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求79814-40-7beilstein或CA检索一个
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检索目的:全合成 标题:R)-(+)-2-Acetoxysuccinic anhydride Synonym： (R)-3-Acetoxy-dihydro-2,5-furandione O-Acetyl-D-malic anhydride 登录号CAS Number:79814-40-7 Beilstein Registry Number :130824 [ Last edited by Merck2006 on 2007-7-5 at 10:05 ] |
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Beilstein Data: Copyright (c) 1988-2006, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved. Reaction (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction ID 3316068 Reactant BRN 1723541 (S)-hydroxysuccinic acid 605303 acetyl chloride Product BRN 82504 (S)-acetoxy-succinic acid-anhydride No. of Reaction Details 7 Find similar reactions click here Field Availability List (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Code Field Name Occ. RX Reaction Details 7 Reaction Details 1 of 7 (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction Classification Preparation Yield 99 percent (BRN=82504) Time 3 hour(s) Other Conditions Heating Ref. 1 6407216; Journal; Ensch, Corinne; Hesse, Manfred; HCACAV; Helv. Chim. Acta; EN; 86; 1; 2003; 233 - 246. Reaction Details 2 of 7 (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction Classification Preparation Time 5 hour(s) Other Conditions Heating Reaction Type Acetylation cyclization Ref. 1 6202664; Journal; Jin, Liren; Wu, Hong; Wu, Huailing; Huang, Peiqiang; Jung, Kyeongeun; Lim, Hong; CMLTAG; Chem. Lett.; EN; 7; 1999; 687 - 688. Reaction Details 3 of 7 (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction Classification Preparation Reagent acetic anhydride Reaction Type Acetylation dehydratation Ref. 1 6175361; Journal; Delagrange, Samuel; Nepveu, Francoise; TELEAY; Tetrahedron Lett.; EN; 40; 27; 1999; 4989 - 4992. Reaction Details 4 of 7 (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction Classification Preparation Yield 100 percent (BRN=82504) Time 2 hour(s) Other Conditions Heating Ref. 1 6017128; Journal; Louwrier, Saskia; Ostendorf, Martin; Boom, Arnoud; Hiemstra, Henk; Speckamp, W. Nico; TETRAB; Tetrahedron; EN; 52; 7; 1996; 2603-2628. Reaction Details 5 of 7 (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction Classification Preparation Time 3 hour(s) Other Conditions Heating Ref. 1 5785890; Journal; Meier, Heidi; Uebelhart, Peter; Eugster, Conrad Hans; HCACAV; Helv. Chim. Acta; GE; 69; 1986; 106-123. Reaction Details 6 of 7 (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction Classification Preparation Time 10 hour(s) Other Conditions Heating Ref. 1 5653519; Journal; Yoda, Hidemi; Kitayama, Hidekazu; Katagiri, Takao; Takabe, Kunihiko; TETRAB; Tetrahedron; EN; 48; 16; 1992; 3313-3322. Reaction Details 7 of 7 (Beilstein(2006/04):Reactions:Q08 hit 6, RX.ID 3316068) Reaction Classification Preparation Time 1.5 hour(s) Other Conditions Heating Ref. 1 5642974; Journal; Klaver, Wim J.; Hiemstra, Henk; Speckamp, W. Nico; JACSAT; J. Am. Chem. Soc.; EN; 111; 7; 1989; 2588-2595. |
6楼2007-07-05 11:05:52
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至今无人合成 相关文献 1 Jung, Grace; Yee, James Gee Ken; Chou, Doug Ta Hung; Plouvier, Bertrand M. C. Synthetic processes for the preparation of aminocyclohexyl ether compounds. PCT Int. Appl. (2006), 104pp. CODEN: PIXXD2 WO 2006138673 A2 20061228 CAN 146:100552 AN 2006:1354283 CAPLUS 2 Plouvier, Betrand M. C.; Chou, Doug Ta Hung; Jung, Grace; Choi, Lewis Siu Leung; Sheng, Tao; Barrett, Anthony G. M.; Passafaro, Marco S.; Kurz, Martin; Moeckli, Daniel; Ulmann, Pirmin; Hedinger, Alfred. Synthetic process for stereoselective preparation of aminocyclohexyl ether compounds using resolution of racemic intermediates. PCT Int. Appl. (2006), 231pp. CODEN: PIXXD2 WO 2006088525 A1 20060824 CAN 145:271413 AN 2006:841658 CAPLUS 3 Gogoi, Sanjib; Argade, Narshinha P. A facile two-step chemoenzymatic access to natural germination