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1power1

木虫 (正式写手)

[求助] 求微谱

氘代氯仿
11.6,14.7,15.8,16.3,17.3,18.0,18.5,19.3,20.4,27.4,29.3,30.7,32.6,34.2,34.3,34.9,35.1,35.2,35.6,37.4,37.6,37.7,39.2,41.6,49.2,52.6,61.3,72.8
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1power1

木虫 (正式写手)

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2楼: Originally posted by yanghaowei at 2012-10-29 21:31:45
1 .     epifriedelinol
    相似度:86.2%
Korean Journal of Pharmacognosy          2007          38(1)          67-70
Isolation of Isoprenoidal Compounds from the Stems of Acer tegmentosum Max
Hu ...

氘代氯仿
14.7,16.3,17.3,18.0,18.5,19.3,20.4,27.4,29.3,30.7,32.6,34.2,34.3,34.9,35.1,37.4,37.6,37.7,39.2,41.6,52.6,61.3
3楼2012-10-29 22:05:45
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yanghaowei

木虫 (小有名气)

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感谢参与,应助指数 +1
1power1: 金币+30, ★★★★★最佳答案 2012-10-29 21:39:01
1 .     epifriedelinol
    ?????:86.2%
Korean Journal of Pharmacognosy          2007          38(1)          67-70
Isolation of Isoprenoidal Compounds from the Stems of Acer tegmentosum Max
Hur, Jong-Moon; Jun, Mi-Ra; Yang, Eun-Ju; Choi, Sun-Ha; Park, Jong-Cheol; Song, Kyung-Sik
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

2 .     4??-methyl-3??-hydroxylfriedelan
    ?????:86.2%
Journal of Shenyang Pharmaceutical University          2009          26          348-352
Chemical constituents from Portulaca oleracea L.
DING Huai-wei, LI Fei-fei, SONG Shao-jiang
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

3 .     3-Epifriedelinol
    ?????:83.3%
Biochemical Systematics and Ecology          2005          33          445-449
Terpenes and acetylene derivatives from the roots of Santolina corsica (Asteraceae)
Bernard Ferrari, F??lix Tomi, Joseph Casanova
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

4 .     f riedelinol
    ?????:83.3%
Guihaia          2008          28          558-560
Chemical constituents of Vaccinium carlesii
WEI Jian; YANG Xiao-Sheng; ZHU Hai-Yan; HAO Xiao-Jiang
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

5 .     epi-friedelanol
    ?????:83.3%
China Journal of Chinese Materia Medica          2007          32          403-406
Study on chemical constituents of Myricaria paniculata I
Li Shuai, CHENG Ruoyun, YU Dequan
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

6 .     epifriedelanol
    ?????:83.3%
China Journal of Chinese Materia Medica          2003          28          235-237
Studies on the Constituents from the Herb of Vernonia patutula
LIANG Qiaoli, MIN Zhida
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

7 .     friedelan-3??-ol
    ?????:83.3%
China Journal of Chinese Materia Medica          1998          23          552-553
Studies on Chemical constituents of Conyza blinii L??vl.
Xu Liping, Liu Jiansheng, Min De, Wang Sanwu, Zhang Zhizhen, Guo Dean and Zheng Junhua
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

8 .     epifriedlinol
    ?????:83.3%
China Journal of Chinese Materia Medica          1997          22          423-424
Studies on Fat Soluble Constituents of the Leaves of Vaccinium bracteatum Thunb
Tu Pengfei , Liu jiangyun and Li J unshan
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

9 .     epifriedelanol
C30H52O     ?????:83.3%
Fitoterapia          2000          71          577-579
Antitumor activity of epifriedelanol from Vitis trifolia
J.K. Kundu, A.S.S. Rouf, Md. Nazmul Hossain, C.M.Hasan, M.A. Rashid
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

