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求助几种氧化物的标准谱图！
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各位大虾请帮忙，我想查询几个氧化物的标准谱图，TiO2、SiO2以及ZrO2的各相的标准谱图，请问在哪能查到并下载？？？？？？？ 谢谢各位，知道的一定要帮忙啊！！！急用呢！！！！！！！！ |
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daiqiguang
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2楼2007-07-13 08:15:51
3楼2007-07-13 08:16:48
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PDF#48-1278: QM=Intermediate; d=Diffractometer; I=Film/Visual Titanium Oxide Ti O2 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= d-Cutoff= I/Ic(RIR)= Ref= Sato, H., Endo, S., Sugiyama, M., Kikegawa, T., Shimomura, O., Kusaba, K. Science, 251 786 (1991) Monoclinic - Powder Diffraction, P21/c (14) Z=4 mp= Cell=4.64x4.76x4.81<99.2> Pearson=mP12 (O2 Zr) Density(c)=5.061 Density(m)=5.01A Mwt=79.90 Vol=104.87 F(15)=1.9(0.210,38) Ref= Ibid. Strong Line: 2.86/X 2.59/8 1.99/5 2.36/3 2.28/2 1.66/1 1.53/1 1.83/1 1.69/1 3.32/1 NOTE: Preparation: Ti O2 powder, obtained from 99.99% purity rutile single crystal, was heated at 770 C for 30 minutes at a pressure of 20.3 GPa. Pattern taken at 20.3 GPa and room temperature. Intensities read by Editor. Data obtained by energy dispersive diffraction. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.3700 4.0 3.0 0 1 1 26.426 13.213 0.1484 1.8644 3.3200 6.0 5.0 1 1 0 26.831 13.416 0.1506 1.8925 2.8580 100.0 100.0 1 1 -1 31.271 15.636 0.1749 2.1985 2.5880 75.0 83.0 1 1 1 34.631 17.316 0.1932 2.4278 2.3570 27.0 33.0 0 2 0 38.150 19.075 0.2121 2.6658 2.3570 27.0 33.0 0 0 2 38.150 19.075 0.2121 2.6658 2.2810 24.0 30.0 2 0 0 39.473 19.736 0.2192 2.7546 1.9870 51.0 73.0 1 0 2 45.618 22.809 0.2516 3.1621 1.9870 51.0 73.0 1 2 -1 45.618 22.809 0.2516 3.1621 1.8340 8.0 12.0 1 1 2 49.669 24.835 0.2726 3.4259 1.8030 2.0 3.0 2 0 -2 50.583 25.291 0.2773 3.4849 1.6910 8.0 14.0 0 2 2 54.196 27.098 0.2957 3.7157 1.6600 14.0 24.0 2 2 0 55.294 27.647 0.3012 3.7851 1.6290 2.0 4.0 2 2 -1 56.439 28.220 0.3069 3.8571 1.5320 10.0 19.0 3 0 0 60.370 30.185 0.3264 4.1013 1.4940 2.0 4.0 1 1 -3 62.073 31.036 0.3347 4.2056 1.4940 2.0 4.0 1 3 0 62.073 31.036 0.3347 4.2056 1.4400 4.0 8.0 2 2 -2 64.677 32.338 0.3472 4.3633 |
4楼2007-07-13 19:56:13
