| 查看: 694 | 回复: 4 | |||
| 当前主题已经存档。 | |||
| 【有奖交流】积极回复本帖子，参与交流，就有机会分得作者 wjh522996 的 1 个金币 | |||
wjh522996银虫 (正式写手)
|
[交流]
X射线能谱仪中Cu和Mg的出峰位置？？？
|
||
|
那位大侠告我X射线能谱仪分析中Cu和Mg的出峰位置，测试时忘了标注，谢谢！！ [ Last edited by dongfang1629 on 2007-6-19 at 10:53 ] |
回复此楼» 猜你喜欢
316求调剂
已经有14人回复
-
chinese chemical letters英文版投稿求助
已经有6人回复
-
264分，求任意工科调剂
已经有5人回复
-
求生物学调剂
已经有9人回复
-
求调剂 302分初试 0854
已经有3人回复
-
交通运输考试264分求工科调剂
已经有3人回复
-
材料与化工306分找调剂
已经有8人回复
-
一志愿北京科技材料科学与工程288分，求调剂
已经有13人回复
-
413求调剂
已经有3人回复
-
319求调剂
已经有14人回复
zjx121610
木虫 (文坛精英)
做个会思考的虫子！
- 应助: 0 (幼儿园)
- 贵宾: 0.35
- 金币: 3551.1
- 红花: 4
- 帖子: 10774
- 在线: 16.6小时
- 虫号: 205726
- 注册: 2006-03-03
- 性别: GG
- 专业: 色谱分析
★
dongfang1629(金币+1):谢谢应助!!
dongfang1629(金币+1):谢谢应助!!
|
你是做金属粉末吗？ PDF#04-0836: QM=Star(+); d=(Unknown); I=Diffractometer Copper, syn Cu (Red) Radiation=CuKa1 Lambda=1.5405 Filter=Ni Calibration= d-Cutoff= I/Ic(RIR)= Ref= Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539, I 15 (1953) Cubic - Powder Diffraction, Fm-3m (225) Z=4 mp=1083 Cell=3.615 Pearson=cF4 (Cu) Density(c)=8.936 Density(m)=8.950 Mwt=63.55 Vol=47.24 F(8)=87.0(.0115,8) Ref= Ibid. Strong Line: 2.09/X 1.81/5 1.28/2 1.09/2 0.83/1 0.81/1 1.04/1 0.90/1 0.00/1 0.00/1 NOTE: It had been heated in an H2 atmosphere at 300 C. See ICSD 64699 (PDF 01-085-1326). Sample from metallurgical laboratory of NBS, Gaithersburg, Maryland, USA. Pattern taken at 26 C. Impurities from 0.001-0.01%, Ag, Al, Bi, Fe, Si, Zn. Opaque mineral optical data on specimen from unspecified locality, R3R%=60.65, Disp.=Std. VHN100=96-104, d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.0880 100.0 100.0 1 1 1 3 43.297 21.648 0.2395 3.0092 1.8080 46.0 53.0 2 0 0 4 50.433 25.216 0.2765 3.4752 1.2780 20.0 33.0 2 2 0 8 74.130 37.065 0.3912 4.9164 1.0900 17.0 33.0 3 1 1 11 89.931 44.965 0.4587 5.7644 1.0436 5.0 10.0 2 2 2 12 95.139 47.570 0.4791 6.0207 0.9038 3.0 7.0 4 0 0 16 116.918 58.459 0.5532 6.9520 0.8293 9.0 23.0 3 3 1 19 136.507 68.253 0.6029 7.5765 0.8083 8.0 21.0 4 2 0 20 144.714 72.357 0.6186 7.7733 [ Last edited by zjx121610 on 2007-6-19 at 20:13 ] |
2楼2007-06-19 20:09:29
zjx121610
木虫 (文坛精英)
做个会思考的虫子！
- 应助: 0 (幼儿园)
- 贵宾: 0.35
- 金币: 3551.1
- 红花: 4
- 帖子: 10774
- 在线: 16.6小时
- 虫号: 205726
- 注册: 2006-03-03
- 性别: GG
- 专业: 色谱分析
|
