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杨大松至尊木虫 (文坛精英)
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[求助]
求助微谱数据，谢谢
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碳谱数据如下： 18.0,21.0,21.4,24.3,27.2,28.9,29.6,31.7,32.4,33.1,34.3,35.7,39.3,42.3,50.4,51.7,68.4,68.6,71.2,77.8,78.3,85.1,122.1,167.9,206.4 辛苦各位了，谢谢 |
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二氯甲烷
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
杨大松: 金币+17, ★★★★★最佳答案 2012-07-07 20:49:19
感谢参与，应助指数 +1
杨大松: 金币+17, ★★★★★最佳答案 2012-07-07 20:49:19
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1 . β-ecdysterone 相似度:96% Natural Product Research and Development 2003 15 93-97 ECDYSTEROIDS FROM THE STEMS OF DIPLOCLISIA GLAUCESCENS HUANG Xiao chun GUO Yue wei ZHOU Wen liang ZUO Jian ping WANG Zheng tao Structure 13C NMR 碳谱模拟图 2 . β-ecdysone C27H44O7 相似度:92.5% Chinese Traditional and Herbal Drugs 2006 37 1304-1306 拔毒散化学成分的研究 李维峰;宋启示;项伟;杨淑敏 Structure 13C NMR 碳谱模拟图 3 . 20-hydroxyecdysone 相似度:92.3% Steroids 2002 67 127-135 Photochemical transformation of 20-hydroxyecdysone: production of monomeric and dimeric ecdysteroid analogues Juraj Harmatha, Milo? Bud??ínsky, Karel Voká? Structure 13C NMR 碳谱模拟图 4 . 20-hydroxyecdysone C27H44O7 相似度:92.3% Phytochemistry 1998 49 2109-2114 Ecdysteroid constituents of the mushroom Tapinella panuoides Karel Voká, Milo Budnsky, Juraj Harmathα, Jitka Kohoutová Structure 13C NMR 碳谱模拟图 5 . Ecdysterone 相似度:92.3% Journal of Natural Products 1995 Vol 58 264-268 4-Dehydroecdysterone, a New Ecdysteroid from the Zoanthid Parazoanthus sp. Philip A. Searle, Tadeusz F. Molinski Structure 13C NMR 碳谱模拟图 6 . 20-hydroxy-ecdysone 相似度:92.3% Phytochemistry 1994 37 707-711 Ecdysteroids from the roots of Leuzea carthamoides Jaroslav Pí?, Milo? Budě?ínsky?, Karel Voká?, Věra Laudová, Juraj Harmatha Structure 13C NMR 碳谱模拟图 7 . 20-hydroxyecdysone 相似度:92.3% Tetrahedron 1998 54 1657-1666 New ergostane type ecdysteroids from fungi. Ecdysteroid constituents of mushroom Paxillus atrotomentosus Karel Voká?, Milo? Budě?ínsky, Juraj Harmatha, Jaroslav Pí? Structure 13C NMR 碳谱模拟图 8 . 2'-hydroxyecdysone 相似度:88.8% Phytochemistry 2003 1179-1184 Ecdysteroids and other constituents from Sida spinosa L. Faten M.M. Darwish, Manfred G. Reinecke Structure 13C NMR 碳谱模拟图 9 . 20-Hydroxyecdysone 相似度:88.8% Steroids 2008 73 502-514 Additional minor ecdysteroid components of Leuzea carthamoides Milo? Budě?ínsky, Karel Voká?, Juraj Harmatha, Josef Cva?ka Structure 13C NMR 碳谱模拟图 10 . 20-hydroxyecdysone 相似度:88.8% China Journal of Chinese Materia Medica 2003 28 730-732 Studies on Chemical Constituents in Herb of Lamium maculatum L. var Kansuense DENG Yanru, HE Li, LI Weiqi, WANG Hanqing Structure 13C NMR 碳谱模拟图 11 . 20-hydroxyecdysone 相似度:88.8% Phytochemistry 1997 44 513-521 Ecdysteroid xylosides from Limnanthes douglasii Satyajit D. Sarker, Jean-Pierre Girault, René Lafont, Laurence N. Dinan Structure 13C NMR 碳谱模拟图 12 . 