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¸÷λ´óÏÀ£¬ÎÒµÄ Final R indices [I>2sigma(I)]     R1 = 0.0692, wR2 = 0.1144
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µ«±à¼­ËµÊý¾Ýare of no particularly good quality. The data resolution should be increased (redundancy is too small) and the data should be measured at lower T (e.g. 200 K). The R-values are rather poor

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2Â¥: Originally posted by pengw007 at 2012-08-30 16:37:07
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_diffrn_measured_fraction_theta_max    0.984
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_refine_diff_density_max    0.485
_refine_diff_density_min   -0.654
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2Â¥: Originally posted by pengw007 at 2012-08-30 16:37:07
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4Â¥2012-08-30 17:39:07
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5Â¥2012-08-30 17:59:50
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5Â¥: Originally posted by pengw007 at 2012-08-30 17:59:50
theta_full»¹ºÃ,´óÓÚ25¾ÍÐÐÁË.¿ÉÄÜÊÇÆäËüÎÊÌâ°É.±à¼­¿ÉÄÜŪ´íÁËÊý¾Ý°É.

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The reported single crystal data, especially that of structure 2, are of no particularly good quality. The data resolution should be increased (redundancy is too small) and the data should be measured at lower T (e.g. 200 K). The R-values are rather poor.
What kind of absorption correction was applied?
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6Â¥2012-08-30 18:02:51
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7Â¥2012-08-30 18:11:45
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7Â¥: Originally posted by pengw007 at 2012-08-30 18:11:45
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