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chenjjun1982木虫 (著名写手)
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[求助]
求微谱数据,谢谢,非常感谢
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碳谱数据1: 12.9, 15.2, 19.6, 21.7, 25.8, 31.2, 32.4, 38.4, 43.9, 46.3, 46.5, 49.4, 54.9, 59.3, 62.2, 70.0, 73.4, 75.9, 77.7, 99.1, 100.5, 116.5, 137.9, 148.1, 148.4, 188.1, 192.7, 198.8 碳谱数据2: 15.7, 16.0, 16.9, 19.4, 23.7, 26.2, 27.9, 28.9, 30.0, 33.7, 34.7, 43.6, 50.9, 209.6 |
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wq0616
铁杆木虫 (正式写手)
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chenjjun1982: 金币+5, ★★★★★最佳答案, 非常感谢 2013-01-25 08:56:45
感谢参与，应助指数 +1
chenjjun1982: 金币+5, ★★★★★最佳答案, 非常感谢 2013-01-25 08:56:45
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化合物1： 1 . picrasinoside B 相似度:85.7% Journal of Natural Products 1991 Vol 54 844 Picrasinoside H, a New Quassinoid Glucoside, and Related Compounds from the Stem Wood of Picrasma ailanthoides Takayuki Matsuzaki, Narihiko Fukamiya, Masayoshi Okano, Tomoyuki Fujita, Kiyoshi Tagahara, Kuo-Hsiung Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . picrasinoside-C C22H34O6 相似度:64.2% Bulletin of the Chemical Society of Japan 1985 58 1793-1800 New Quassinoid Glucosides, Picrasinoside-A, -B, -C, -D, -E, -F, and -G and New Hemiacetals, Picrasinol-A and -B, from the Stem Bark of Picrasma ailanthoides PLANCHON Masayoshi Okano, Tomoyuki Fujita, Narihiko Fukamiya, Takaaki Aratani Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . javanicinoside C C27H38O11 相似度:60.7% Phytochemistry 1990 29 2617-2621 Quassinoids from Picrasma javanica Kazuo Koike,Taichi Ohmoto Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . javanicinoside J C29H44O13 相似度:58.6% Journal of Natural Products 1992 Vol 55 482 New Quassinoid Glucosides, Javanicinosides I, J, K, and L, from Picrasma javanica Kazuo Koike, Taichi Ohmoto Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . picrasinoside C 相似度:57.1% Journal of Natural Products 1991 Vol 54 844 Picrasinoside H, a New Quassinoid Glucoside, and Related Compounds from the Stem Wood of Picrasma ailanthoides Takayuki Matsuzaki, Narihiko Fukamiya, Masayoshi Okano, Tomoyuki Fujita, Kiyoshi Tagahara, Kuo-Hsiung Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . javanicinoside L C27H42O12 相似度:57.1% Journal of Natural Products 1992 Vol 55 482 New Quassinoid Glucosides, Javanicinosides I, J, K, and L, from Picrasma javanica Kazuo Koike, Taichi Ohmoto Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . picrasinoside H C30H44O13 相似度:56.6% Journal of Natural Products 1991 Vol 54 844 Picrasinoside H, a New Quassinoid Glucoside, and Related Compounds from the Stem Wood of Picrasma ailanthoides Takayuki Matsuzaki, Narihiko Fukamiya, Masayoshi Okano, Tomoyuki Fujita, Kiyoshi Tagahara, Kuo-Hsiung Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 11-α-O-(B-glucopyranosyl)-16-α-O-Methylneoquassin 相似度:55.1% Phytochemistry 1993 32 1007-1013 Quassinoids from Quassia amara P. Barbetti, G. Grandolini, G. Fardella, I. Chiappini Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . baimantuoluoline B C28H42O7 相似度:53.5% Helvetica Chimica Acta 2007 Vol. 90 1522 Withanolide Compounds from the Flower of Datura metel L. Bingyou Yang, Qiuhong Wang, Yonggang Xia, Weisheng Feng, and Haixue Kuang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . tomatidine 相似度:53.5% Chemical & Pharmaceutical Bulletin 1990 38 827-829 STRUCTURES OF THREE NEW