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PDF#46-1238: QM=(Unknown); d=Calculated; I=Calculated Titanium Oxide Ti O2 (White) Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= d-Cutoff=17.7 I/Ic(RIR)=1.68 Ref= Kaduk, J., Chen, Y.-M., Amoco Corporation, Naperville, IL, USA. Private Communication (1995) Monoclinic - Profile Analysis, C2/m (12) Z=8 mp= Cell=12.2077x3.7488x6.535<107.36> Pearson=mC24 ($GB O2) Density(c)=3.718 Density(m)=3.720 Mwt=79.90 Vol=285.45 F(30)=999.9(.0008,34) Ref= Marchand, R., Brohan, L., Tournoux, M. Mater. Res. Bull., 15 1129 (1980) Strong Line: 3.57/X 6.24/6 5.83/6 3.12/4 3.01/3 1.87/3 2.69/3 2.03/2 2.98/2 2.70/2 NOTE: Rietveld method. Synthetic analog of the unnamed mineral Ti O2, 35-88. Coordinates reported by Banfield yield unreasonable distances and angles. Structure derived from that of Al Nb O4. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 6.2373 60.2 34.4 0 0 1 14.188 7.094 0.0802 1.0074 5.8258 56.2 34.4 2 0 0 15.196 7.598 0.0858 1.0785 5.0803 9.8 6.9 -2 0 1 17.442 8.721 0.0984 1.2368 3.7374 15.5 14.8 2 0 1 23.788 11.894 0.1338 1.6812 3.5686 100.0 100.0 1 1 0 24.930 12.465 0.1401 1.7607 3.2272 1.0 1.1 -1 1 1 27.617 13.809 0.1549 1.9469 3.1712 4.9 5.5 -2 0 2 28.115 14.057 0.1577 1.9813 3.1187 40.9 46.8 0 0 2 28.599 14.300 0.1603 2.0147 3.0054 30.3 36.0 -4 0 1 29.701 14.851 0.1664 2.0907 2.9822 21.7 26.0 1 1 1 29.937 14.969 0.1677 2.1069 2.9129 6.7 8.2 4 0 0 30.667 15.333 0.1716 2.1570 2.6973 21.3 28.2 3 1 0 33.187 16.593 0.1854 2.3294 2.6869 25.3 33.6 -3 1 1 33.319 16.660 0.1861 2.3385 2.5401 5.0 7.0 -4 0 2 35.305 17.652 0.1968 2.4735 2.4625 4.5 6.5 2 0 2 36.457 18.229 0.2030 2.5516 2.4625 4.5 6.5 -1 1 2 36.457 18.229 0.2030 2.5516 2.3809 2.7 4.0 4 0 1 37.752 18.876 0.2100 2.6390 2.3076 11.8 18.2 3 1 1 38.999 19.499 0.2167 2.7228 2.2882 5.8 9.0 -3 1 2 39.344 19.672 0.2185 2.7460 2.2487 2.7 4.3 1 1 2 40.064 20.032 0.2224 2.7942 2.1742 0.2 0.3 -2 0 3 41.498 20.749 0.2300 2.8898 2.0791 19.1 32.8 0 0 3 43.491 21.746 0.2405 3.0221 2.0344 22.3 39.1 -6 0 1 44.497 22.248 0.2458 3.0884 1.9974 1.6 2.9 -4 0 3 45.368 22.684 0.2503 3.1457 1.9791 0.4 0.7 5 1 0 45.810 22.905 0.2526 3.1748 1.9419 2.2 4.0 6 0 0 46.738 23.369 0.2575 3.2355 1.9265 1.2 2.2 -6 0 2 47.137 23.568 0.2595 3.2615 1.9034 0.6 1.1 -5 1 2 47.742 23.871 0.2627 3.3010 1.8744 26.2 49.9 0 2 0 48.529 24.264 0.2668 3.3521 1.8687 17.5 33.4 4 0 2 48.686 24.343 0.2676 3.3623 1.8415 0.5 1.0 -3 1 3 49.453 24.727 0.2715 3.4120 1.7959 4.8 9.5 0 2 1 50.798 25.399 0.2784 3.4987 1.7959 4.8 9.5 2 0 3 50.798 25.399 0.2784 3.4987 1.7843 2.5 5.0 2 2 0 51.150 25.575 0.2802 3.5213 1.7585 0.6 1.2 -2 2 1 51.956 25.978 0.2843 3.5730 1.7290 11.7 24.1 1 1 3 52.910 26.455 0.2892 3.6339 1.7146 2.7 5.6 6 0 1 53.390 26.695 0.2916 3.6645 1.6934 5.7 12.0 -6 0 3 54.112 27.056 0.2953 3.7103 1.6755 1.6 3.4 2 2 1 54.740 27.370 0.2984 3.7501 1.6587 1.0 2.2 -5 1 3 55.342 27.671 0.3014 3.7881 1.6329 0.6 1.3 -2 0 4 56.293 28.146 0.3062 