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qinpei8901新虫 (正式写手)
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[求助]
求助微谱数据查询
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| 26.0,28.6,30.2,31.5,35.5,49.2,49.5,60.5,61.9,62.1,69.9,70.0,70.5,71.6,72.7,72.8,74.3,77.1,82.5,91.7,99.5,104.0,118.7,197.7,209.0 |
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peter002
木虫 (正式写手)
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【答案】应助回帖
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感谢参与，应助指数 +1
qinpei8901: 金币+20, ★有帮助 2012-10-13 11:23:51
感谢参与，应助指数 +1
qinpei8901: 金币+20, ★有帮助 2012-10-13 11:23:51
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????????????? ??????????? ????С??????????????????????????(,)??????磺 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 ?????? ?????? (???????????????趨) ?????? %(?????>=50%) ???????????鵽66????????(???????????ο?) 1 . crenulatanoside B C24H38O12 ?????:72% Journal of Asian Natural Products Research 2012 14 862-866 Two new compounds from the roots of Rhodiola crenulata Ya-Nan Yang, Fan Zhang, Zi-Ming Feng, Jian-Shuang Jiang & Pei-Cheng Zhang Structure 13C NMR??????? 2 . Grasshopper ketone 3-O-primveroside C24H38O12 ?????:64% Journal of Asian Natural Products Research 2012 14 503-507 Grasshopper ketone 3-O-primveroside from Sinocrassula indica Hai-Hui Xie and Masayuki Yoshikawa Structure 13C NMR??????? 3 . C-fr.16 ?????:60% Chemical & Pharmaceutical Bulletin 1989 37 54-56 The Structure of Nephritogenoside Tadahiro TAKEDA,Masahiko SAWAKI,Yukio OGIHARA and Seiichi SHIBATA Structure 13C NMR??????? 4 . Mono-4-O-octylcarbamate ?????:60% Tetrahedron Letters 2004 45 583-586 Preparation of amphiphilic sucrose carbamates by reaction with alkyl isocyanates in water-alcohol mixtures Delphine Christian, Juliette Fitremann, Alain Bouchu, Yves Queneau Structure 13C NMR??????? 5 . octyl ??-D-mannopyranosyl-(1??2)-??-D-mannopyranosyl-(1??5)-??-D-arabinofuranoside C25H46O15 ?????:60% Tetrahedron 1999 55 5965-5976 Synthesis of oligosaccharide fragments of mannosylated lipoarabinomannan from Mycobacterium tuberculosis Vinodhkumar Subramaniam, Todd L. Lowary Structure 13C NMR??????? 6 . DGDG ?????:56% Natural Product Research 2006 20 766-774 Diacylglycerolipids isolated from a thermophile cyanobacterium from the Euganean hot springs Gabriele Marcolongo; Francesca De Appolonia; Alfonso Venzo; Christopher P. Berrie; Tommaso Carofiglio; Cristina Ceschi Berrini Structure 13C NMR??????? 7 . 2-Oxyoethyl ??-D-garactopyranosyl-(1??4)-??-D-glucopyranoside-O-2-[2-[2-(biotynylaminoethoxy)-ethoxy]-ethoxy]-4-[3-(trifluoromethyl)-3H-diazirin-3-yl]-benzyloxime C37H55F3N6O16S ?????:56% Bioorganic & Medicinal Chemistry 2011 19 894-899 The effect of structural differences in the reducing terminus of sugars on the binding affinity of carbohydrates and proteins analyzed using photoaffinity labeling Isao Ohtsuka, Yutaka Sadakane, Mari Higuchi, Noriyasu Hada, Junko Hada, Nobuko Kakiuchi,Akiyo Sakushima Structure 13C NMR??????? 8 . (1R,2R,4S)-1,8-epoxy-p-methan-2-O-??