STEROIDAL ALKALOID GLYCOSIDES, SOLAVERINES I, II AND III FROM SOLANUM TOXICARIUM AND S. VERBASCIFOLIUM Tomoyuki YAMASHITA,Nobuyo FUJIMURA,Shoji YAHARA,Toshihiro NOHARA,Syuji KAWANOBU and Kunimitsu FUJIEDA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . soladunalinidine C27H46N2O 相似度:53.5% Phytochemistry 1996 43 913-915 3-Aminospirosolane alkaloids from Solanum arboreum Anderson Maxwell, Ramish Pingal, William F. Reynolds, Stewart McLean Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . picrasinoside G 相似度:53.5% Journal of Natural Products 1991 Vol 54 844 Picrasinoside H, a New Quassinoid Glucoside, and Related Compounds from the Stem Wood of Picrasma ailanthoides Takayuki Matsuzaki, Narihiko Fukamiya, Masayoshi Okano, Tomoyuki Fujita, Kiyoshi Tagahara, Kuo-Hsiung Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 16-α-O-methylneoquassin 相似度:53.5% Phytochemistry 1993 32 1007-1013 Quassinoids from Quassia amara P. Barbetti, G. Grandolini, G. Fardella, I. Chiappini Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . scutalpin C C27H38O9 相似度:53.5% Phytochemistry 1993 34 1589-1594 Neo-clerodane diterpenoids from Scutellaria alpina subsp. javalambrensis Maria C. de la Torre, Benjamín Rodríguez, Maurizio Bruno, Peter Y. Malakov, Georgi Y. Papanov, Franco Piozzi, Giuseppe Savona Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . tomatidine 相似度:53.5% Phytochemistry 1980 19 299-302 Structure of solanaviol, a new steroidal alkaloid from Solanum aviculare Ko Kaneko, Kasuaki Niitsu, Naotoshi Yoshida, Hiroshi Mitsuhashi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . compound 2a 相似度:53.5% Australian Journal of Chemistry 1977 30 917-921 Carbon-13 nuclear magnetic resonance spectroscopy of naturally occurring substances. LI. Solanum glycoalkaloids RJ Weston, HE Gottlieb, EW Hagaman and E Wenkert Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . N(3)-isopropylidenesoladunalinidine 相似度:53.5% Australian Journal of Chemistry 1979 32 611-617 Soladunalinidine, a New Dibasic Analogue of Tomatidine Extracted From Solanum dunalianum GJ Bird, DJ Collins, FW Eastwood and JM Swan Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . scutalpin B C29H40O10 相似度:51.7% Phytochemistry 1993 34 1589-1594 Neo-clerodane diterpenoids from Scutellaria alpina subsp. javalambrensis Maria C. de la Torre, Benjamín Rodríguez, Maurizio Bruno, Peter Y. Malakov, Georgi Y. Papanov, Franco Piozzi, Giuseppe Savona Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . stigmastanol glucoside 相似度:51.6% Fitoterapia 2000 71 722-724 New constituents from Gliricidia sepium H.M.T.B. Herath, Susila deSilva Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . picraqualide B C25H34O9 相似度:50% Helvetica Chimica Acta 2004 Vol. 87 1591 Five New Quassinoids from the Bark of Picrasma quassioides Sheng-Ping Yang, and Jian-Min Yue Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . 2,3-dihydro-3β-methoxyixocarpalactone B C29H42O9 相似度:50% Chemical & Pharmaceutical Bulletin 2003 51(5) 530-539 Minor Withanolides from Physalis philadelphica: Structures, Quinone Reductase Induction Activities, and Liquid Chromatography (LC)-MS-MS Investigation as Artifacts Jian-Qiao GU, Wenkui LI, Young-Hwa KANG, Bao-Ning SU, Harry H. S. FONG,Richard B. VAN BREEMEN, John M. PEZZUTO, and A. Douglas KINGHORN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . tubocapsanolide A C28H36O6 相似度:50% Journal of Natural Products 2007 70 747-753 Cytotoxic Withanolides