PDF#35-0821: QM=Star(+); d=Diffractometer; I=Diffractometer Magnesium Mg (Dark gray) Radiation=CuKa1 Lambda=1.5405981 Filter=Graph Calibration=Internal(W) d-Cutoff=17.7 I/Ic(RIR)= Ref= Natl. Bur. Stand. (U.S.) Monogr. 25, 21 82 (1985) Hexagonal - Powder Diffraction, P63/mmc (194) Z=2 mp= Cell=3.2094x5.2112 Pearson=hP2 (Mg) Density(c)=1.736 Density(m)=1.74A Mwt=24.31 Vol=46.48 F(27)=75.3(.0124,29) Ref= Jevins, A. et al. Z. Phys. Chem. (B), 40 347 (1938) Strong Line: 2.45/X 2.61/4 2.78/3 1.47/2 1.90/2 1.37/1 1.60/1 1.34/1 1.03/1 1.09/1 NOTE: The sample was obtained from Fisher Scientific Company, Fair Lawn, New Jersey, USA. It contained a small amount of Mg ( O H )2. The temperature of data collection was approximately 25.0 C. To replace 00-004-0770. Pyrotechnic. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.7782 25.0 22.0 1 0 0 32.193 16.097 0.1800 2.2616 2.6050 36.0 34.0 0 0 2 34.398 17.199 0.1919 2.4120 2.4520 100.0 100.0 1 0 1 36.619 18.310 0.2039 2.5625 1.9002 15.0 19.0 1 0 2 47.828 23.914 0.2631 3.3066 1.6047 12.0 18.0 1 1 0 57.374 28.687 0.3116 3.9155 1.4730 16.0 27.0 1 0 3 63.056 31.528 0.3394 4.2655 1.3899 2.0 4.0 2 0 0 67.312 33.656 0.3597 4.5207 1.3664 13.0 23.0 1 1 2 68.631 34.316 0.3659 4.5985 1.3430 8.0 15.0 2 0 1 69.996 34.998 0.3723 4.6784 1.3028 2.0 4.0 0 0 4 72.493 36.246 0.3838 4.8229 1.2264 2.0 4.0 2 0 2 77.821 38.910 0.4077 5.1234 1.1797 2.0 4.0 1 0 4 81.526 40.763 0.4238 5.3260 1.0854 3.0 7.0 2 0 3 90.412 45.206 0.4606 5.7886 1.0506 1.0 2.0 2 1 0 94.312 47.156 0.4759 5.9808 1.0299 4.0 10.0 2 1 1 96.817 48.408 0.4855 6.1006 1.0116 3.0 7.0 1 1 4 99.184 49.592 0.4943 6.2111 0.9760 2.0 5.0 1 0 5 104.232 52.116 0.5123 6.4380 0.9742 2.0 5.0 2 1 2 104.497 52.249 0.5132 6.4496 0.9505 1.0 3.0 2 0 4 108.263 54.132 0.5260 6.6102 0.9266 1.0 3.0 3 0 0 112.473 56.236 0.5396 6.7812 0.8988 2.0 5.0 2 1 3 117.959 58.980 0.5563 6.9904 0.8729 1.0 3.0 3 0 2 123.881 61.940 0.5728 7.1982 0.8338 1.0 3.0 2 0 5 134.979 67.490 0.5997 7.5355 0.8289 1.0 3.0 1 0 6 136.639 68.320 0.6032 7.5800 0.8178 1.0 3.0 2 1 4 140.731 70.366 0.6114 7.6827 0.8174 1.0 3.0 3 0 3 140.882 70.441 0.6117 7.6863 0.8023 1.0 3.0 2 2 0 147.515 73.758 0.6232 7.8314 |
3楼2007-06-19 20:10:23
zjx121610
木虫 (文坛精英)
做个会思考的虫子！
- 应助: 0 (幼儿园)
- 贵宾: 0.35
- 金币: 3551.1
- 红花: 4
- 帖子: 10774
- 在线: 16.6小时
- 虫号: 205726
- 注册: 2006-03-03
- 性别: GG
- 专业: 色谱分析
|
PDF#65-3365: QM=Calculated; d=Calculated; I=Calculated Magnesium Mg Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= d-Cutoff= I/Ic(RIR)=4.01 Ref= Calculated from NIST using POWD-12++ Hexagonal - (Unknown), P63/mmc (194) Z=2 mp= Cell=3.2089x5.2101 Pearson=hP2 (Mg) Density(c)=1.737 Density(m)=1.74A Mwt=24.31 Vol=46.46 F(27)=203.6(.0046,29) Ref= G.Raynor Proc. R. Soc. London, Ser. A, A17 457 (1940) Strong Line: 2.45/X 2.61/3 2.78/2 1.47/2 1.37/1 1.60/1 1.90/1 1.34/1 1.03/1 0.90/1 NOTE: N AL4841 5594 IB=Mg See PDF 01-089-4894. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.7790 24.5 21.6 1 0 0 32.184 16.092 0.1799 2.2610 2.6051 26.9 25.3 0 0 2 34.397 17.199 0.1919 2.4119 2.4520 100.0 100.0 1 0 1 36.618 18.309 0.2039 2.5625 1.9006 14.0 18.1 1 0 2 47.818 23.909 0.2631 3.3059 1.6044 14.5 22.2 1 1 0 57.383 28.691 0.3116 3.9161 1.4728 15.3 25.5 1 0 3 63.070 31.535 0.3395 4.2663 1.3895 2.0 3.5 2 0 0 67.334 33.667 0.3598 4.5219 1.3661 14.6 26.2 1 1 2 68.644 34.322 0.3660 4.5993 1.3426 10.1 18.4 2 0 1 70.022 35.011 0.3724 4.6800 1.3025 2.0 3.8 0 0 4 72.509 36.254 0.3839 4.8238 1.2260 2.3 4.6 2 0 2 77.848 38.924 0.4078 5.1249 1.1794 1.9 4.0 1 0 4 81.553 40.777 0.4239 5.3274 1.0850 3.9 8.8 2 0 3 90.463 45.231 0.4608 5.7911 1.0504 1.1 2.6 2 1 0 94.336 47.168 0.4760 5.9819 1.0296 6.3 15.0 2 1 1 96.853 48.427 0.4856 6.1023 1.0112 3.9 9.5 1 1 4 99.232 49.616 0.4944 6.2133 0.9757 2.7 6.8 1 0 5 104.273 52.137 0.5125 6.4398 0.9742 2.0 5.0 2 1 2 104.505 52.252 0.5133 6.4499 0.9503 0.8 2.1 2 0 4 108.305 54.153 0.5262 6.6119 0.9263 1.5 4.0 3 0 0 112.514 56.257 0.5398 6.7829 0.8988 4.1 11.2 2 1 3 117.972 58.986 0.5563 6.9909 0.8728 2.6 7.3 3 0 2 123.902 61.951 0.5729 7.1989 0.8684 0.4 1.1 0 0 6 125.013 62.506 0.5758 7.2358 0.8336 1.7 5.0 2 0 5 135.033 67.517 0.5998 7.5370 0.8288 0.6 1.8 1 0 6 136.670 68.335 0.6033 7.5808 0.8176 1.1 3.3 3 0 3 140.810 70.405 0.6115 7.6846 0.8176 1.1 3.3 2 1 4 140.810 70.405 0.6115 7.6846 0.8022 1.1 3.4 2 2 0 147.553 73.777 0.6233 7.8322 |
4楼2007-06-19 20:11:13
zjx121610
木虫 (文坛精英)
做个会思考的虫子！
- 应助: 0 (幼儿园)
- 贵宾: 0.35
- 金币: 3551.1
- 红花: 4
- 帖子: 10774
- 在线: 16.6小时
- 虫号: 205726
- 注册: 2006-03-03
- 性别: GG
- 专业: 色谱分析
★
mxg330(金币+1):谢谢应助～～～
mxg330(金币+1):谢谢应助～～～
|
PDF#65-7219: QM=Calculated; d=Calculated; I=Calculated Magnesium Mg Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= d-Cutoff= I/Ic(RIR)=5.55 Ref= Calculated from NIST using POWD-12++ Cubic - (Unknown), Im-3m (229) Z=2 mp= Cell=2.953 Pearson=cI2 (W) Density(c)=3.135 Density(m)=1.74A Mwt=24.31 Vol=25.75 F(6)=999.9(.0002,6) Ref= Olijnyk, H., Holzapfel, W. B. Phys. Rev. B: Condens. Matter, 31 4682 (1985) Strong Line: 2.09/X 1.21/2 1.48/1 0.93/1 1.04/1 0.85/1 0.00/1 0.00/1 0.00/1 0.00/1 NOTE: L 38616 14899 0 TF was not given, B set to 1.000 for calc. not mentioned 58GPa high-pressure phase stable above 50 GPa. High-pressure structural phase transition in Mg Mg(bcc) d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 2.0881 100.0 100.0 1 1 0 2 43.295 21.647 0.2395 3.0091 1.4765 12.5 17.7 2 0 0 4 62.892 31.446 0.3386 4.2555 1.2056 19.3 33.4 2 1 1 6 79.426 39.713 0.4147 5.2118 1.0440 4.8 9.6 2 2 0 8 95.087 47.543 0.4789 6.0181 0.9338 6.1 13.6 3 1 0 10 111.150 55.575 0.5354 6.7285 0.8525 1.6 3.9 2 2 2 12 129.270 64.635 0.5865 7.3707 |
5楼2007-06-19 20:11:41
