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[交流] EPA标准方法免费下载(pdf格式)

EPA标准方法免费下载(pdf格式)

EPA Methods for Organic Chemical Analysis

EPA 500 Methods
The EPA 500 methods are designed to identify and quantify organic compounds in municipal drinking water. These methods are cited under the Safe Drinking Water Act (SDWA).


Method 502.2
Volatile Organic Compounds in Water by Purge and Trap Capillary Column Gas Chromatography with Photoionization and Electrolytic Conductivity Detectors in Series - Revision 2.1.

Method 504.1
1,2-Dibromoethane (EDB), 1,2-Dibromo-3-Chloropropane (DBCP), and 1,2,3- Trichloropropane (123TCP) in Water by Microextraction and Gas Chromatography - Revision 1.1.
Method 505
Analysis of Organohalide Pesticides and Commercial Polychlorinated Biphenyl (PCB) Products in Water by Microextraction and Gas Chromatography - Revision 2.1.
Method 506
Determination of Phthalate and Adipate Esters in Drinking Water by Liquid-Liquid Extraction or Liquid-Solid Extraction and Gas Chromatography with Photoionization Detection - Revision 1.1.
Method 507
Determination of Nitrogen- and Phosphorus-Containing Pesticides in Water by Gas Chromatography with a Nitrogen-Phosphorus Detector - Revision 2.1.
Method 508
Determination of Chlorinated Pesticides in Water by Gas Chromatography with an Electron Capture Detector - Revision 3.1.
Method 508.1
Determination of Chlorinated Pesticides, Herbicides, and Organohalides by Liquid-Solid Extraction and Electron Capture Gas Chromatography -Revision 2.0.
Method 508A
Screening for Polychlorinated Biphenyls by Perchlorination and Gas Chromatography - Revision 1.0.
Method 509
Determination of Ethylene Thiourea (ETU) in Water using Gas Chromatography with a Nirogen-Phosphorus Detector.
Method 515.1
Determination of Chlorinated Acids in Water by Gas Chromatography with an Electron Capture Detector - Revision 4.1.
Method 515.2
Determination of Chlorinated Acids in Water using Liquid-Solid Extraction and Gas Chromatography with an Electron Capture Detector - Revision 1.1.
Method 524.2
Measurement of Purgeable Organic Compounds in Water by Capillary Column Gas Chromatography/Mass Spectrometry - Revision 4.1.
Method 525.1
Determination of Organic Compounds in Drinking Water by Liquids-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry, Revision 2.2.
Method 525.2
Determination of Organic Compounds in Drinking Water by Liquid-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry -Revision 2.0.
Method 526
Determination of Selected Semi-Volatile Organic Compounds in Drinking Water by Solid Phase Extraction and Capillary Column Gas Chromatography/Mass Spectrometry.
Method 531.1
Measurement of N-Methylcarbamoyloximes and N-Methylcarbamates in Water by Direct Aqueous Injection HPLC with Post Column Derivatization -Revision 3.1.
Method 547
Determination of Glyphosate in Drinking Water by Direct-Aqueous-Injection b HPLC, Post-Column Derivatization, and Fluorescence Detection - July 1990.
Method 548
Determination of Endothall in Drinking Water by Aqueous Derivatization, Liquid-Solid Extraction, and Gas Chromatography with Electron Capture Detection.
Method 548.1
Determination of Endothall in Drinking Water by Ion Exchange Extraction, c Acidic Methanol Methylation and Gas Chromatography/Mass Spectrometry -Revision 1.0.
Method 549.1
Determination of Diquat and Paraquat in Drinking Water by Liquid-Solid c Extraction and HPLC with Ultraviolet Detection - Revision 1.0.
Method 550
Determination of Polycyclic Aromatic Hydrocarbons in Drinking Water By b Liquid-Liquid Extraction and HPLC with Coupled Ultraviolet and Fluorescence Detection.
Method 550.1
Determination of Polycyclic Aromatic Hydrocarbons in Drinking Water by Liquid-Solid Extraction and HPLC with Coupled Ultraviolet and Fluorescence Detection.
Method 551
Determination of Chlorination Disinfection Byproducts and Chlorinated Solvents in Drinking Water by Liquid-Liquid Extraction and Gas Chromatography with Electron Capture Detection.
Method 551.1
Determination of Chlorination Disinfection Byproducts, Chlorinated Solvents, and Halogenated Pesticides/Herbicides in Drinking Water by Liquid-Liquid Extraction and Gas Chromatography with Electron-Capture Detection -Revision 1.0.
Method 552
Determination of Haloacetic Acids in Drinking Water by Liquid-Liquid Extraction, Derivatization, and Gas Chromatography with Electron Capture Detection.
Method 552.1
Determination of Haloacetic Acids and Dalapon in Drinking Water by Ion Exchange Liquid-Solid Extraction and Gas Chromatography with an Electron Capture Detector - Revision 1.0.
Method 552.2
Determination of Haloacetic Acids and Dalapon in Drinking Water by Liquid-Liquid Extraction, Derivatization and Gas Chromatography with Electron Capture Detection - Revision 1.0.
Method 553
Determination of Benzidines and Nitrogen-Containing Pesticides in Water by Liquid-Liquid Extraction or Liquid-Solid Extraction and Reverse Phase High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry -Revision 1.1.
Method 554
Determination of Carbonyl Compounds in Drinking Water by Dinitrophenylhydrazine Derivatization and High Performance Liquid Chromatography - Revision 1.0.
Method 555
Determination of Chlorinated Acids in Water by High Performance Liquid Chromatography with a Photodiode Array Ultraviolet Detector - Revision 1.0.