from Tubocapsicum anomalum Pei-Wen Hsieh,Zih-You Huang, Jyun-Hong Chen, Fang-Rong Chang, Ching-Chung Wu, Yu-Liang Yang,Michael Y. Chiang, Ming-Hon Yen, Shu-Li Chen,Hsin-Fu Yen, Tilo Lübken,Wen-Chun Hung,and Yang-Chang Wu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . anomanolide A C28H38O7 相似度:50% Journal of Natural Products 2007 70 747-753 Cytotoxic Withanolides from Tubocapsicum anomalum Pei-Wen Hsieh,Zih-You Huang, Jyun-Hong Chen, Fang-Rong Chang, Ching-Chung Wu, Yu-Liang Yang,Michael Y. Chiang, Ming-Hon Yen, Shu-Li Chen,Hsin-Fu Yen, Tilo Lübken,Wen-Chun Hung,and Yang-Chang Wu Structure 13C NMR 碳谱模拟图 化合物2： 1 . ent-3β-Hydroxyspathulenol 相似度:93.3% Phytochemistry 2000 53 845-849 Sesquiterpenoids and diterpenoids from the Chilean liverwort Lepicolea ochroleuca Huei-Ju Liu, Chia-Li Wu, Hans Becker, Josef Zapp Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . japodic acid C13H22O3 相似度:78.5% Records of Natural Products 2008 2 100-106 Japodic acid, A Novel Aliphatic Acid from Jatropha podagrica Hook Olapeju O. Aiyelaagbe and James B. Gloer Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 4β-dihydroeudesmol 相似度:73.3% Planta Medica 1982 46 20-22 Constituents of Local Plants XXV, Constitution of the Antispasmodic Principle of Cymbopogon proximus H. D. Locksley, M. B. E. Fayez, A. S. Radwan, V. M. Chari, G. A. Cordell and H. Wagner Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . 1-epinitraramine 相似度:71.4% Natural Product Research 1995 6 119-125 Alkaloids from Nitraria billardieri May Ying Shen; José Angelo Zuanazzi; Christiane Kan; Jean-Charles Quirion; Henri-Philippe Husson; I. R. C. Bick Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . yielded (-)-apoaromadendrone 相似度:71.4% Natural Product Research 2000 14 447-452 (-)-Ledol from Calophyllum teysmanii: Structure and Stereochemistry Shu-Geng Cao; Keng-Yeow Sim; S. H. Goh Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . (1S,10S)-9α-hydroxy-allo-aromadendrane C15H26O 相似度:66.6% Phytochemistry 2002 60 475-481 Aromadendrane transformations by Curvularia lunata ATCC 12017 Dwight O. Collins, William F. Reynolds, Paul B. Reese Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . alpinolide 相似度:66.6% Chemical & Pharmaceutical Bulletin 1987 35 2849-2859 Novel Guaiane-and Secoguaiane-Type Sesquiterpenes from Alpinia japonica (THUNB.) MIQ. HIDEJI ITOKAWA,HIROSHI MORITA,KENJI OSAWA,KINZO WATANABE and YOICHI IITAKA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . epoxycyperene C15H24O 相似度:66.6% Phytochemistry 1997 45 1435-1439 Sesquiterpenes from the essential oil of Cyperus alopecuroides Mesmin Mekem Sonwa, Wilfried A. König, Karl-Heinz Kubeczka, Otakar Motl Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . dihydroeudesmol 相似度:66.6% Australian Journal of Chemistry 1978 31 2527-2538 The Constituents of Rubus rosifolius. The Structure of Rosifoliol, a Biogenetically Significant Sesquiterpenoid I Southwell Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 5,5-Dimethyl-9-oxodecansaure-methylester C13H24O3 相似度:64.2% Helvetica Chimica Acta 1980 63 1833-1855 Photochemische Reaktionen 111. Mitteilung [1] Zur Photochemie , -ungesättigter , -Epoxyester I: Singulett- versus Triplettreaktivität Alex Peter Alder, Hans Richard Wolf, Oskar Jeger Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . cyprotene C14H24 相似度:64.2% Phytochemistry 1997 45 1435-1439 Sesquiterpenes from the essential oil of Cyperus alopecuroides Mesmin Mekem Sonwa, Wilfried