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yymslx2010

金虫 (著名写手)


[求助] 求助微谱数据

化合物1:溶剂:氯仿
C:178,175,170,153,151,121,109,63,62,56,53,14.
化合物2:溶剂:氯仿
C:200,168,137,136,74,65,40,24,15.

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【答案】应助回帖

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感谢参与,应助指数 +1
yymslx2010: 金币+10, 有帮助, 谢谢帮助! 2012-11-24 17:11:45
第一个1 .     dimethyl 3,3',4,4',5,5'-hexamethoxybiphenyl-2,2'-dicarboxylate
    相似度:58.3%
Australian Journal of Chemistry          1981          34          799-817
Constituents of Eupomatia species. VII. Dienone-phenol and dienol-benzene rearrangements in the eupodienone-1 series
BF Bowden, RW Read and WC Taylor
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

2 .     (E)-4-methyl-1-(5-methylfuran-2-yl)pent-2-en-1-one
C10H14O2     相似度:50%
Archives of Pharmacal Research          2011          Vol 34, No 8          1277-1282
Biological Evaluation of Isoegomaketone Isolated from Perilla frutescens and its Synthetic Derivatives as Anti-inflammatory Agents
Yong Dae Park, Chang Hyun Jin, Dae Seong Choi, Myung-Woo Byun, and Il Yun Jeong
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

3 .     Ethyl (2R*,3S*)-and (2R*,3R*)-3-(Furan-2-yl)-3-hydroxy-2-(methylsulfanyl)propanoate
C10H14NaO4S     相似度:50%
Helvetica Chimica Acta          2011          Vol. 94          1533-1542
Synthesis of b-Hydroxy a-Sulfanyl Esters by Using Nanocrystalline Magnesium Oxide
Koosam Mahendar, A. V. S. Sarma, P. Raghavaiah, Mannepalli Lakshmi Kantam, and Kenneth J. Klabunde
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

4 .     comopund 2f
C12H15NO4     相似度:50%
Journal of Heterocyclic Chemistry          2001          38          221-225
Attempted synthesis of ethyl 3,4-dihydro-2H-1,4-benzoxazine-3-carboxylate and 3-acetate derivatives
Stanislas Mayer, Axelle Arrault, GéRald Guillaumet and Jean-Yves Mérour
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

5 .     (S)-6,6'-dihydroxymethyl-2,2',3,3',4,4'-hexamethoxy-1,1'-biphenyl
C20H26O8     相似度:50%
Heterocycles          2008          76          291-303
Synthesis of Highly Oxygenated Biphenyl Derivative in an Optically Active Form through Palladium-Mediated Intramolecular Biaryl Coupling Reaction
Hitoshi Abe, Masatsugu Arai, Keisuke Nishioka, Tatsuya Kida, Kazuma Shioe, Yasuo Takeuchi, and Takashi Harayama
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

6 .     2-diethylamino-5,8-dimethoxy-4H-1,3-benzoselenazine
C14H20N2O2Se     相似度:50%
Heterocycles          2004          63          1067-1075
KF-Alumina Immobilized in Ionic Liquids: A Novel Heterogeneous Base for Heterocyclization of Alkylsulfanylphenylamines into 1,4-Benzothiazine
Bhupender S. Chhikara, Anil K. Mishra, and Vibha Tandon*
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

7 .     methyl 6-amino-N-ethoxycarbonyl-3-hydroxybenzoate
    相似度:50%
Heterocycles          2003          60          2023-2044
Approach to the Synthesis of (+)-Ifforestine. Model Studies Directed at the Tetracyclic Framework
Gregory H. P. Roos* and Kim A. Dastlik
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

8 .     ethyl 2-formyl-4-furoate
C8H8O4     相似度:50%
Tetrahedron          1996          52          4245-4256
Two practical syntheses of an anti-inflammatory sesquiterpene furoic acid from Sinularia spp
David H. Williams, D. John Faulkner
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

9 .     ethyl (3RS,3aRS,9bSR)-1-tert-butyl-2-oxo-1,2,3,3a,4,9b-hexahydrochromeno[4,3-b]pyrrole-3-carboxylate
C18H23NO4     相似度:50%
Russian Journal of Organic Chemistry          2005          41          361-369
Intramolecular 1,3-Dipolar Cycloaddition of Geminal Difluoro Azomethine Ylides at Multiple Carbon-Carbon Bonds
M. S. Novikov, A. F. Khlebnikov, I. V. Voznyi, O. V. Besedina and R. R. Kostikov
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

10 .     1-(3-tert-butyl-2,2-dimethyl-2H-thiet-4-yl)-5,5-dimethyl-3-phenyl-imidazolidine-2,4-dione
C20H26N2O2S     相似度:50%
Heterocycles          2012          84          945-961
Reactivity of N-Alkylthiiranimines toward Simple Nucleophiles and Iso(thio)cyanates
Hildegard Nimmesgern, Ernst Schaumann,* and Gunadi Adiwidjaja
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

11 .     methyl rel-(1R,4S)-4-[(phenoxycarbonyl)amino]cyclopent-2-ene-1-carboxylate
C14H15NO4     相似度:50%
European Journal of Organic Chemistry          2010                   3281-3294
Metal-Catalyzed Reactions between 2-Azabicyclo[2.2.1]hept-5-en-3-ones and Arylboronic Acids
Takumi Abe, Hiroyuki Takeda, Yumi Takahashi, Yoshihisa Miwa, Koji Yamada and Minoru Ishikura
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

12 .     Methyl 2-bromo-3,4,5-trimethoxybenzoate
C11H13BrO5     相似度:50%
Tetrahedron          2012          68          5744-5753
Aryl-β-C-glucosidation using glucal boronate: application to the synthesis of tri-O-methylnorbergenin
Shigeki Sakamaki, Eiji Kawanishi, Sumihiro Nomura, Tsutomu Ishikawa
Structure      13C NMR   碳谱模拟图  
第二个1 .     (±)-1-(4-Hydroxyphenyl)hexanol
C12H18O2     相似度:55.5%
Archiv der Pharmazie          2002          335          94-98
Synthesis and Antimicrobial Activity of Hydroxyalkyl-and Hydroxyacyl-phenols and Their Benzyl Ethers
Jürgen Krauß and D. Unterreitmeier
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

2 .     3-(Allyloxy)-2-hydroxypropyl bis(dimethylamino)methylenecarbamodithioate
C12H23N3O2S2     相似度:55.5%
Chinese Chemical Letters          2012          23          699-702
Synthesis of alkyl bis(dimethylamino)methylenecarbamodithioates from 1,1,3,3-tetramethylguanidine, CS2 and oxiranes
Sima Yavari, Samira Nasiri-Gheidari, Avat (Arman) Taherpour, Issa Yavari
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

3 .     (+)-(3S,4S,6R)-6-hydroxypiperitol
    相似度:50%
Planta Medica          1993          59          482
Additional Terpenoids from Chrysactinta mexicana
Guillermo Delgado, Maria Yolanda Rios, and Carlos Rodriguez
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

4 .     compound 1h
    相似度:50%
Molecules          1999          4          279-286
Synthetical Application of Alkyl 2-isothiocyanatocarboxylates. A Simple Synthesis of 5-Substituted-3-amino-2-thioxo-4-imidazolidinones (3-Amino-2-thiohydantoins)
Lubomir Floch1, Vladimir Oremus2 and Martin Kovac
Structure      13C NMR   碳谱模拟图
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