10 .     epifriedelanol
    ?????:83.3%
Phytochemistry          1998          49          1115-1118
Acyclic diterpenes from perymenium HINTONII
Emma Maldonado, Marisela Bello, Jos?? Luis Villaseñor, Alfredo Ortega
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

11 .     Friedlan-3??-ol
C30H52O     ?????:83.3%
Zeitschrift f??r Naturforschung B          2010          65b          521-524
Terpenoids from Clerodendrum formicarum G??rke (Lamiaceae) of Cameroon
Muhammad Shaiq Ali, Zeeshan Ahmed, Joseph Ngoupayo, and Muhammad Imran Ali
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

12 .     epifridelelanol
    ?????:83.3%
China Journal of Chinese Materia Medica          2010          35          1720-1722
Chemical constituents of stem barks of Mucuna birdwoodiana
GONG Ting; WANG Dongxiao; Liu Ping; CHEN Ruoyun
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

13 .     friedelinol
    ?????:83.3%
China Journal of Chinese Materia Medica          2010          35          327-330
Triterpenes from Kalimeris indica
GONG Xiaojian; ZHOU Xin; ZHAO Chao; CHEN Huaguo; XU Wenqing; LONG Shangxiang
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

14 .     epifriedelanol
    ?????:83.3%
Fitoterapia          2010          81          586-589
Triterpenoids from Calophyllum inophyllum and their growth inhibitory effects on human leukemia HL-60 cells
Yan-Zhi Li, Zhan-Lin Li, Shi-Liang Yin, Guang Shi, Ming-Sheng Liu, Yong-Kui Jing, Hui-Ming Hua
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

15 .     ??????
    ?????:83.3%
Chinese Traditional and Herbal Drugs          2003          34          785-786
??????????????????о?
????,?????,?????,??????,???
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

16 .     epi-friedelanol
    ?????:83.3%
Chinese Journal of Natural Medicines          2005          3          25-27
Studies on the Chemical Constituents of Paeonia veitchii L.
WANG Rui; CHOU Gui-Xin; ZHU En-Yuan; WANG Zheng-Tao; BI Kai-Shun
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

17 .     epi-friedelinol
C30H52O     ?????:83.3%
Chinese Journal of Natural Medicines          2006          4          156-158
Chemical Constituents of Gynura divaricata
HU Yong; LI Wei-Lin; LIN Hou-Wen; ZHUO Min; REN Bing-Ru
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

18 .     Friedelinol
C30H52O     ?????:83.3%
Pharmazie          2004          59          882-884
Pentacyclic triterpenoids from Aster ageratoides var. pilosus
Fu-Lin Yan, Ai-Xia Wang, and Zhong-Jian Jia
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

19 .     Epifriedelanol
    ?????:83.3%
Archives of Pharmacal Research          2005          28          39-43
Antitumor and antiinflammatory constituents from celtis sinensis
Dae Keun Kim, Jong Pil Lim, Jin Wook Kim, Hee Wook Park and Jae Soon Eun
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

20 .     ??-Sitosterol
    ?????:83.3%
Archives of Pharmacal Research          2005          28          39-43
Antitumor and antiinflammatory constituents from celtis sinensis
Dae Keun Kim, Jong Pil Lim, Jin Wook Kim, Hee Wook Park and Jae Soon Eun
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

21 .     epifriedelanol
    ?????:83.3%
Chemistry of Natural Compounds          2010          46          298-300
Chemical constituents from Inula cappa
Zhi-Jun Wu, Lei Shan, Min Lu, Yun-Heng Shen and Jian Tang, et al.
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

22 .     friedelan-3-ol
    ?????:83.3%
Chinese Pharmaceutical Journal          2006          41          251-253
Studies on Chemical Constituents of Kalimeris indica
LIN Cai, CAO Pei-xue, LIANG Guang-yi
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

23 .     epifriedelanol
    ?????:83.3%
Chinese Pharmaceutical Journal          2007          42          494-496
Studies on Triterpenes from Elephantopus scaber
LIANG Qiao-li, GONG Zhu-nan, MIN Zhi-da
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