EPA 600 Methods
The EPA 600 methods are designed for monitoring organic pollutants in industrial and municipal waste discharges. These methods are cited under the Clean Water Act (CWA).

Method 601
Purgeable Hydrocarbons
Method 602
Purgeable Aromatics
Method 603
Acrolein and Acrylonitrile
Method 604
Phenols
Method 605
Benzidines
Method 606

Phthalate Ester
Method 607
Nitrosamines
Method 608
Organochlorine Pesticides and PCBs
Method 609
Nitroaromatics and Isophorone
Method 610
Polynuclear Aromatic Hydrocarbons
Method 611
Haloethers
Method 612
Chlorinated Hydrocarbons
Method 613
2,3,7,8-Tetrachloro Dibenzo-p-Dioxin
Method 624
Purgeables
Method 625
Semivolatile Organic Compounds by Isotope Dilution GC/MS

EPA 1300 Methods

Method 1311
Toxicity Characteristic Leaching Procedure (TCLP)
Method 1312
Synthetic Precipitation Leaching Procedure

EPA 1600 Methods

Method 1614
Brominated diphenyl ethers in water, soil, sediment, and tissue by
HRGC/HRMS

EPA 8000 Methods
The EPA 8000 methods are designed for monitoring organic pollutants in ground water, as prescribed in the Resource Recovery and Conservation Act (RCRA).

Method 8000B
Determinative Chromatographic Separations
Method 8011
1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane by Microextraction and Gas Chromatography
Method 8015B
Nonhalogenated Organics Using GC/FID
Method 8021B
Aromatic and Halogenated Volatiles by Gas Chromatography Using Photoionization and/or Electrolytic Conductivity Detectors
Method 8031
Acrylonitrile by Gas Chromatography
Method 8032A

Acrylamide by Gas Chromatography
Method 8033

Acetonitrile by Gas Chromatography with Nitrogen-Phosphorus Detection
Method 8041
Phenols by Gas Chromatography
Method 8061A
Phthalate Esters by Gas Chromatography with Electron Capture Detection (GC/ECD)
Method 8070A
Nitrosamines by Gas Chromatography
Method 8081A
Organochlorine Pesticides by Gas Chromatography
Method 8082
Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Method 8091
Nitroaromatics and Cyclic Ketones by Gas Chromatography
Method 8100
Polynuclear Aromatic Hydrocarbons
Method 8111
Haloethers by Gas Chromatography
Method 8121
Chlorinated Hydrocarbons by Gas Chromatography: Capillary Column Technique
Method 8131
Aniline and Selected Derivatives by Gas Chromatography
Method 8141A
Organophosphorus Compounds by Gas Chromatography: Capillary Column Technique
Method 8151A
Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Derivatization
Method 8260B
Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method 8270C
Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method 8275A
Semivolatile Organic Compounds (PAHs and PCBs) in Soils/Sludges and Solid Wastes Using Thermal Extraction/Gas Chromatography/Mass Spectrometry (TE/GC/MS)
Method 8280A
The Analysis of Polychlorinated Dibenzo-p-Dioxins and Polychlorinated Dibenzofurans by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS)
Method 8290
Polychlorinated Dibenzodioxins (PCDDs) and Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS)
Method 8310
Polynuclear Aromatic Hydrocarbons
Method 8315A
Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC)
Method 8316
Acrylamide, Acrylonitrile and Acrolein by High Performance Liquid Chromatography (HPLC)

Method 8318
N-Methylcarbamates by High Performance Liquid Chromatography (HPLC)
Method 8321A
Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermospray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) Detection
Method 8325
Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry (HPLC/PB/MS)
Method 8330
Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC)
Method 8331
Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC)
Method 8332
Nitroglycerine by High Performance Liquid Chromatography
Method 8410
Gas Chromatography/Fourier Transform Infrared (GC/FT-IR) Spectrometry for Semivolatile Organics: Capillary Column
Method 8430
Analysis of Bis(2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection GC/FT-IR
Method 8440
Total Recoverable Petroleum Hydrocarbons by Infrared Spectrophotometry

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