20-hydroxyecdysone 相似度:88.8% Korean Journal of Pharmacognosy 1999 30(3) 335-339 Isolatin and Quantitative Determination of 20-Hydroxyecdysone from Achyranthis Radix Hwang, Ji-Hyun; Lee, Seung-Ho; Park, Jeong-Hill; Kang, Shin-Jung; Chang, Seung-Yeup; Lee, Kyong-Soon; Son, Kun-Ho Structure 13C NMR 碳谱模拟图 13 . β-ecdysone C27H44O7 相似度:88.8% Journal of Natural Medicines 2010 64 114-116 New naphthoquinone from the root of Lygodium japonicum (Thunb.) Sw. Lijuan Chen, Guogang Zhang, Jie He, Jin Guan and Chunyuan Pan, et al. Structure 13C NMR 碳谱模拟图 14 . Ecdysterone 相似度:88.8% Chemistry of Natural Compounds 2010 46 173-175 A new alloside from Neocheiropteris palmatopedata Ye-Gao Chen, Jian-Hong Yang, Yan Zhang and Ying Liu Structure 13C NMR 碳谱模拟图 15 . β-ecdysterone C27H44O7 相似度:88.8% Journal of China Pharmaceutical University 2006 37 487-490 Chemical constituents from Asparagus filicinus WU Jia-jun; WANG Hao; YE Wen-cai; ZUO Xiao-feng; ZHAO Shou-xun Structure 13C NMR 碳谱模拟图 16 . cholest-7-en-2β,3β,14α,20β,22α,25-hexahydroxy-6-one C27H44O7 相似度:88.8% Acta Scientiarum Naturalium Universitatis Sunyatseni 2003 42(5) 51-53 Polyhydroxylated Sterols from the Soft Coral Sinularia depressa ZHANG Guang-wen, MA Xiang-quan, SU Jing-yu, ZENG Long-mei Structure 13C NMR 碳谱模拟图 17 . 20-hydroxyecdysone 相似度:85.1% Food Chemistry 2005 92 125-132 Nutritional and antinutritional composition of Kancolla seeds: an interesting and underexploited andine food plant Irene Dini, Gian Carlo Tenore, Antonio Dini Structure 13C NMR 碳谱模拟图 18 . Sileneoside D 相似度:81.4% Chemistry of Natural Compounds 1998 34 602-604 PItYTOECDYSTEROIDS OF PLANTS OF THE Silene GENUS. XIX. THE STRUCTURE OF SILENEOSIDE G Z. T. Sadykov and Z. Saatov Structure 13C NMR 碳谱模拟图 19 . 20β-hydroxy-ecdysone 相似度:81.4% Natural Product Research and Development 2005 17 125-127 Chemical Constituents of Tinospora craveniana LI Hong-bo; HU Jun; CHEN Jian-chao; QIU Ming-hua Structure 13C NMR 碳谱模拟图 20 . makisterone C 相似度:81.4% Natural Product Research and Development 2003 15 93-97 ECDYSTEROIDS FROM THE STEMS OF DIPLOCLISIA GLAUCESCENS HUANG Xiao chun GUO Yue wei ZHOU Wen liang ZUO Jian ping WANG Zheng tao Structure 13C NMR 碳谱模拟图 21 . ponasterone A C27H44O6 相似度:80.7% Phytochemistry 1998 49 2109-2114 Ecdysteroid constituents of the mushroom Tapinella panuoides Karel Voká, Milo Budnsky, Juraj Harmathα, Jitka Kohoutová Structure 13C NMR 碳谱模拟图 22 . 20-hydroxyecdysone 相似度:80.7% Phytochemistry 1997 46 103-105 24(241)[Z]-dehydroamarasterone B, a phytoecdysteroid from seeds of Leuzea carthamoides U. A. Baltayev, L. Dinan, J. -P. Girault, R. Lafont Structure 13C NMR 碳谱模拟图 23 . ponasterone A 相似度:80.7% Russian Journal of Organic Chemistry 2002 38 525-529 Ozonolysis of Alkenes and Study of Reactions of Polyfunctional Compounds: LXVI.2* Ozonolysis and Hydrogenation of Diacetonides of 24,25- and 25,26-Anhydro-20-hydroxyecdysones. Synthesis of Ponasterone A V. N. Odinokov, R. G. Savchenko, S. R. Nazmeeva, I. V. Galyautdinov and L. M. Khalilov Structure 13C NMR 碳谱模拟图 24 . 20-Hydroxyecdysone 2-acetate C29H46O8 相似度:79.3% Steroids 2008 73 502-514 Additional minor ecdysteroid components of Leuzea carthamoides Milo? Budě?ínsky, Karel Voká?, Juraj Harmatha, Josef Cva?ka Structure 13C NMR 碳谱模拟图 25 . 