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zhaojiantjpu新虫 (小有名气)
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[求助]
求助DSC等温结晶的问题，审稿人的意思是？另外大家等温结晶数据波动是多少？
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| DSC section - It is very difficult to cool rapidly as required for isothermal crystallization work and then to stop at the required isothermal test temperature. Overshoot is common. Only experiemtns with less than 0.3 over or undershoot are considered to be isothermal. The authors do not appear to address this question. An expanded scale figure of the temperature approach to isothermal test temperature showing the under or overshoot would address this question. |
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