3.8479 1.6136 1.3 2.9 -2 2 2 57.027 28.513 0.3099 3.8939 1.6066 7.2 16.0 0 2 2 57.300 28.650 0.3112 3.9110 1.5904 6.2 13.9 -4 2 1 57.936 28.968 0.3144 3.9506 1.5856 10.1 22.7 -4 0 4 58.129 29.064 0.3153 3.9626 1.5805 16.5 37.3 -7 1 1 58.334 29.167 0.3164 3.9754 1.5763 9.6 21.7 4 2 0 58.507 29.254 0.3172 3.9861 1.5593 0.8 1.8 0 0 4 59.205 29.603 0.3207 4.0294 1.5431 0.4 0.9 -7 1 2 59.890 29.945 0.3240 4.0717 1.5213 4.9 11.5 7 1 0 60.839 30.420 0.3287 4.1301 1.5082 2.5 5.9 -4 2 2 61.423 30.712 0.3315 4.1659 1.5030 10.8 25.6 3 1 3 61.662 30.831 0.3327 4.1805 1.4945 3.4 8.1 4 0 3 62.050 31.025 0.3346 4.2042 1.4904 8.9 21.3 -3 1 4 62.239 31.119 0.3355 4.2157 1.4793 0.8 1.9 -1 1 4 62.757 31.379 0.3380 4.2473 1.4728 1.5 3.6 4 2 1 63.069 31.535 0.3395 4.2662 1.4641 1.8 4.4 6 0 2 63.488 31.744 0.3415 4.2916 1.4564 1.1 2.7 8 0 0 63.859 31.929 0.3433 4.3140 1.4443 2.8 6.9 -6 0 4 64.460 32.230 0.3462 4.3503 1.4271 3.6 9.0 -7 1 3 65.332 32.666 0.3504 4.4027 1.4197 2.1 5.3 -2 2 3 65.718 32.859 0.3522 4.4258 1.4109 0.1 0.3 -5 1 4 66.179 33.089 0.3544 4.4533 1.3922 6.4 16.4 0 2 3 67.187 33.594 0.3592 4.5133 1.3785 6.9 17.9 -6 2 1 67.943 33.971 0.3627 4.5580 1.3668 0.6 1.6 -4 2 3 68.605 34.302 0.3658 4.5970 1.3486 0.8 2.1 6 2 0 69.661 34.830 0.3707 4.6589 1.3434 0.5 1.3 -6 2 2 69.971 34.986 0.3722 4.6770 1.3330 0.1 0.3 8 0 1 70.602 35.301 0.3751 4.7137 1.3234 0.1 0.3 4 2 2 71.190 35.595 0.3778 4.7478 1.2967 1.0 2.8 2 2 3 72.885 36.442 0.3856 4.8454 1.2806 0.2 0.6 5 1 3 73.957 36.978 0.3905 4.9066 1.2768 1.1 3.1 -7 1 4 74.214 37.107 0.3916 4.9212 1.2704 0.5 1.4 -9 1 1 74.648 37.324 0.3936 4.9458 1.2671 0.9 2.5 -9 1 2 74.875 37.437 0.3946 4.9586 1.2651 1.4 3.9 6 2 1 75.013 37.506 0.3952 4.9664 1.2566 2.7 7.7 -6 2 3 75.614 37.807 0.3979 5.0003 1.2475 1.1 3.1 0 0 5 76.264 38.132 0.4008 5.0368 1.2425 3.1 8.9 1 3 0 76.625 38.313 0.4024 5.0570 1.2425 3.1 8.9 3 1 4 76.625 38.313 0.4024 5.0570 1.2405 5.6 16.1 7 1 2 76.772 38.386 0.4031 5.0651 1.2338 0.8 2.3 -3 1 5 77.262 38.631 0.4052 5.0924 1.2312 0.9 2.6 -6 0 5 77.455 38.728 0.4061 5.1032 1.2312 0.9 2.6 -2 2 4 77.455 38.728 0.4061 5.1032 1.2260 0.5 1.5 -1 3 1 77.845 38.923 0.4078 5.1248 1.2237 1.5 4.4 9 1 0 78.021 39.011 0.4086 5.1345 1.2170 1.0 2.9 -10 0 2 78.534 39.267 0.4108 5.1628 1.2150 1.0 2.9 -9 1 3 78.690 39.345 0.4115 5.1714 1.2106 3.7 10.9 -4 2 4 79.032 39.516 0.4130 5.1903 1.2016 0.2 0.6 -5 1 5 79.742 39.871 0.4161 5.2291 1.1988 0.4 1.2 0 2 4 79.967 39.984 0.4171 5.2414 1.1887 1.1 3.3 3 3 0 80.786 40.393 0.4206 5.2860 1.1887 1.1 3.3 -3 3 1 80.786 40.393 0.4206 5.2860 1.1818 0.1 0.3 -8 2 1 81.357 40.678 