2楼: Originally posted by David_Ji at 2012-11-15 10:34:29
This looks upside down. At high voltage, you should have oxidation peaks. r u sure this figure is the right one?

2楼: Originally posted by David_Ji at 2012-11-15 10:34:29
This looks upside down. At high voltage, you should have oxidation peaks. r u sure this figure is the right one?

5楼: Originally posted by 想飞的树 at 2012-11-15 12:52:06
1，你的电极电极电阻比较大。
2，还原峰0V左右有一个，和0.5V处氧化峰对应，物质在电极上可以氧化还原，峰电位差宽，应该为准可逆或不可逆。1.5V还有还原。
3，也觉得你的图看着怪别扭的。

7楼: Originally posted by 想飞的树 at 2012-11-15 14:15:22
如果你的溶液电解质符合要求的话，一般这种情况是电极本身电阻大。

9楼: Originally posted by willto123 at 2012-11-15 15:23:52
从图形看，你在系统设置时，电流选的是阴极正，以致电流数值反号。你将电流乘以-1，图形就会正常了。0.6V有一氧化峰，对应的还原峰为0.0V。0V不是氢还原峰，因为你的参比电极据我推断不会是标准氢电极。而是通常的饱 ...