24 .     ??????
    ?????:83.3%
Modern Chinese Medicine          2008          10(6)          20-22
Study on chemical Constituents from Aster tataricus L. f.
Jin Jing, Zhang Chaofeng, Zhang Mian
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

25 .     4??-methyl-3??-hydroxylfriedelan
C30H42O     ?????:83.3%
Journal of Shenyang Pharmaceutical University          2007          24          727-757
Chemical constituents from the Portulaca oleracea L.
YAO Jia-qi, MENG Na, SONG Shao-jiang, DING Huai-wei
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

26 .     epifriedelanol
C30H52O     ?????:83.3%
Journal of Shenyang Pharmaceutical University          2006          23          764-767
Chemical constituents of root barks of Ulmus pumila (II)
WANG Dong, CUI Zheng, DONG Yan, FU Ming-yao
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

27 .     ??????
    ?????:83.3%
Journal of Shenyang Pharmaceutical University          1999          16          194-197
A Study on the Chemical Constituents of Quercus engleriana Seem.
Zhou Yingjun, Sun Qishi
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

28 .     epifricdelinol
    ?????:83.3%
Journal of Shenyang Pharmaceutical University          1999          16          194-197
A Study on the Chemical Constituents of Quercus engleriana Seem.
Zhou Yingjun, Sun Qishi
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

29 .     ??????
    ?????:83.3%
Journal of Shenyang Pharmaceutical University          1999          16          235-256
A Study on the Chemical Constituents of the Leaves of Quercus acut issima Carruth.
Yuan Jiuzhi, Sun Qishi
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

30 .     Epi-friedelanol
    ?????:83.3%
Journal of China Pharmaceutical University          1998          29          97-99
Studies on the Constituents of Aster tataricus L.f.
Lu Yanhua; Wang Zhengtao; Ye Wencai; Xu Luoshan; Shu Yaozhong
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

31 .     friedelinol
    ?????:83.3%
Natural Product Research and Development          2010          22          995-997
Chemical Constituent of Active Fraction from Radix Aerio Fici microcarpae L.
YA Qi-kang; LU Wen-jie; CHEN Jia-yuan; TAN Xiao
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

32 .     epifriedelanol
    ?????:83.3%
Natural Product Research and Development          2005          17          166-168
Lipophilic Constituents from the Leaves of Ipomoea batatas(cv.Simon)
LUO Jian-guang; KONG Ling-yi
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

33 .     friedelinol
    ?????:83.3%
Journal of the Chinese Chemical Society          1995          42          93-95
Chemical Components from Triumfetta bartramia
??禮??(Li-Kang Ho);??????(Chiann-Rong Chang);??????(Yuan-Shiun Chang)
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

34 .     ?????-3??-??
    ?????:83.3%
Chinese Traditional and Herbal Drugs          2011          42          450-453
Chemical constituents of Equisetum ramosissimum
YU Hong-wei, YAN Ming-ming, YANG Zhi, FU Ying-chao, YU Lei, ZHAN Yue, WAN Zhi-qiang
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

35 .     friedelan-4-??-methyl-3??-OH
C30H52O     ?????:80.6%
Journal of Chinese Pharmaceutical Sciences          2004          13          291-292
Chemical Constituents from Portulaca oleracea L.
SUN JianSupervisors: ZHANG Hong-gui; ZHANG Jing-min; ZHANG Tian-bin; GUO Bin5; ZHANG Han-qi
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

36 .     epifriedlinol
    ?????:80%
China Journal of Chinese Materia Medica          1997          22          103-104
Studies on the Chemical Constituents of Aster poliothamnus Diels
Zhang Jiamin and Chen Yaozu, Li Bogang and Wang Mingkui
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