A. König, Karl-Heinz Kubeczka, Otakar Motl Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . pathylactone A(synthetic) 相似度:64.2% Tetrahedron 2002 58 1647-1656 Studies on the synthesis of (±)-pathylactone A, a nor-sesquiterpene lactone isolated from marine sources Fernando Coelho, Gaspar Diaz Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . (±)-10-hydroxy-6,7-dimethyl-6-(2-oxopropyl)-1-oxaspiro[4,5]decane-2-one C14H22O4 相似度:64.2% Tetrahedron 2002 58 1647-1656 Studies on the synthesis of (±)-pathylactone A, a nor-sesquiterpene lactone isolated from marine sources Fernando Coelho, Gaspar Diaz Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . (-)-nor-aromadendr-10β-ol 相似度:64.2% Zeitschrift für Naturforschung C 2009 64 840-846 Structure-Activity Relationships of Aromadendranes in Uterus-Relaxant Activity N. Pérez-Hernández, H. Ponce-Monter, M. I. Ortiz, R. Cariño-Cortésa, and P. Joseph-Nathan Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . (6α,8α)-6-hydroxyeremophil-7(11)-en-12,8-olide C15H22O3 相似度:60% Helvetica Chimica Acta 2006 Vol. 89 915 Terpenoids from the Roots of Ligularia muliensis Qiu-Hong Wu, Chun-Mei Liu, Yan-Jun Chen, and Kun Gao Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . pentadeca-(8Z,13Z)-dien-11-yn-2-one C15H22O 相似度:60% Phytochemistry 2006 67 1359-1364 Isolation and structure elucidation of cytotoxic polyacetylenes and polyenes from Echinacea pallida Federica Pellati, Samuele Calò, Stefania Benvenuti, Barbara Adinolfi, Paola Nieri, Michele Melegari Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . 11-Hydroxy-4-oxo-tetradecanoic acid methyl ester C15H28O4 相似度:60% Journal of Natural Products 2005 68 487-492 Ipomoeassins A−E, Cytotoxic Macrocyclic Glycoresins from the Leaves of Ipomoea squamosa from the Suriname Rainforest Shugeng Cao, Rebecca C. Guza, Jan H. Wisse, James S. Miller, Randy Evans, and David G. I. Kingston Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . (9R)-9-hydroxypatchoulol C15H26O2 相似度:60% Journal of Natural Products 1999 62 437-440 Biotransformation of the Fungistatic Sesquiterpenoid Patchoulol by Botrytis cinerea Josefina Aleu, James R. Hanson, Rosario Hernández Galán, and Isidro G. Collado Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 6α-hydroxy-8βHeremophil-7(11)-en-12,8α-olide C15H22O3 相似度:60% Chinese Chemical Letters 2006 17 215-217 Two New Eremophilenolides from Ligularia muliensis Qiu Hong WU, He Xiang WANG, Kun GAO Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . curcarabranol A C15H24O3 相似度:60% Chemical & Pharmaceutical Bulletin 1998 46 1186-1188 Absolute Stereostructures of Carabrane-Type Sesquiterpenes, Curcumenone, 4S-Dihydrocurcumenone, and Curcarabranols A and B : Vasorelaxant Activity of Zedoary Sesquiterpenes Masayuki YOSHIKAWA,Toshiyuki MURAKAMI,Toshio MORIKAWA and Hisashi MATSUDA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . 6β-hydroxy-7(11)-eremophilen-12,8α-olide 相似度:60% China Journal of Chinese Materia Medica 2001 26 835-837 Constituents of Liguliria vellerea (Franch.)Hand-Mazz. LI Yunsen, LUO Shide, ZHANG Mian, CHEN Jijun, WANG Zhengtao Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . 1α,10β,11-trihydroxy-4α,5α,7β-eremophilane C15H28O3 相似度:60% Phytochemistry 1999 52 1063-1067 The hydroxylation of the sesquiterpenoid valerianol by Mucor plumbeus Simone Fontes Arantes, James R. Hanson, Peter B. Hitchcock Structure 13C NMR 碳谱模拟图 |
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