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mcjudyzyp

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[交流] Fe3O4的XRD衍射峰归属

我使用FeSO4、氨水、葡萄糖制备四氧化三铁、但是在31度左右出现一较强的衍射峰，但是在JADE中为找到归属，请各位帮帮忙啊，鄙人现在急求啊！

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1楼2012-11-13 20:46:41

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

fjwzjg

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mcjudyzyp(金币+1): 谢谢参与

来个原文件

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3楼2012-11-14 09:40:46

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

mcjudyzyp

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3楼: Originally posted by fjwzjg at 2012-11-14 09:40:46
来个原文件

这几天小木虫无法上传文件，只好将倒出来的TXT数据拷贝过来了...
3.0    56
3.02    77
3.04    58
3.06    48
3.08    73
3.1    56
3.12    62
3.14    72
3.16    71
3.18    72
3.2    68
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3.24    67
3.26    61
3.28    60
3.3    69
3.32    50
3.34    77
3.36    56
3.38    77
3.4    61
3.42    78
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3.46    71
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3.5    62
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3.54    74
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3.58    59
3.6    45
3.62    56
3.64    53
3.66    67
3.68    60
3.7    65
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13.8    115
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17.0    150
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21.44 142
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22.16 166
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22.2    149
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22.24 132
22.26 148
22.28 148
22.3    135
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22.36 150
22.38 157
22.4    153
22.42 144
22.44 132
22.46 157
22.48 159
22.5    137
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22.54 159
22.56 154
22.58 162
22.6    142
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22.64 136
22.66 135
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22.76 147
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22.8    145
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22.86 136
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22.9    136
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22.98 138
23.0    128
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23.68 166
23.7    168
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23.8    149
23.82 173
23.84 144
23.86 139
23.88 144
23.9    137
23.92 153
23.94 158
23.96 185
23.98 161
24.0    139
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24.06 122
24.08 147
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24.26 140
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24.44 149
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24.48 142
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24.52 134
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24.56 128
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24.6    175
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24.64 157
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24.68 152
24.7    155
24.72 155
24.74 149
24.76 155
24.78 143
24.8    155
24.82 148
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24.86 135
24.88 150
24.9    150
24.92 169
24.94 163
24.96 131
24.98 144
25.0    155
25.02 131
25.04 150
25.06 169
25.08 124
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25.16 121
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25.2    138
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25.24 143
25.26 147
25.28 147
25.3    144
25.32 150
25.34 151
25.36 145
25.38 149
25.4    154
25.42 174
25.44 157
25.46 158
25.48 146
25.5    147
25.52 147
25.54 148
25.56 145
25.58 129
25.6    144
25.62 140
25.64 135
25.66 156
25.68 166
25.7    161
25.72 144
25.74 155
25.76 146
25.78 139
25.8    164
25.82 153
25.84 160
25.86 142
25.88 145
25.9    159
25.92 144
25.94 168
25.96 151
25.98 149
26.0    119
26.02 147
26.04 122
26.06 164
26.08 146
26.1    149
26.12 126
26.14 140
26.16 143
26.18 146
26.2    170
26.22 152
26.24 156
26.26 166
26.28 133
26.3    155
26.32 129
26.34 159
26.36 145
26.38 167
26.4    148
26.42 150
26.44 147
26.46 138
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43.5    181
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48.2    163
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49.2    158
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49.32 154
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49.36 145
49.38 165
49.4    137
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49.44 141
49.46 135
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49.5    155
49.52 124
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49.56 135
49.58 146
49.6    134
49.62 144
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49.9    133
49.92 141
49.94 166
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50.0    158
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50.9    170
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51.3    144
51.32 159
51.34 167
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51.4    169
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51.5    161
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51.54 136
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51.68 168
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51.76 163
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51.8    136
51.82 154
51.84 158
51.86 158
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51.9    136
51.92 144
51.94 158
51.96 132
51.98 151
52.0    161
52.02 148
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52.06 162
52.08 139
52.1    137
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52.14 146
52.16 173
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52.2    159
52.22 162
52.24 165
52.26 166
52.28 148
52.3    147
52.32 150
52.34 156
52.36 156
52.38 117
52.4    159
52.42 152
52.44 138
52.46 134
52.48 165
52.5    128
52.52 142
52.54 150
52.56 159
52.58 160
52.6    132
52.62 183
52.64 180
52.66 154
52.68 154
52.7    160
52.72 160
52.74 151
52.76 146
52.78 159
52.8    148
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79.2    155
79.22 131
79.24 133
79.25 162
79.28 142
79.3    136
79.32 128
79.34 172
79.36 153
79.38 143
79.4    175
79.42 133
79.43 159
79.46 134
79.48 147
79.5    152
79.52 164
79.54 144
79.56 138
79.58 161
79.6    140
79.62 158
79.64 138
79.66 136
79.68 134
79.7    130
79.72 151
79.74 144
79.75 167
79.78 120
79.8    140
79.82 133
79.84 159
79.86 158
79.88 152
79.9    153
79.92 168
79.93 148
79.96 149
79.98 132
80.0    123