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[求助]
求助微谱数据库
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溶剂：氘代氯仿 碳谱数据：14.2867，21.1734，22.7949，29.7961，60.5190，171.3162 |
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superspace
至尊木虫 (著名写手)
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
hy35855318: 金币+10, ★有帮助, 结果有点出乎意料，不管怎么样，谢谢~~~~ 2012-11-07 09:22:12
感谢参与，应助指数 +1
hy35855318: 金币+10, ★有帮助, 结果有点出乎意料，不管怎么样，谢谢~~~~ 2012-11-07 09:22:12
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给你重新查了一下，这是相似度在60%以上的匹配信息 1 . (±)-Selenane-2-carbonitrile 相似度:66.6% Canadian Journal of Chemistry 2010 88 831-838 Concerning the conformational preferences of the 2-cyano derivatives of oxane, thiane, and selenane Michael H. Benn, Yan Yan Huang, Frank Johannsen, Michael O’Reilly,Masood Parvez, Arvi Rauk, and Ted Sorensen Structure 13C NMR 碳谱模拟图 2 . N-methylpentan-1-amine 相似度:66.6% Indian Journal of Chemistry 2010 49B 1257-1260 A facile preparation of N-methylpentan-1-amine: A key intermediate for ibandronate sodium V V R M Krishna Reddy,U S Chintamani,D Udaykiran,G Madhusudhan* & K Mukkanti Structure 13C NMR 碳谱模拟图 3 . 10-methyl-n-heptacosane C28H58 相似度:66.6% Indian Journal of Chemistry 2006 45B 2154-2156 10-Methyl-n-heptacosane and diglucosyldirhamnoside from the stem bark of Balanites aegyptiaca Delile Ansari,M M; Ahmad,J; Ali,M; Ansari,S H Structure 13C NMR 碳谱模拟图 4 . 2,5-diethoxy-3,6-diisopropylpyrazine C14H24N2O2 相似度:66.6% Heterocycles 2010 81 1239-1251 Synthesis of (3S)-2,5-Diethoxy-3,6-dihydro-3-isopropyl-6-methylsulfanylpyrazines and Stereoselectivity in Alkylation of the Anions Yoshihide Usami, Masao Arimoto, Chisaka Kioka, Masako Yamanaka, Naoko Matsuda, and Hayato Ichikawa Structure 13C NMR 碳谱模拟图 5 . ethyl N-acetyl-3-N-chloroaminopropionate C7H12ClNO3 相似度:66.6% Heterocycles 2008 76 1511-1524 Synthesis of Substituted Aziridines via Intramolecular Reaction of β-N-Chloroethylamino Carbanions Mieczyslaw Makosza, Karolina Bobryk, and Dariusz Krajewski Structure 13C NMR 碳谱模拟图 6 . 2-(2-甲基丁酞氧基)乙基-十四酸酯 相似度:66.6% Chinese Traditional and Herbal Drugs 2007 38 1157-1159 小叶三点金化学成分研究 毛绍春;李竹英;李聪 Structure 13C NMR 碳谱模拟图 7 . β-谷甾醇-3-β-D-葡萄吡喃糖苷 相似度:66.6% Chinese Traditional and Herbal Drugs 2007 38 1157-1159 小叶三点金化学成分研究 毛绍春;李竹英;李聪 Structure 13C NMR 碳谱模拟图 8 . N,N'-Terephthaloyl-bis-(2,6-dimethylpiperidine) C22H32N2O2 相似度:66.6% Zeitschrift für Naturforschung B 2011 66 397-406 Weak Hydrogen Bonds in the Molecular Packing of N-Tetraalkyl Terephthalamides P. G. Jones and P. Ku\'s Structure 13C NMR 碳谱模拟图 9 . compound Va 相似度:66.6% Russian Journal of Organic Chemistry 2008 44 1235-1237 ReductiveselenationofaliphaticketonestodialkyldiselenideswithSe-CO-H2Ounderatmosphericpressure Yahong Chen, Fengshou Tian, Maoping Song and Shiwei Lu Structure 13C NMR 碳谱模拟图 10 . bis(endo-6-bicyclo[3.1.1]heptyl) sulfone C14H22O2S 相似度:66.6% Russian Journal of Organic Chemistry 2002 38 1582-1587 Products of Reaction of Tricyclo[4.1.0.02,7]heptane and 1-Bromotricyclo[4.1.0.02,7]heptane with Hydrogen Sulfide, and Syntheses Based Thereon V. A. Vasin, S. G. Kostryukov and V. V. Razin Structure 13C NMR 碳谱模拟图 11 . 5-butyltetrazole 相似度:66.6% European Journal of Organic Chemistry 2011 6343-6355 Highly Efficient Synthesis of 5-Substituted 1H-Tetrazoles Catalyzed by Cu–Zn Alloy Nanopowder, Conversion into 1,5- and 2,5-Disubstituted Tetrazoles, and Synthesis and NMR Studies of New Tetrazolium Ionic Liquids Gopalakrishnan Aridoss and Kenneth K. Laali Structure 13C NMR 碳谱模拟图 12 . butanedioic acid monoethyl ester 相似度:66.6% Journal of Medicinal Chemistry 2007 50 1528-1536 Synthesis and Anti-Cancer Activity of C-Ring-Functionalized Prodigiosin Analogues Jasmine Regourd, Adeeb Al-Sheikh Ali, and Alison Thompson Structure 13C NMR 碳谱模拟图 13 . 