inhibitor (+)-erigeronic acid A. Tetrahedron (2006), 62(13), 2999-3003. CODEN: TETRAB ISSN:0040-4020. CAN 144:432595 AN 2006:206999 CAPLUS 4 Wu, Hon-sun. Preparation of (optically active) b-substituted g-butyrolactones. Jpn. Kokai Tokkyo Koho (2004), 25 pp. CODEN: JKXXAF JP 2004161614 A 20040610 CAN 141:23414 AN 2004:472267 CAPLUS 5 Giordani, Antonio; Pevarello, Paolo; Speciale, Carmela; Varasi, Mario. Preparation of 4-phenyl-4-oxobutanoates as kynurenine-3-hydroxylase inhibitors. PCT Int. Appl. (1997), 63 pp. CODEN: PIXXD2 WO 9717317 A1 19970515 CAN 127:50402 AN 1997:433650 CAPLUS 6 Kurauchi, Masahiko; Hagiwara, Yoshimasa; Matsueda, Hiroyuki; Nakano, Takashi; Izawa, Kunisuke. Process for producing optically active 2-hydroxy-4-arylbutyric acid or its ester, and intermediate therefor. Eur. Pat. Appl. (1997), 10 pp. CODEN: EPXXDW EP 759424 A1 19970226 CAN 126:238130 AN 1997:257370 CAPLUS 7 Hart, David J.; Yang, Teng Kuei. N-Acyliminium ion rearrangements: generalities and application to the synthesis of pyrrolizidine alkaloids. Journal of Organic Chemistry (1985), 50(2), 235-42. CODEN: JOCEAH ISSN:0022-3263. CAN 102:62494 AN 1985:62494 CAPLUS 8 Hart, David J.; Yang, Teng Kuei. Enantioselective syntheses of (-)-hastanecine and its enantiomer using malic acid as a chiral educt. Journal of the Chemical Society, Chemical Communications (1983), (3), 135-6. CODEN: JCCCAT ISSN:0022-4936. CAN 99:54039 AN 1983:454039 CAPLUS 9 Kumar, S.; Gupta, R. C.; Gupta, C. M.; Anand, Nitya. A new synthetic approach to 8-aza analogs of prostaglandins. Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry (1981), 20B(7), 595-6. CODEN: IJSBDB ISSN:0376-4699. CAN 95:203380 AN 1981:603380 CAPLUS |
2楼2007-07-05 10:33:50
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Beilstein Data: Copyright (c) 1988-2006, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved. Reaction (Beilstein(2006/04):Reactions:Q08 hit 1, RX.ID 556438) Reaction ID 556438 Reactant BRN 1723541 (S)-hydroxysuccinic acid 385737 acetic acid anhydride Product BRN 82504 (S)-acetoxy-succinic acid-anhydride No. of Reaction Details 2 Find similar reactions not available Field Availability List (Beilstein(2006/04):Reactions:Q08 hit 1, RX.ID 556438) Code Field Name Occ. RX Reaction Details 2 Reaction Details 1 of 2 (Beilstein(2006/04):Reactions:Q08 hit 1, RX.ID 556438) Reaction Classification Preparation Yield 98 percent (BRN=82504) Time 2 hour(s) Temperature 30 C Ref. 1 6319336; Journal; Mhaske, Santosh B.; Argade, Narshinha P.; JOCEAH; J. Org. Chem.; EN; 66; 26; 2001; 9038 - 9040. Ref. 2 6547969; Journal; Mhaske, Santosh B.; Argade, Narshinha P.; JOCEAH; J. Org. Chem.; EN; SIR66; 26; 2001; 9038 - 9040. Reaction Details 2 of 2 (Beilstein(2006/04):Reactions:Q08 hit 1, RX.ID 556438) Reaction Classification Preparation Reagent sulfuric acid Ref. 1 529642; Journal; Jones; JCSOA9; J. Chem. Soc.; 1933; 788, 795. |
3楼2007-07-05 11:00:55
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Beilstein Data: Copyright (c) 1988-2006, Beilstein Institut zur Foerderung der Chemischen Wissenschaften licensed to Beilstein GmbH and MDL Information Systems GmbH. All rights reserved. Reaction (Beilstein(2006/04):Reactions:Q08 hit 4, RX.ID 3316064) Reaction ID 3316064 Reactant BRN 1723530 L-aspartic acid 605303 acetyl chloride Product BRN 82504 (S)-acetoxy-succinic acid-anhydride No. of Reaction Details 1 Find similar reactions click here Field Availability List (Beilstein(2006/04):Reactions:Q08 hit 4, RX.ID 3316064) Code Field Name Occ. RX Reaction Details 1 Reaction Details (Beilstein(2006/04):Reactions:Q08 hit 4, RX.ID 3316064) Reaction Classification Preparation Reagent 1.) sodium nitrite, aq. HCl Other Conditions 1.) water, 0 deg C, 14 h, 2.) 40 deg C, 2 h Note 1 Yield given. Multistep reaction Ref. 1 5773177; Journal; Henrot, Serge; Larcheveque, Marc; Petit, Yves; SYNCAV; Synth. Commun.; EN; 16; 2; 1986; 183-190. |
4楼2007-07-05 11:01:16