0.4231 5.3168 1.1772 0.4 1.2 -10 0 3 81.737 40.869 0.4247 5.3374 1.1724 0.1 0.3 -8 2 2 82.142 41.071 0.4265 5.3591 1.1685 1.3 4.0 4 2 3 82.476 41.238 0.4279 5.3770 1.1652 1.2 3.7 10 0 0 82.767 41.383 0.4291 5.3926 1.1538 1.2 3.7 6 2 2 83.763 41.881 0.4333 5.4456 1.1515 1.0 3.1 2 0 5 83.970 41.985 0.4342 5.4565 1.1493 1.3 4.0 3 3 1 84.166 42.083 0.4350 5.4669 1.1469 1.5 4.7 -3 3 2 84.385 42.193 0.4360 5.4785 1.1441 2.4 7.5 -6 2 4 84.642 42.321 0.4370 5.4920 1.1441 2.4 7.5 1 1 5 84.642 42.321 0.4370 5.4920 1.1418 1.2 3.8 1 3 2 84.847 42.424 0.4379 5.5028 1.1298 0.2 0.6 -9 1 4 85.969 42.985 0.4426 5.5615 1.1270 0.7 2.2 -7 1 5 86.230 43.115 0.4436 5.5750 1.1243 0.4 1.3 2 2 4 86.486 43.243 0.4447 5.5883 1.1047 0.2 0.6 -10 0 4 88.417 44.208 0.4526 5.6876 1.1013 0.1 0.3 5 3 0 88.766 44.383 0.4540 5.7055 1.0871 0.6 2.0 -4 0 6 90.233 45.117 0.4599 5.7796 1.0818 0.2 0.7 -1 3 3 90.800 45.400 0.4622 5.8080 1.0791 0.1 0.3 3 3 2 91.094 45.547 0.4634 5.8227 1.0700 0.3 1.0 6 0 4 92.095 46.047 0.4673 5.8724 1.0632 0.6 2.0 -11 1 2 92.850 46.425 0.4703 5.9095 1.0592 0.4 1.3 5 3 1 93.308 46.654 0.4720 5.9320 1.0571 0.6 2.0 -6 0 6 93.553 46.776 0.4730 5.9439 1.0542 0.4 1.4 8 0 3 93.886 46.943 0.4743 5.9601 1.0519 1.5 5.1 1 3 3 94.154 47.077 0.4753 5.9731 1.0454 0.8 2.7 -3 1 6 94.921 47.461 0.4783 6.0102 1.0435 1.1 3.8 9 1 2 95.155 47.578 0.4792 6.0214 1.0399 0.6 2.1 4 0 5 95.583 47.791 0.4808 6.0419 1.0399 0.6 2.1 -11 1 3 95.583 47.791 0.4808 6.0419 1.0385 1.0 3.4 0 2 5 95.757 47.878 0.4815 6.0503 1.0345 0.5 1.7 -5 1 6 96.242 48.121 0.4833 6.0734 1.0309 0.5 1.7 -9 1 5 96.692 48.346 0.4850 6.0947 1.0286 0.6 2.1 -6 2 5 96.981 48.491 0.4861 6.1084 1.0286 0.6 2.1 4 2 4 96.981 48.491 0.4861 6.1084 1.0207 0.9 3.1 -10 2 2 97.989 48.994 0.4899 6.1556 1.0193 0.4 1.4 11 1 0 98.168 49.084 0.4905 6.1640 1.0181 0.7 2.5 -10 2 1 98.332 49.166 0.4911 6.1717 1.0156 2.2 7.7 -7 3 1 98.659 49.330 0.4923 6.1869 1.0156 2.2 7.7 -10 0 5 98.659 49.330 0.4923 6.1869 1.0061 0.1 0.4 -12 0 1 99.920 49.960 0.4970 6.2450 1.0049 0.2 0.7 8 2 2 100.083 50.041 0.4976 6.2524 1.0018 0.1 0.4 -12 0 3 100.511 50.256 0.4991 6.2720 0.9993 0.8 2.9 7 3 0 100.851 50.425 0.5003 6.2874 0.9982 0.6 2.1 10 0 2 101.010 50.505 0.5009 6.2946 0.9969 0.9 3.2 -10 2 3 101.189 50.594 0.5016 6.3027 0.9953 0.5 1.8 5 3 2 101.415 50.708 0.5024 6.3129 0.9941 2.1 7.5 3 3 3 101.586 50.793 0.5030 6.3206 0.9904 1.6 5.8 -3 3 4 102.106 51.053 0.5048 6.3439 0.9904 1.6 5.8 10 2 0 102.106 51.053 0.5048 6.3439 0.9872 0.7 2.5 -1 3 4 102.577 51.288 0.5065 6.3650 0.9811 0.2 0.7 2 2 5 103.457 51.728 0.5096 6.4039 0.9744 0.3 1.1 1 1 6 