-D-glucopyranosyl-(1??6)-??-D-glucopyranoside ?????:56% Pharmazie 2002 57 279-281 New isopimarane diterpene and new cineole type glucoside from Nepeta prattii Zhen-Fu Hou - Yong-Qiang Tu - Yu Li Structure 13C NMR??????? 9 . compound 2 ?????:56% Tetrahedron Letters 2004 45 857-862 Synthesis of potential bisubstrate inhibitors of Leishmania elongating ??-d-mannosyl phosphate transferase Vladimir S. Borodkin, Michael A.J. Ferguson, Andrei V. Nikolaev Structure 13C NMR??????? 10 . 8-Methoxycarbonyloctyl ??-D-galactopyranosyl-(1??4)-2-deoxy-2-(methyl-??-D-glucohexopyranosyluronamide)-??-D-glucopyranoside C29H51NO18 ?????:56% Bioorganic & Medicinal Chemistry 1998 6 1673-1682 Glycosyl-transferase catalyzed assemblage of sialyl-lewisx-saccharopeptides Gabi Baisch, Reinhold ??e??????` Structure 13C NMR??????? 11 . 8-Methoxycarbonyloctyl ??-D-galactopyranosyl-(1??4)-2-deoxy-2-(methyl-??-L-galactohexopyranosyluronamide)-??-D-glucopyranoside C29H51NO18 ?????:56% Bioorganic & Medicinal Chemistry 1998 6 1673-1682 Glycosyl-transferase catalyzed assemblage of sialyl-lewisx-saccharopeptides Gabi Baisch, Reinhold ??e??????` Structure 13C NMR??????? 12 . Methyl [??-D-glucopyranosyl-(1??4)-??-(1-thio-??5,5a carbaglucopyranosyl)-(1??4)-??-(??-D-glucopyranoside)] C20H34O14S ?????:56% Bioorganic & Medicinal Chemistry 2011 19 3812-3830 Syntheses of cellotriose and cellotetraose analogues as transition state mimics for mechanistic studies of cellulases Shogo Noguchi, Shintaro Takemoto, Shun-ichi Kidokoro, Kazunori Yamamoto, Masaru Hashimoto Structure 13C NMR??????? 13 . serrulatoside C27H42O14 ?????:53.8% Planta Medica 1984 50 417-420 Serruloside and Serrulatoside, two New Iridoid Glycosides from Penstemon serrulatus Peter Junior Structure 13C NMR??????? 14 . lobetyolinin C26H38O13 ?????:53.8% Phytochemistry 1992 31 1577-1579 A polyacetylene gentiobioside from hairy roots of Lobelia inflata Kanji Ishimaru, Shinji Sadoshima, Sumana Neera, Kiyotaka Koyama, Kunio Takahashi, Koichiro Shimomura Structure 13C NMR??????? 15 . Compound 1 C26H48O16 ?????:53.8% Bioorganic & Medicinal Chemistry Letters 1998 8 2051-2054 A synthetic acceptor substrate for Trypanosoma brucei UDP-Gal: GPI anchor side-chain ??-galactosyltransferases Jillian R. Brown, Terry K. Smith, Michael A. J. Ferguson, Robert A. Field Structure 13C NMR??????? 16 . compound 3 ?????:53.8% Tetrahedron Letters 2004 45 857-862 Synthesis of potential bisubstrate inhibitors of Leishmania elongating ??