,123.50,128.82,130.87,131.56,148.77,148.89,148.93,153.25,165.27,208.97 化合物3： 13.6,19.19,28.49,30.6,52.50,56.23,56.31,60.80,60.91,65.55,78.62,104.47,107.11,124.88,128.85,130.88,133.61,153.03,153.42,164.96,209.39 打谱溶剂均为氘代氯仿 一般打谱溶剂要写吗？ |
3楼2013-01-25 18:10:45
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化合物1 1 . puctatene C20H34O2 相似度:60% Tetrahedron 2005 61 8910-8915 Isolation of naturally occurring dactylomelane metabolites as Laurencia constituents José J. Fernández, María L. Souto, Laura V. Gil, Manuel Norte Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . puctatene C20H34O2 相似度:60% Tetrahedron 2005 61 8910-8915 Isolation of naturally occurring dactylomelane metabolites as Laurencia constituents José J. Fernández, María L. Souto, Laura V. Gil, Manuel Norte Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 3-Hydroxybakuchiol 相似度:57.8% Phytochemistry 1996 42 1299-1303 Bakuchiol derivatives from the leaves of Psoralea glandulosa Cecilia Labbé, Francesca Faini, Joseph Coll, Joseph D. Connolly Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . 9α-hydroxycallicarpic acid A C20H30O3 相似度:55% Journal of Natural Products 2009 72 223-228 seco-Abietane Diterpenoids, a Phenylethanoid Derivative, and ntitubercular Constituents from Callicarpa pilosissima Jih-Jung Chen Hung-Ming Wu, Chien-Fang Peng,Ih-Sheng Chen, and Shih-Der Chu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . 6-hydroxysalvonolone C20H26O4 相似度:55% Chemistry of Natural Compounds 2008 44 824-825 DITERPENES AND STEROLS FROM THE ROOTS OF Salvia verbenaca subsp. Clandestina A. Kabouche, Z. Kabouche,R. Touzani, and C. Bruneau Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . 8,10-dihydroxy-iso-depressin C20H30O3 相似度:55% Journal of Natural Products 2010 73 133-138 Rare Casbane Diterpenoids from the Hainan Soft Coral Sinularia depressa Yan Li, Marianna Carbone, Rosa Maria Vitale, Pietro Amodeo, Francesco Castelluccio, Giovanna Sicilia, Ernesto Mollo, Michela Nappo, Guido Cimino, Yue-Wei Guo and Margherita Gavagnin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 14-Deoxycoleon U C20H26O4 相似度:55% Journal of Agricultural and Food Chemistry 2005 53 5200-5206 Diterpenes from Salvia broussonetii Transformed Roots and Their Insecticidal Activity Braulio M. Fraga, Carmen E. Díaz, Ana Guadaño, and Azucena González-Coloma Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . omphadiol C15H26O2 相似度:52.6% Journal of Natural Products 2000 63 1557-1559 Sesquiterpenes from the Basidiomycete Omphalotus illudens Trevor C. McMorris, Ricardo Lira, Peter K. Gantzel, Michael J. Kelner, and Robin Dawe Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . 4-Bromo-17β-estradiol 相似度:52.6% Steroids 2006 71 618-631 Estrogen conjugation and antibody binding interactions in surface plasmon resonance biosensing John S. Mitchell, Yinqiu Wu, Christian J. Cook, Lyndsay Main Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . (-)-2'-isovaleryloxy-l'-2'-dihydroxanthyletin 相似度:52.6% Journal of Natural Products 1989 Vol 52 888 Tortuoside, A New Natural Coumarin Glucoside from Seselitortuosum Paolo Ceccherelli, Massimo Curini, Maria Carla Marcotullio, Gianfederico Madruzza, Alessandro Menghini 化合物2: 1 . heptamethyl ether of proanthocyanidin A-2 相似度:55.2% Phytochemistry 1999 51 297-308 A-type proanthocyanidins from peanut skins Hongxiang