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杨大松至尊木虫 (文坛精英)
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[求助]
求助微谱数据，谢谢
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碳谱数据如下： 22.9,33.9,38.1,72.4,73.4,90.1,90.2,175.6. 辛苦各位了，非常感谢 |
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新新手
木虫 (小有名气)
- 应助: 122 (高中生)
- 金币: 3977.8
- 散金: 11
- 红花: 2
- 帖子: 245
- 在线: 67.3小时
- 虫号: 1357992
- 注册: 2011-07-31
- 性别: MM
- 专业: 中药学其他科学问题
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
karl2100: 金币+1, 多谢提供！ 2013-01-18 00:10:59
杨大松: 金币+15, ★★★★★最佳答案 2013-01-21 10:47:20
感谢参与，应助指数 +1
karl2100: 金币+1, 多谢提供！ 2013-01-18 00:10:59
杨大松: 金币+15, ★★★★★最佳答案 2013-01-21 10:47:20
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1 . threo-5-n-pentyl-4-hydroxy tetrahydrofuran-2-one 相似度:55.5% Chinese Traditional and Herbal Drugs 1998 29 580-582 Isolation and Identification of Thellungianin C and D from the Root of Thellung Pimpinella (Pimpinella thellungiana) Qiao Boling; J Tadashima; Wang Changdai; et al.(Shanxi Provincial Academy of Traditional Chinese Materia Medica; Xi-an; Mitsubishi Chemical Industries Limited); Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . N-acetyl-γ-hydroxyvaline Lactone C7H11NO3 相似度:50% Journal of Natural Products 2000 63 664-665 N-Acetyl-γ-hydroxyvaline Lactone, an Unusual Amino Acid Derivative from a Marine Streptomycete Isara L. C. Hernandez, Mirna J. L. Godinho, Alviclér Magalhães, Alexandre B. Schefer, Antonio G. Ferreira, and Roberto G. S. Berlinck Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 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Izatt Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . t-butoxycyclopentane 相似度:50% Indian Journal of Chemistry 2008 47B 575-578 A convenient synthesis of tert-butyl ethers under microwave condition Mahammed,K A; Murthy,P S Keshava; Raju,K Mohana Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . Compound S-5 C8H14O3 相似度:50% Bioorganic & Medicinal Chemistry Letters 1992 2 1713-1716 Identification and synthesis of a metabolite of KH 1060, a new potent 1α,25-dihydroxyvitamin D3 analogue Niels Rastrup Andersen, Frants A. Buchwald, Gunnar Grue-Sørensen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . Compound 4a 相似度:50% Journal of Natural Medicines 2009 63 241-247 Iridoid glucoside, (3R)-oct-1-en-3-ol glycosides, and phenylethanoid from the aerial parts of Caryopteris incana Da Peng Zhao, Katsuyoshi Matsunami and Hideaki Otsuka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . Compound 5b 相似度:50% Journal of Natural Medicines 2009 63 241-247 Iridoid glucoside, (3R)-oct-1-en-3-ol glycosides, and phenylethanoid from the aerial parts of Caryopteris incana Da Peng Zhao, Katsuyoshi Matsunami and Hideaki Otsuka Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . Compound h3 相似度:50% Magnetic Resonance in Chemistry 2008 46 1168-1174 Structural elucidation of propargylated products of 3-substituted-1, 2, 4-triazole-5-thiols by NMR techniques (pages 1168–1174) Preeti M. Chaudhary, Sayalee R. Chavan, M. Kavitha, Shailaja P. Maybhate, Sunita R. Deshpande, Anjali P. Likhite and P. R. Rajamohanan Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . 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Reeve, Samuel Suhard Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . compound 2h C17H32N2O5F6 相似度:50% Heterocycles 2000 53 1317-1328 Solution Parallel Synthesis of Cyclic Guanidines Christelle Marmillon, Jacques Bompart, Michèle Calas, Roger Escale,* and Pierre-Antoine Bonnet Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . compound 2i C25H48N2O5F6 相似度:50% Heterocycles 2000 53 1317-1328 Solution Parallel Synthesis of Cyclic Guanidines Christelle Marmillon, Jacques Bompart, Michèle Calas, Roger Escale,* and Pierre-Antoine Bonnet Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . (3aR*,6aR*)-6-hydroxy-6-(1-hydroxy-1-methyl-ethyl)-3,3a,6,6a-tetrahydro-2H-cyclopenta-furan-2-one C10H14O4 相似度:50% Russian Journal of Organic Chemistry 2011 47 185-191 Syntheses and oxidative transformations of 6-(1-methylethylidene)-3,3a,6,6a-tetrahydro-2H-cyclopentafuran-2-one and its precursors Z. R. Valiullina, N. P. Akhmetdinova, N. A. Ivanova, O. V. Shitikova and M. S. Miftakhov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . compound 18 相似度:50% The Journal of Antibiotics 1994 47 216-224 FUNGAL METABOLITES. Part 12. POTENT IMMUNOSUPPRESSANT, 14-DEOXOMYRIOGIN, (2S, 3R, 4R-(E)2-AMINO-3, 4-DIHYDROXY-2-HYDROXYMETHYLEICOS-6-ENOIC ACID AND STRUCTURE-ACTIVITY RELATIONSHIPS OF MYRIOCIN DERIVATIVES TETSURO FUJITA, KENICHIRO INOUE, SATOSHI YAMAMOTO, TAKESHI IKUMOTO, SHIGEO SASAKI, RYOUSUKE TOYAMA, KENJI CHIBA, YUKIO HOSHINO, TAKEKI OKUMOTO Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . calystegine B4 C7H13NO4 相似度:50% European Journal of Organic Chemistry 2010 3337-3344 Total Synthesis of Calystegine B4 Panawan Moosophon, Morwenna C. Baird, Somdej Kanokmedhakul and Stephen G. Pyne Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 7-hydroxycineole(3,3-dimethyl-2-oxabicyclo[2.2.2]octane-1-methanol) C10H18O2 相似度:50% Australian Journal of Chemistry 1993 46 441-447 7-Hydroxy- l,8-cineole and 7-Cineolic Acid. Two New Possum Urinary Metabolites SD Bull, RM Carman, FN Carrick and KD Klika Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . (iodomethyl)(2-acetoxypropyl)dimethylammonium iodide C8H17I2NO2 相似度:50% Journal of Medicinal Chemistry 1991 34 2031-2036 Neurochemistry of aging. 2. Design, synthesis and biological evaluation of halomethyl analogs of choline with high affinity choline transport inhibitory activity Jehangir S. Mistry, Donald J. Abraham, Alan P. Kozikowski, Israel Hanin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . Aspinolide A C10H16O3 相似度:50% Helvetica Chimica Acta 2011 94 224-229 An Iterative Acetylene–Epoxide Coupling Strategy for the Total Synthesis of Aspinolide A Gowravaram Sabitha, Teega Rammohan Reddy, Chitti Srinivas and Jhillu Singh Yadav Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . endo-2-Hydroxybicyclo[3.2.1]octane 相似度:50% Organic Magnetic Resonance 1976 8 74-78 Carbon-13 chemical shifts of bicyclo[3.2.1]octane and bicyclo[2.2.1]heptane derivatives E. Lippmaa, T. Pehk, N. A. Belikova, A. A. Bobyleva, A. N. Kalinichenko, M. D. Ordubadi and A. F. Platé Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . aspinolide A C10H16O3 相似度:50% European Journal of Organic Chemistry 1997 1997 87-95 Secondary Metabolites by Chemical Screening, 34. – Aspinolides and Aspinonene/Aspyrone Co-Metabolites, New Pentaketides Produced by Aspergillus ochraceus Jens Fuchser and Axel Zeeck Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . 1,3,4,6-tetra-O-acetyl-2-deoxy-2-acetamido-β-D-mannose 相似度:50% Journal of Medicinal Chemistry 1981 24 848-852 Haloacetamido analogs of 2-amino-2-deoxy-D-mannose. Syntheses and effects on tumor-bearing mice Thomas P. Fondy, Cheryl A. Emlich Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . [{k1-SntBu2OSntBu2(h5-C5H4)}Ru(CO)2] C23H40O3RuSn2 相似度:50% Zeitschrift für Naturforschung B 2012 67 1173-1177 Insertion of Chalcogens and Bis(tert-butylisonitrile)palladium(0) into a Strained Ruthenium Half-sandwich Complex Holger Braunschweig, Alexander Damme, Jan Mies, and Marius Schäfer |
2楼2013-01-17 14:47:40