-d-mannosyl phosphate transferase Vladimir S. Borodkin, Michael A.J. Ferguson, Andrei V. Nikolaev Structure 13C NMR??????? 17 . physanoside B C25H40O12 ?????:52% Chemistry & Biodiversity 2008 Vol. 5 758 Two New Megastigmane Glycosides, Physanosides A and B, from Physalis alkekengi L. var. franchetii, and Their Effect on NO Release in Macrophages Li Qiu, Feng Zhao, Hongwei Liu, Lixia Chen, Zhihu Jiang, Hongxia Liu, Naili Wang, Xinsheng Yao, and Feng Qiu Structure 13C NMR??????? 18 . compound (ref) ?????:52% Phytochemistry 2002 60 409-414 3-Methylbutanoyl and 3-methylbut-2-enoyl disaccharides from green coffee beans (Coffea arabica) Bernhard Weckerle, Tam??s G??ti, G??bor T??th, Peter Schreier Structure 13C NMR??????? 19 . nonioside E C24H42O17 ?????:52% Planta Medica 2006 72 1322-1327 Noniosides E-H, New Trisaccharide Fatty Acid Esters from the Fruit of Morinda citrifolia (Noni) Petur W. Dalsgaard,Olivier Potterat, Fiona Dieterle,Thomas Paululat,Till K??hn,Matthias Hamburger Structure 13C NMR??????? 20 . Laportoside A C48H93NO10 ?????:52% Zeitschrift f??r Naturforschung B 2007 62b 1208-1212 Laportoside A and Laportomide A: A New Cerebroside and a New Ceramide from Leaves of Laportea ovalifolia Dagobert Tazoo, Karsten Krohn, Hidayat Hussain, Simeon F. Kouam, and Etienne Dongo Structure 13C NMR??????? 21 . Grasshopper ketone 3-O-primveroside C24H38O12 ?????:52% Journal of Asian Natural Products Research 2012 14 503-507 Grasshopper ketone 3-O-primveroside from Sinocrassula indica Hai-Hui Xie and Masayuki Yoshikawa Structure 13C NMR??????? 22 . compound 8 ?????:52% Phytochemistry 1989 28 2701-2704 Iridoids from Scrophularia ningpoensis Tetsuya Kajimoto,Mitsuharu Hidaka,Kayoko Shoyama,Toshihiro Nohara Structure 13C NMR??????? 23 . 2-(trimethylsilyl)ethyl 4,6-O-[(R)-1-methoxycarbonylethylidene]-??-D-galactopyranosyl-(1??4)-??-D-mannopyranosyl-(1??4)-??-D-galactopyranoside C26H48O18Si ?????:52% Indian Journal of Chemistry 2005 44B 137-140 Synthesis of (R)-4,6-O-pyruvated trisaccharide related to the repeating unit of the antigen from Shigella dysenteriae type 9 in the form of its 2-(trimethylsilyl)ethyl glycoside Roy,Samarpita; Sarkar,Sujit Kumar; Roy,Nirmolendu Structure 13C NMR??????? 24 . compound 5 ?????:52% Heterocycles 2007 71 1715-1721 Design and Synthesis of Novel Ring-Expanded Arbekacin Analogues Nobuto Minowa, Yukiko Hiraiwa, Yoshihisa Akiyama, Kazunori Maebashi, Takayuki Usui, and Daishiro Ikeda Structure 13C NMR??????? 25 . Compound 4 C48H95NO9 ?????:52% Bioorganic & Medicinal Chemistry Letters 2010 20 3475-3478 Synthesis and biological activity of ??-glucosyl C24:0 and C20:2 ceramides Peter J. Jervis, Natacha Veerapen, Gabriel Bricard, Liam R. Cox, Steven A. Porcelli, Gurdyal S. Besra Structure 13C NMR??????? 26 . compound 2 C29H58NO13P ?????:52% Tetrahedron Letters 2001 42 5305-5308 Synthesis of ??-d-Galp-(1??4)-??-d-Manp methanephosphonate, a substrate analogue for the elongating ??-d-mannosyl phosphate transferase in the Leishmania Vladimir S Borodkin, Michael A.J Ferguson, Andrei V Nikolaev Structure 13C NMR??????? 27 . 8-p-Methoxyphenoxyloctyl 2-acetamido-2-deoxy-3-O-(??-D-galactopyranosyl)-??-D-glucopyranoside ?????:52% Bioorganic & Medicinal Chemistry 1996 4 683-692 Towards oligosaccharide libraries: A study of the random galactosylation of unprotected N-acetylglucosamine Yili Ding, Jill Labbe, Osamu Kanie, Ole Hindsgaul Structure 13C NMR??????? 28 . 