Lou, Yoshimitsu Yamazaki, Tsutomu Sasaki, Masaru Uchida, Hideoki Tanaka, Syuichi Oka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . heptamethyl ether of epicatechin-(2β→O→7, 4β→8)-ent-epicatechin C37H38O12 相似度:55.2% Phytochemistry 1999 51 297-308 A-type proanthocyanidins from peanut skins Hongxiang Lou, Yoshimitsu Yamazaki, Tsutomu Sasaki, Masaru Uchida, Hideoki Tanaka, Syuichi Oka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . heptamethyl ether of epicatechin-(2β→O→7,4β→6)-ent-epicatechin 相似度:55.2% Phytochemistry 1999 51 297-308 A-type proanthocyanidins from peanut skins Hongxiang Lou, Yoshimitsu Yamazaki, Tsutomu Sasaki, Masaru Uchida, Hideoki Tanaka, Syuichi Oka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . herveline A C39H44N2O7 相似度:53.8% Tetrahedron 1995 51 1221-1228 A new group of isoquinoline dimers from Hernandia voyronii Philippe Rasoanaivo, Suzanne Ratsimamanga-Urverg, Corrado Galeffi, Marcello Nicoletti, François Frappier, Marie-Thérèse Martin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . hexamethyl ether of epicatechin-(2β→O→7, 4β→8)-ent-epicatechin 相似度:52.6% Phytochemistry 1999 51 297-308 A-type proanthocyanidins from peanut skins Hongxiang Lou, Yoshimitsu Yamazaki, Tsutomu Sasaki, Masaru Uchida, Hideoki Tanaka, Syuichi Oka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . heptamethyl ether of epicatechin-(2β→O→7, 4β→6)-catechin C37H38O12 相似度:52.6% Phytochemistry 1999 51 297-308 A-type proanthocyanidins from peanut skins Hongxiang Lou, Yoshimitsu Yamazaki, Tsutomu Sasaki, Masaru Uchida, Hideoki Tanaka, Syuichi Oka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . cis-N-[1,2-bis-(3',4'-dimethoxyphenyl)-9,10-dimethoxy-4-oxo-3,4,6,7-tetrahydro-2H-pyrido[2,1-a]isoquinolin-3-yl]benzamide C38H38N2O8 相似度:52.6% Tetrahedron 2012 68 2864-2875 Synthesis of benzoindoloquinolizines via a Cu(I)-mediated C–N bond formation Rattana Worayuthakarn, Prattya Nealmongkol, Somsak Ruchirawat, Nopporn Thasana Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . Methyl 2-(3-(2,5-dimethoxyphenyl)propanoyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-3-carboxylate C24H29NO7 相似度:52.3% Tetrahedron 2012 68 2027-2040 Electronically rich N-substituted tetrahydroisoquinoline 3-carboxylic acid esters: concise synthesis and conformational studies Rami A. Al-Horani, Umesh R. Desai Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . fauripavine C39H42N2O8 相似度:51.2% Journal of Natural Products 1999 62 803-810 Four Dimeric Aporphine-Containing Alkaloids from Thalictrum fauriei1 Shoei-Sheng Lee and Raymond W. Doskotch Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . Methyl-2-(2-(2,5-dimethoxy phenyl) acetyl)-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-3-carboxylate C23H27NO7 相似度:51.2% Tetrahedron 2012 68 2027-2040 Electronically rich N-substituted tetrahydroisoquinoline 3-carboxylic acid esters: concise synthesis and conformational studies Rami A. Al-Horani, Umesh R. Desai Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . Labd-8(17)-en-15,19-dioic acid,15,19-ditryptophanyl ethyl ester amide C46H60N4O6 相似度:51.1% Molecules 2010 15 7378-7394 Synthesis, Gastroprotective Effect and Cytotoxicity of New Amino Acid Diterpene Monoamides and Diamides Guillermo Schmeda-Hirschmann, Mariano Walter Pertino, Jaime A. Rodriguez, Francisco Monsalve, Daniel