104.461 52.231 0.5131 6.4480 0.9712 0.9 3.3 -7 3 3 104.960 52.480 0.5148 6.4697 0.9653 0.8 3.0 7 1 4 105.879 52.939 0.5180 6.5093 0.9632 0.6 2.2 11 1 1 106.201 53.101 0.5191 6.5231 0.9632 0.6 2.2 -12 0 4 106.201 53.101 0.5191 6.5231 0.9602 0.3 1.1 7 3 1 106.676 53.338 0.5207 6.5433 0.9570 0.1 0.4 1 3 4 107.200 53.600 0.5225 6.5655 0.9517 0.3 1.1 -10 2 4 108.066 54.033 0.5254 6.6019 0.9446 0.4 1.5 9 1 3 109.272 54.636 0.5293 6.6520 0.9404 0.7 2.7 -4 2 6 109.989 54.994 0.5317 6.6814 0.9372 1.0 3.8 0 4 0 110.550 55.275 0.5335 6.7042 0.9344 0.5 1.9 8 0 4 111.054 55.527 0.5351 6.7246 0.9335 0.4 1.5 -4 0 7 111.200 55.600 0.5356 6.7305 0.9311 0.5 1.9 -11 1 5 111.637 55.818 0.5370 6.7480 0.9292 0.5 1.9 6 2 4 111.982 55.991 0.5381 6.7618 0.9268 0.4 1.5 0 4 1 112.428 56.214 0.5395 6.7795 0.9253 0.2 0.8 2 4 0 112.705 56.352 0.5404 6.7904 0.9229 0.2 0.8 -2 0 7 113.151 56.575 0.5418 6.8079 0.9208 0.8 3.1 -6 2 6 113.561 56.780 0.5430 6.8240 0.9195 0.4 1.6 -7 3 4 113.794 56.897 0.5438 6.8331 0.9187 0.5 1.9 12 0 1 113.961 56.980 0.5443 6.8395 0.9171 0.3 1.2 -9 3 1 114.253 57.126 0.5452 6.8508 0.9159 0.2 0.8 -9 3 2 114.493 57.246 0.5459 6.8601 0.9109 1.2 4.7 -13 1 2 115.487 57.744 0.5489 6.8981 0.9089 2.1 8.2 3 1 6 115.886 57.943 0.5501 6.9132 0.9075 0.8 3.1 10 0 3 116.163 58.081 0.5510 6.9237 0.9067 1.5 5.9 3 3 4 116.333 58.166 0.5515 6.9301 0.9057 1.6 6.3 7 3 2 116.531 58.265 0.5521 6.9375 0.9037 1.9 7.5 -3 1 7 116.942 58.471 0.5533 6.9528 0.8999 1.0 4.0 -13 1 1 117.741 58.870 0.5556 6.9824 0.8991 0.8 3.2 9 3 0 117.902 58.951 0.5561 6.9883 0.8975 1.4 5.6 4 0 6 118.231 59.116 0.5571 7.0004 0.8975 1.4 5.6 0 4 2 118.231 59.116 0.5571 7.0004 0.8956 0.9 3.6 -9 3 3 118.646 59.323 0.5583 7.0155 0.8956 0.9 3.6 11 1 2 118.646 59.323 0.5583 7.0155 0.8947 0.9 3.6 -4 4 1 118.843 59.421 0.5588 7.0226 0.8933 1.5 6.0 -10 2 5 119.157 59.578 0.5597 7.0340 0.8910 1.0 4.0 0 0 7 119.644 59.822 0.5611 7.0515 0.8865 0.1 0.4 -12 2 1 120.665 60.332 0.5640 7.0877 0.8837 0.3 1.2 -1 1 7 121.304 60.652 0.5658 7.1101 0.8810 0.7 2.8 10 2 2 121.920 60.960 0.5675 7.1315 0.8793 0.5 2.0 -4 4 2 122.339 61.170 0.5687 7.1460 0.8770 1.2 4.9 -13 1 4 122.888 61.444 0.5701 7.1647 0.8721 0.5 2.0 4 4 1 124.080 62.040 0.5733 7.2049 0.8721 0.5 2.0 -14 0 2 124.080 62.040 0.5733 7.2049 0.8666 0.3 1.2 1 3 5 125.448 62.724 0.5769 7.2500 0.8645 0.2 0.8 2 2 6 125.996 62.998 0.5784 7.2678 0.8622 0.2 0.8 -11 1 6 126.615 63.308 0.5799 7.2877 0.8622 0.2 0.8 12 2 0 126.615 63.308 0.5799 7.2877 0.8592 0.3 1.2 -14 0 1 127.394 63.697 0.5819 7.3125 |
5楼2007-07-13 19:57:34
6楼2007-07-13 22:04:27
7楼2007-07-13 22:37:14