3-chlorocarbonyl-propanoic acid ethyl ester 相似度:66.6% Journal of Medicinal Chemistry 2007 50 1528-1536 Synthesis and Anti-Cancer Activity of C-Ring-Functionalized Prodigiosin Analogues Jasmine Regourd, Adeeb Al-Sheikh Ali, and Alison Thompson Structure 13C NMR 碳谱模拟图 14 . Methyl 2-methyl-6-oxopiperidine-2-carboxylate C8H13NO3 相似度:62.5% Molecules 2007 12 439-454 Solventless Lactam Synthesis by Intramolecular Cyclizations of α-Iminoester Derivatives under Microwave Irradiation Fatima-Zohra Zradni, Jack Hamelin and Aicha Derdour Structure 13C NMR 碳谱模拟图 15 . compound 2a(less polar) C8H12BrNO3 相似度:62.5% Tetrahedron Letters 2001 42 6041-6044 Influence of N-substituted lactams on acyclic free radical based hydrogen transfer Yvan Guindon, Mohammed Bencheqroun Structure 13C NMR 碳谱模拟图 16 . 3-oxooctanoic acid C8H14O3 相似度:62.5% European Journal of Organic Chemistry 2011 311-318 A Stereoselective and Practical Synthesis of (E)-,β-Unsaturated Ketones from Aldehydes Evita Balducci, Emanuele Attolino and Maurizio Taddei Structure 13C NMR 碳谱模拟图 17 . (Z)-Oct-2-enyl acetate 相似度:60% Chemistry-A European Journal 2008 14 10978-10984 Synthesis and Cannabinoid Receptor Activity of Ketoalkenes from Echinacea pallida and Nonnatural Analogues Michael Egger, Patrina Pellett, Kathrin Nickl, Sarah Geiger, Stephanie Graetz, Roland Seifert, Jörg Heilmann and Burkhard König Structure 13C NMR 碳谱模拟图 |
3楼2012-11-06 22:05:42
潘宪伟
木虫 (正式写手)
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【答案】应助回帖
★ ★ ★ ★ ★
感谢参与，应助指数 +1
hy35855318: 金币+5, ★有帮助, 仿佛对不上，如果碳谱数据是:14,21,60,171是怎么样的呢，麻烦您了，谢谢~~~ 2012-11-06 20:45:08
感谢参与，应助指数 +1
hy35855318: 金币+5, ★有帮助, 仿佛对不上，如果碳谱数据是:14,21,60,171是怎么样的呢，麻烦您了，谢谢~~~ 2012-11-06 20:45:08
|
1 . 10-methyl-n-heptacosane C28H58 相似度:66.6% Indian Journal of Chemistry 2006 45B 2154-2156 10-Methyl-n-heptacosane and diglucosyldirhamnoside from the stem bark of Balanites aegyptiaca Delile Ansari,M M; Ahmad,J; Ali,M; Ansari,S H Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . ethyl N-acetyl-3-N-chloroaminopropionate C7H12ClNO3 相似度:66.6% Heterocycles 2008 76 1511-1524 Synthesis of Substituted Aziridines via Intramolecular Reaction of β-N-Chloroethylamino Carbanions Mieczyslaw Makosza, Karolina Bobryk, and Dariusz Krajewski Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 2-(2-甲基丁酞氧基)乙基-十四酸酯 相似度:66.6% Chinese Traditional and Herbal Drugs 2007 38 1157-1159 小叶三点金化学成分研究 毛绍春;李竹英;李聪 Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . β-谷甾醇-3-β-D-葡萄吡喃糖苷 相似度:66.6% Chinese Traditional and Herbal Drugs 2007 38 1157-1159 小叶三点金化学成分研究 毛绍春;李竹英;李聪 Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . compound 4u 相似度:66.6% Tetrahedron Letters 2002 43 3203-3207 Chemical versus enzymatic acetylation of α-bromo-ω-hydroxyaldehydes: decyclization of hemiacetals by lipase Ly Villo, Andrus Metsala, Omar Parve, Tõnis Pehk Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . N,N'-Terephthaloyl-bis-(2,6-dimethylpiperidine) C22H32N2O2 相似度:66.6% Zeitschrift für Naturforschung B 2011 66 397-406 Weak Hydrogen Bonds in the Molecular Packing of N-Tetraalkyl Terephthalamides P. G. Jones and P. Ku\'s Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . compound Va 相似度:66.6% Russian Journal of Organic Chemistry 2008 44 1235-1237 ReductiveselenationofaliphaticketonestodialkyldiselenideswithSe-CO-H2Ounderatmosphericpressure Yahong Chen, Fengshou Tian, Maoping Song and Shiwei Lu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 5-butyltetrazole 相似度:66.6% European Journal of Organic Chemistry 2011 6343-6355 Highly Efficient Synthesis of 5-Substituted 1H-Tetrazoles Catalyzed by Cu–Zn Alloy Nanopowder, Conversion into 1,5- and 2,5-Disubstituted Tetrazoles, and Synthesis and NMR Studies of New Tetrazolium Ionic Liquids Gopalakrishnan Aridoss and Kenneth K. Laali Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . butanedioic