Droguett and Cristina Theoduloz 化合物3： 1 . tsangin C C24H30O9 相似度:76.1% Journal of Natural Products 2011 74 1875-1880 Anti-inflammatory Endiandric Acid Analogues from the Roots of Beilschmiedia tsangii Yun-Ting Huang, Hsun-Shuo Chang, Guei-Jane Wang, Ming-Jen Cheng, O Chu-Huang Chen, Yi-Jen Yang, and Ih-Sheng Chen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . tsangin A C23H26O9 相似度:60.8% Planta Medica 2006 72 351-357 New Cytotoxic Tetrahydrofuran- and Dihydrofuran-Type Lignans from the Stem of Beilschmiedia tsangii Jih-Jung Chen,En-Tzu Chou,Chang-Yih Duh,Sheng-Zehn Yang,Ih-Sheng Chen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . tsangin B C23H26O9 相似度:59.0% Planta Medica 2006 72 351-357 New Cytotoxic Tetrahydrofuran- and Dihydrofuran-Type Lignans from the Stem of Beilschmiedia tsangii Jih-Jung Chen,En-Tzu Chou,Chang-Yih Duh,Sheng-Zehn Yang,Ih-Sheng Chen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . colchicine C22H25NO6 相似度:59.0% Acta Botanica Yunnanica 1999 21(3) 364-368 Alkaloids from the Flowers of Colchicum autumnale HE Hong-Ping,LIU Fu-Chu, HU Lin,ZHU Hong-You Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . cispervilleine B C30H37NO10 相似度:57.1% Journal of Natural Products 2006 69(3) 414-417 Tropane Aromatic Ester Alkaloids from a Large-Scale Re-collection of Erythroxylum pervillei Stem Bark Obtained in Madagascar Young-Won Chin, William P. Jones, Timothy J. Waybright, Thomas G. McCloud,Philippe Rasoanaivo, Gordon M. Cragg, John M. Cassady, and A. Douglas Kinghorn Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . 2-(2,3,4,6-tetramethoxyphenyl)-5-(E)-propenylbenzofuran 相似度:57.1% Phytochemistry 1987 26 2041-2043 Ramosissin and other methoxylated nor-neolignans from Krameria ramosissima Hans Achenbach,Johann Grob,Xorge A. Dominguez,Julia Verde Star,Fernando Salgado Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . catuabine B C25H29NO7 相似度:57.1% Chemistry & Biodiversity 2011 8 155-165 Tropane Alkaloids from Erythroxylum caatingaePlowman Steno L. de Oliveira, Josean F. Tavares, Marianna V. S. Castello Branco, Hellane F. S. Lucena, José M. Barbosa-Filho, Maria de F. Agra, Silene C. do Nascimento, Jaciana dos S. Aguiar, Teresinha G. da Silva, Carlos A. de Simone, João X. de Araújo-Júnior an Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . pervilleine B C30H37NO10 相似度:56% Journal of Natural Products 2001 64 1514-1520 Modulation of the Multidrug-Resistance Phenotype by New Tropane Alkaloid Aromatic Esters from Erythroxylum pervillei Gloria L. Silva,Baoliang Cui,Daniel Chávez, Min You,Hee-Byung Chai, Philippe Rasoanaivo,Sean M. Lynn,X Melanie J. O’Neill,X Jane A. Lewis, Jeffrey M. Besterman,Anne Monks,Norman R. Farnsworth, Geoffrey A. Cordell, John M. Pezzuto,and A. Douglas Kinghorn Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . colchicine 相似度:54.5% Helvetica Chimica Acta 1980 63 406-412 Revision of the Structure of 'Epoxycolchicine' Arnold Brossi, Manfred Rösner, James V. Silverton, Maria A. Iorio, Charles D. Hufford Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . colchicine 相似度:54.5% Journal of Natural Products 1988 Vol 51 88 Nmr Studies of Colchicine and its Photoisomers, β- and λ-Lumicolchicines Duangdeun Meksuriyen, Lee-Juian Lin, Geoffrey A. Cordell, Sibabrata Mukhopadhyay, Sunil K. Banerjee |
4楼2013-01-26 10:56:10