8-Methoxycarbonyloctyl 2-deoxy-2-(methyl-??-D-galacto-hexopyranosyluronamide)-??-D-glucopyranoside C23H41NO13 ?????:52% Bioorganic & Medicinal Chemistry 1998 6 1673-1682 Glycosyl-transferase catalyzed assemblage of sialyl-lewisx-saccharopeptides Gabi Baisch, Reinhold ??e??????` Structure 13C NMR??????? 29 . benzyl ??-D-glucopyranosyl-(1??3)-??-D-glucopyranosyl-(1??3)-??-D-glucopyranosyl-(1??3)-??-D-glucopyranosyl-(1??3)-??-D-mannopyranoside C37H58O26 ?????:52% Bioorganic & Medicinal Chemistry 2010 18 348-357 New oligo-??-(1, 3)-glucan derivatives as immunostimulating agents Karine Descroix, Vaclav V??tvi???, Isabelle Laurent, Frank Jamois, Jean-Claude Yvin, Vincent Ferri??res Structure 13C NMR??????? 30 . 3-(2-aminoethylthio)propyl 2-acetamido-2-deoxy-3-O-(??-L-fucopyranosyl)-4-O-(??-D-galactopyranosyl)-??-D-glucopyranoside C25H46N2O15S ?????:52% Bioorganic & Medicinal Chemistry 2010 18 7174-7185 Synthesis of a BSA-Lex glycoconjugate and recognition of Lex analogues by the anti-Lex monoclonal antibody SH1: The identification of a non-cross reactive analogue Jo-Wen Wang, Ari Asnani, France-Isabelle Auzanneau Structure 13C NMR??????? 31 . agelasphin-7a C46H91NO10 ?????:52% Tetrahedron 1994 50 2771-2784 Agelasphins, novel antitumor and immunostimulatory cerebrosides from the marine sponge Agelas mauritianus Takenori Natori, Masahiro Morita, Kohji Akimoto, Yasuhiko Koezuka Structure 13C NMR??????? 32 . agelasphin-9a C47H93NO10 ?????:52% Tetrahedron 1994 50 2771-2784 Agelasphins, novel antitumor and immunostimulatory cerebrosides from the marine sponge Agelas mauritianus Takenori Natori, Masahiro Morita, Kohji Akimoto, Yasuhiko Koezuka Structure 13C NMR??????? 33 . Fan(0)3-Lac C66H116O33S3Si1 ?????:52% Bioorganic & Medicinal Chemistry 2009 17 5465-5475 Syntheses and biological evaluations of carbosilane dendrimers uniformly functionalized with sialyl ??(2??3) lactose moieties as inhibitors for human influenza viruses Hiroyuki Oka, Tomotsune Onaga, Tetsuo Koyama, Chao-Tan Guo, Yasuo Suzuki, Yasuaki Esumi, Ken Hatano, Daiyo Terunuma, Koji Matsuoka Structure 13C NMR??????? 34 . Dumbbell(1)6-Lac C128H240O66S6Si3 ?????:52% Bioorganic & Medicinal Chemistry 2009 17 5465-5475 Syntheses and biological evaluations of carbosilane dendrimers uniformly functionalized with sialyl ??(2??3) lactose moieties as inhibitors for human influenza viruses Hiroyuki Oka, Tomotsune Onaga, Tetsuo Koyama, Chao-Tan Guo, Yasuo Suzuki, Yasuaki Esumi, Ken Hatano, Daiyo Terunuma, Koji Matsuoka Structure 13C NMR??????? 35 . amikacin ?????:52% The Journal of Antibiotics 1990 43 1611-1614 SYNTHESIS OF 6''-CHLORO-6''-DEOXYAMIKACIN AND SOME ITS ANALOGS EIJIRO UMEMURA, TSUTOMU TSUCHIYA, KOICHI TANAKA, SUMIO UMEZAWA Structure 13C NMR??????? 36 . actinoidin A ?????:52% The Journal of Antibiotics 1986 39 910-913 13C NMR STUDY OF ACTINOIDINS: CARBOHYDRATE MOIETIES AND THEIR GLYCOSIDIC LINKAGES GYULA BATTA, FERENC SZTARICSKAI, J????? CSANADI, ISTV? KOM????MI, REZS BOGN?? Structure 13C NMR??????? 37 . boholmycin hydrochloride C27H48N4O21 ?????:52% The Journal of Antibiotics 1988 41 855-861 BOHOLMYCIN, A NEW AMINOGLYCOSIDE ANTIBIOTIC I. PRODUCTION, ISOLATION AND PROPERTIES KYOICHIRO SAITOH, MITSUAKI TSUNAKAWA, KOJI TOMITA, TAKEO MIYAKI, MASATAKA KONISHI, HIROSHI KAWAGUCHI Structure 13C NMR??????? 38 . 