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[求助] XPS校正方法英文书写（参考文献）

审稿人提问说，能量校正的方法应该给出
The method of binding energy calibration in XPS spectra should be detailed.

问了测试老师是这样说的：用Ni样品做费米能级校正，分别用Cu、Ag、Au三种元素做能量校准，用污染碳C 284.6eV作核电位移校正。
求英文翻译，或者参考文献

能提供参考文献就可以了，只要文献有写这些条件就OK了，实在是不会翻译

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1楼 2012-11-20 12:19:51

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zuozhijun5134

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XPS analyseswere performed with a V.G. Scientific ESCALAB250
using focused (diameter of the irradiated area was approximately
500m) monochromated Al K (h = 1486.6 eV, 150W). An electron
shower was used in order to compensate for charging effects.
Ahemispherical electrostatic analyzer and a LargeAreaXL Lenswere
used tomaximize the signal. The residual pressure inside the analysis
chamber was 6×10−10 mbar. The spectrometer was calibrated
using the photoemission lines of Au (Au 4f7/2 = 83.95 eV), Ag (Ag
3d5/2 = 368.22 eV) and Cu (Cu 2p3/2 = 932.62 eV). The peaks were
recorded at a constant pass energy of 20 eV and XPS datawere taken
at normal emission ( =0◦

for all catalysts. No smoothing routine
of data was applied to the data during the analysis. Atomic ratios
were then computed from the intensity ratios normalized by the
atomic sensitivity factors of Scofield [6]. A Shirley-type background
subtraction was done prior to curve fitting, and fitting the experimental
curve to 80% Gaussian–20% Lorentzian function. In addition,
aminimum number of doubletswere always used in order to fit the
experimental curves.

W. Huang et al. / Journal of Electron Spectroscopy and Related Phenomena 173 (2009) 88–95