37 .     3-epi-friedelinol
C30H52O     ?????:80%
Natural Product Sciences          2006          12          89-93
Chemical Constituents of Gomphrena globosa. II
Dinda, Biswanath; Ghosh, Biplab; Achari, Basudev; Arima, Shiho; Sato, Nariko; Harigaya, Yoshihiro
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

38 .     compound 190
    ?????:80%
Phytochemistry          1994          37          1517-1575
13C NMR Spectra of pentacyclic triterpenoids??a compilation and some salient features
Shashi B. Mahato, Asish P. Kundu
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

39 .     epi-friedelinol
C30H52O     ?????:80%
Indian Journal of Chemistry          2009          48B          291-294
Flavones and acridones from Atalantia wightii
Kumar,Satish; Raj,Kanwal; Khare,Pratibha
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

40 .     3??-friedelinol
    ?????:80%
Magnetic Resonance in Chemistry          2000          38          977-980
Two epimeric friedelane triterpenes isolated from Maytenus truncata Reiss: 1H and 13C chemical shift assignments
G. C. M. Salazar, G. D. F. Silva, L. P. Duarte, S. A. Vieira Filho and I. S. Lula
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

41 .     canophyllic acid
    ?????:80%
Fitoterapia          2010          81          586-589
Triterpenoids from Calophyllum inophyllum and their growth inhibitory effects on human leukemia HL-60 cells
Yan-Zhi Li, Zhan-Lin Li, Shi-Liang Yin, Guang Shi, Ming-Sheng Liu, Yong-Kui Jing, Hui-Ming Hua
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

42 .     friedelan-3??-ol
    ?????:80%
Natural Product Research and Development          2001          13(1)          14-16
STUDY ON THE CHEMICAL CONSTITUENTS OF ASPIDOPTERYS OBCORDATA HEMSL.
WU Rui; YE Qi; CHEN Neng yu; ZHANG Guo lin
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

43 .     friedelan-3??-ol
    ?????:80%
Journal of Ethnopharmacology          2000          72          465-468
Evaluation of the antiulcerogenic activity of friedelan-3??-ol and friedelin isolated from Maytenus ilicifolia (Celastraceae)
Carmen Lucia Queiroga, Guilherme Faria Silva, Patrı́cia Corr??a Dias, Ana Possenti, João Ernesto de Carvalho
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

44 .     epifriedelanol
    ?????:80%
Chinese Traditional and Herbal Drugs          2011          42          251-254
Chemical constituents of Omphalia lapidescens
XU Ming-feng, SHEN Lian-qing, WANG Kui-wu
Structure      13C NMR   ???????
2楼2012-10-29 21:31:45
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1power1

木虫 (正式写手)

帮忙重新微一下行不?数据有点不对。
氘代氯仿
14.7,16.3,17.3,18.0,18.5,19.3,20.4,27.4,29.3,30.7,32.6,34.2,34.3,34.9,35.1,37.4,37.6,37.7,39.2,41.6,52.6,61.3
4楼2012-10-29 22:08:37
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yanghaowei

木虫 (小有名气)

引用回帖:
4楼: Originally posted by 1power1 at 2012-10-29 22:08:37
帮忙重新微一下行不?数据有点不对。
氘代氯仿
14.7,16.3,17.3,18.0,18.5,19.3,20.4,27.4,29.3,30.7,32.6,34.2,34.3,34.9,35.1,37.4,37.6,37.7,39.2,41.6,52.6,61.3

70%以上只有一个

1 .     methyl 2α-acetoxy-3β,4β-epoxy-neo-clerodan-15-oate
    相似度:73.9%
Tetrahedron          1994          50          10791-10802
Ring a functionalized Neo-clerodane diterpenoids from Cistus populifolius
Julio G. Urones, Pilar Basabe, Isidro S. Marcos, Alicia Jiménez, Anna M. Lithgow, Margarita López, Rosalina F. Moro, Antonio Gómez
Structure      13C NMR   碳谱模拟图
5楼2012-10-30 13:00:17
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