1-N-[(S)-4-amino-2-hydroxybutyryl]-kanamycin C C22H43N5O13 ?????:52% The Journal of Antibiotics 1977 30 1150-1152 SYNTHESES AND PROPERTIES OF KANAMYCIN C DERIVATIVES ACTIVE AGAINST RESISTANT BACTERIA SHINICHI KONDO, TSUYOSHI MIYASAKA, KENZABURO YOSHIDA, KATSUHARU IINUMA, HAMAO UMEZAWA Structure 13C NMR??????? 39 . Sch 20287 C23H45N5O12 ?????:52% The Journal of Antibiotics 1978 31 681-687 THE SYNTHESES AND BIOLOGICAL PROPERTIES OF 1-N-(S-4-AMINO- 2-HYDROXYBUTYRYL)-GENTAMICIN B AND 1-N-(S-3-AMINO- 2-HYDROXYPROPIONYL)-GENTAMICIN B T. L. NAGABHUSHAN, A. B. COOPER, H. TSAI, P. J. L. DANIELS, G. H. MILLER Structure 13C NMR??????? 40 . (3R,4S,5R,6R)-6-(((2S,4S,6R)-6-((S)-1,2-dihydroxyethyl)-4-hydroxypiperidin-2-yl)methyl)tetrahydro-2H-pyran-2,3,4,5-tetraol C13H25NO8 ?????:52% Tetrahedron 2012 68 6674-6687 Highly stereoselective synthesis of imino-C-di- and trisaccharides as hydrolytically stable glycomimetics Eduardo Marca, Ignacio Delso, Tom??s Tejero, Pedro Merino Structure 13C NMR??????? 41 . (3S,4R,5S,6S)-6-(2-((2R,4S,6R)-6-((S)-1,2-dihydroxyethyl)-4-hydroxypiperidin-2-yl)ethyl)tetrahydro-2H-pyran-2,3,4,5-tetraol C14H27NO8 ?????:52% Tetrahedron 2012 68 6674-6687 Highly stereoselective synthesis of imino-C-di- and trisaccharides as hydrolytically stable glycomimetics Eduardo Marca, Ignacio Delso, Tom??s Tejero, Pedro Merino Structure 13C NMR??????? 42 . (3R,4S,5R,6R)-6-(2-((2S,4R,6S)-6-((S)-1,2-dihydroxyethyl)-4-hydroxypiperidin-2-yl)ethyl)tetrahydro-2H-pyran-2,3,4,5-tetraol C14H27NO8 ?????:52% Tetrahedron 2012 68 6674-6687 Highly stereoselective synthesis of imino-C-di- and trisaccharides as hydrolytically stable glycomimetics Eduardo Marca, Ignacio Delso, Tom??s Tejero, Pedro Merino Structure 13C NMR??????? 43 . serrulatoside ?????:51.8% Phytochemistry 2002 61 937-941 4'-Deoxy iridoid glycosides from Centranthus longiflorus Ay?a Kuru??z??m-Uz, Zuhal G??venalpb, L. ????r Demirezer,Isabelle Berg??re, Karsten Str????, Axel Zeeck Structure 13C NMR??????? 44 . 6-dehydrorehmannioside D dodecaacetate C51H64O32 ?????:51.8% Phytochemistry 1982 21 133-138 Iridoid glycosides of Rehmannia glutinosa Haruji Oshio, Hiroyuki Inouye Structure 13C NMR??????? 45 . Buteagibrenol Glycoside C27H48O11 ?????:51.8% Chemistry of Natural Compounds 2010 46 44-48 Phytochemical investigation of the seeds of Butea monosperma S. Alam, M. Ali, P. Alam and M. Shuaib Structure 13C NMR??????? 46 . 8-Methoxycarbonyloctyl ??-D-galactopyranosyl-(1??4)-2-deoxy-2-(methyl-??-L-galactohexopyranosyluronamide)-??