acid monoethyl ester 相似度:66.6% Journal of Medicinal Chemistry 2007 50 1528-1536 Synthesis and Anti-Cancer Activity of C-Ring-Functionalized Prodigiosin Analogues Jasmine Regourd, Adeeb Al-Sheikh Ali, and Alison Thompson Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 3-chlorocarbonyl-propanoic acid ethyl ester 相似度:66.6% Journal of Medicinal Chemistry 2007 50 1528-1536 Synthesis and Anti-Cancer Activity of C-Ring-Functionalized Prodigiosin Analogues Jasmine Regourd, Adeeb Al-Sheikh Ali, and Alison Thompson Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . Methyl 2-methyl-6-oxopiperidine-2-carboxylate C8H13NO3 相似度:62.5% Molecules 2007 12 439-454 Solventless Lactam Synthesis by Intramolecular Cyclizations of α-Iminoester Derivatives under Microwave Irradiation Fatima-Zohra Zradni, Jack Hamelin and Aicha Derdour Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . compound 2a(less polar) C8H12BrNO3 相似度:62.5% Tetrahedron Letters 2001 42 6041-6044 Influence of N-substituted lactams on acyclic free radical based hydrogen transfer Yvan Guindon, Mohammed Bencheqroun Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 3-oxooctanoic acid C8H14O3 相似度:62.5% European Journal of Organic Chemistry 2011 311-318 A Stereoselective and Practical Synthesis of (E)-,β-Unsaturated Ketones from Aldehydes Evita Balducci, Emanuele Attolino and Maurizio Taddei Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . (Z)-Oct-2-enyl acetate 相似度:60% Chemistry-A European Journal 2008 14 10978-10984 Synthesis and Cannabinoid Receptor Activity of Ketoalkenes from Echinacea pallida and Nonnatural Analogues Michael Egger, Patrina Pellett, Kathrin Nickl, Sarah Geiger, Stephanie Graetz, Roland Seifert, Jörg Heilmann and Burkhard König Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 1-Methyl-2-oxa-5-azoniaspiro[4.4]nonane Bis[(trifluoromethyl)sulfonyl]azanide 相似度:57.1% Helvetica Chimica Acta 2009 92 1600-1609 Synthesis of Oxygen-Containing Spirobipyrrolidinium Salts for High Conductivity Room Temperature Ionic Liquids Seiichiro Higashiya, Thamarai Selvi Devarajan, Manisha V. Rane-Fondacaro, Christopher Dangler, Jeremy Snyder, Pradeep Haldar Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . t-Bu2P(CH2)4CH3 C14H39P 相似度:57.1% Canadian Journal of Chemistry 2009 87 1620-1624 Copolymerization of sterically demanding phosphine-olefins and 1-hexene Jenny S.J. McCahill and Douglas W. Stephan Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . 环(甘-L-脯)二肽(cyclo-(Gly-L-Pro)) 相似度:57.1% Chinese Journal of Marine Drugs 2010 29(5) 16-21 Study of anti-MRSA bioactive constituents from a marine actinomycetes Micromonospora sp.(No,69) LI Yi, TANG Jin-shan, GAO Hao, LIN Hai-peng, HONG Kui, YAO Xin-sheng Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . 吡咯并哌嗪2,5-二酮 C7H10N2O2 相似度:57.1% Chinese Journal of Marine Drugs 2005 24(2) 9-12 Studies on the chemical constituents of the fermentation liquid from marine bacterium Bacillus sp. ZHANG Hai-long, FU Hong-wei, TIAN Li, HUA Hui-ming, PEI Yue-hu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . cyclo(L-Pro-Gly) 相似度:57.1% Bioorganic & Medicinal Chemistry Letters 2012 22 3177-3180 The effects of diketopiperazines from Callyspongia sp. on release of cytokines and chemokines in cultured J774A.1 macrophages Jin-Hui Chen, Xiang-Peng Lan, Yonghong Liu, Ai-Qun Jia Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . 1-butyl-3,4,5,6-tetrachloro-2,7-dihydro-1H-azepine 相似度:57.1% Journal of Heterocyclic Chemistry 2002 39 1273-1278 Easy access to medium rings by entropy/strain reduction, Part 3. Competition between dihydroazepine and enamine formation in reaction of tetrahalosubstituted dibromides with primary amines James G. Walsh and Declan G. Gilheany |
2楼2012-11-06 20:16:05