-D-glucopyranoside C29H51NO18 ?????:51.8% Bioorganic & Medicinal Chemistry 1998 6 1673-1682 Glycosyl-transferase catalyzed assemblage of sialyl-lewisx-saccharopeptides Gabi Baisch, Reinhold ??e??????` Structure 13C NMR??????? 47 . Dictamnoside G C27H46O14 ?????:51.8% Bulletin of the Korean Chemical Society 2007 28 467-470 Three Sesquiterpene Glycosides from Elsholtzia bodinieri Hao-bin Hu*, Yu-feng Jian, Xu-dong Zheng, Hong Cao Structure 13C NMR??????? 48 . 11??-hydroxy-desglucohellebrin ?????:51.7% Planta Medica 1986 52 152-153 Bufadienolides from the Seeds of Helleborus odorus B. Kil??mer, M. Wicht Structure 13C NMR??????? 49 . nonioside F C28H51O17 ?????:50% Planta Medica 2006 72 1322-1327 Noniosides E-H, New Trisaccharide Fatty Acid Esters from the Fruit of Morinda citrifolia (Noni) Petur W. Dalsgaard,Olivier Potterat, Fiona Dieterle,Thomas Paululat,Till K??hn,Matthias Hamburger Structure 13C NMR??????? 50 . compound I C52H84O21 ?????:50% Chemical & Pharmaceutical Bulletin 1981 29 676-683 Studies on the Constituents of Zizyphi Fructus. III. Structures of Dammarane-type Saponins NOBUYUKI OKAMURA,TOSHIHIRO NOHARA,AKIRA YAGI and ITSUO NISHIOKA Structure 13C NMR??????? 51 . (1S,2R,4S)-bornan-2-yl 2,6-di-O-??-D-glucopyranosyl)??-D-glucopyranoside deca-acetate ?????:50% Phytochemistry 1993 34 1045-1048 Biotransformation of ()-borneol by cultured cells of Eucalyptus perriniana Yutaka Orihara, Tsutomu Furuya Structure 13C NMR??????? 52 . Ilicifolioside D C26H40O16 ?????:50% Magnetic Resonance in Chmesitry 2004 42 659-662 Complete assignments of 1H and 13C NMR data for 10 phenylethanoid glycosides Jun Wu, Jianshe Huang, Qiang Xiao, Si Zhang, Zhihui Xiao, Qingxin Li, Lijuan Long and Liangmin Huang Structure 13C NMR??????? 53 . 1-O-??-D-glucopyranosyl-(2S,3S,4R,8E)-2-[(2'R)-2'-hydroxy-tetracosanoyl]-8-octadecene-1,3,4-triol C48H93NO10 ?????:50% Chinese Journal of Natural Medicines 2009 7 115-118 Chemical Constituents from the Fruits of Ziziphus jujuba GUO Sheng; TANG Yu-Ping; DUAN Jin-Ao; SU Shu-Lan; QIAN Da-Wei Jiangsu Structure 13C NMR??????? 54 . compound 32 ?????:50% Tetrahedron Letters 2002 43 7821-7825 Synthesis of oligomeric phosphono analogues of Leishmania lipophosphoglycan fragments Vladimir S. Borodkin, Fiona C. Milne, Michael A.J. Ferguson, Andrei V. Nikolaev Structure 13C NMR??????? 55 . compound 33 ?????:50% Tetrahedron Letters 2002 43 7821-7825 Synthesis of oligomeric phosphono analogues of Leishmania lipophosphoglycan fragments Vladimir S. Borodkin, Fiona C. Milne, Michael A.J. Ferguson, Andrei V. Nikolaev Structure 13C NMR??????? 56 . 2-Acetamido-2-deoxy-3-O-(3-O-sulfo-??-D-galactopyranosyl)-4-O-(??-L-flucopyranosyl)-??-D-glucopyranosesodiumsalt C20H34NO18SNa ?????:50% Bioorganic & Medicinal Chemistry 1994 2 1143-1151 First synthesis of the 3?? - sulfated Lewisa pentasaccharide, the most potent human E-selectin ligand so far Andr?? Lubineau, Jo????? Le Gallic, R??my Lemoine Structure 13C NMR??????? |
2楼2012-10-12 08:48:30