24-epi-Makisterone A 相似度:78.5% Steroids 2008 73 502-514 Additional minor ecdysteroid components of Leuzea carthamoides Milo? Budě?ínsky, Karel Voká?, Juraj Harmatha, Josef Cva?ka Structure 13C NMR 碳谱模拟图 26 . makisterone A 相似度:78.5% Korean Journal of Pharmacognosy 1998 29(4) 318-322 Studies on the Constituents from the Herbs of Ajuga multiflora (II) Yu, Young-Jun; Do, Jae-Chul; Kwon, Soon-Youl; Son, Kun-Ho Structure 13C NMR 碳谱模拟图 27 . ponasterone A 相似度:77.7% Helvetica Chimica Acta 2008 Vol. 91 1640 Additional Minor Phytoecdysteroids of Serratula wolffii András Simon, Erika Liktor-Busa, Gábor To′ th, Zoltán Kele, Judit Groska, and Mária Báthorió Structure 13C NMR 碳谱模拟图 28 . 20-Hydroxyecdysone (6-chloronicotinate) 相似度:77.7% Chemistry of Natural Compounds 2009 45 385-388 SYNTHESIS OF 20-HYDROXYECDYSONE 6-CHLORONICOTINATES I. D. Bobaev, N. V. Kovganko, Yu. G. Chernov, Z. R. Utaeva,S. N. Sokolov, Zh. N. Kashkan, and N. Sh. Ramazanov Structure 13C NMR 碳谱模拟图 29 . ecdysterone 相似度:77.7% Chemistry of Natural Compounds 1990 26 301-303 PHYTOECDYSTEROIDS OF PLANTS OF THE GENUS Silene.XVII. ECDYSTERONE 22,25-DI-O-BENZOATE FROM Silene scabrifolia A. Saatov, N. D. Abdullaev,M. B. Gorovits, and N. K. Abubakirov Structure 13C NMR 碳谱模拟图 30 . 2-deoxy-20-hydroxyecdysone 相似度:77.7% Helvetica Chimica Acta 2009 92 753-761 Ecdysteroids from Silene viridiflora András Simon, Noémi Tóth, Gábor Tóth, Zoltán Kele, Judit Groska, Mária Báthori Structure 13C NMR 碳谱模拟图 31 . ecdysterone 相似度:77.7% Acta Botanica Sinica 1996 38 399-405 Studieson the Chemical Constituents of the Leaves of Pseudotaxus chienii (Cheng)Cheng Zhang Jun-zeng, Fang Qi-cheng and Liang Xiao-tian Structure 13C NMR 碳谱模拟图 32 . ecdysterone C27H44O7 相似度:77.7% Acta Pharmaceutica Sinica 1991 26 442-446 PHYTOECDYSTEROIDS OF RHAPONTICUM UNIFLORUM ROOT DA Guo; ZC Lou; CY Gao; L Qiao and JR Peng Structure 13C NMR 碳谱模拟图 33 . ponasterone A 相似度:77.7% China Journal of Chinese Materia Medica 2007 32 1421-1425 Non-taxoid chemical constituents from leaves of Taxus mairei ZHANG Manli, HUO Changhong, DONG Mei, LIANG Chunhui, GU Yucheng, SHI Qingwen Structure 13C NMR 碳谱模拟图 34 . ecdysterone C27H44O7 相似度:77.7% Phytochemistry 1987 26 2505-2507 Ecdysteroids from Pfaffia iresinoides and reassignment of some 13CNMR chemical shifts Nobushige Nishimoto,Yoshinori Shiobara,Masumi Fujino,Shun-Suke Inoue,Tsunematsu Takemoto,Fernando De Oliveira,Gokithi Akisue,Maria Kubota Akisue,Goro Hashimoto,Osamu Tanaka,Ryoji Kasai,Hiromichi Matsuura Structure 13C NMR 碳谱模拟图 35 . ecdysterone 相似度:77.7% Phytochemistry 1988 27 1665-1668 Three ecdysteroid glycosides from Pfaffia iresinoides Nobushige Nishimoto,Yoshinori Shiobara,Shun-suke Inoue,Masumi Fujino,Tsunematsu Takemoto,Cheow Lin Yeoh,Fernando de Oliveira,Gokithi Akisue,Maria Kubota Akisue,Goro Hashimoto Structure 13C NMR 碳谱模拟图 36 . ecdysterone 相似度:77.7% Phytochemistry 1983 22 2320-2321 Abutasterone, an ecdysone from abuta velutina Maria Lucia B. Pinheiro, W. Wolter Filho, Arnaldo I. Da Rocha, Barry Porter, Ernest Wenkertt Structure 13C NMR 碳谱模拟图 37 . ponasterone A 相似度:77.7% Chinese Journal of Medicinal Chemistry 2006 16 46-48 Isolation and identification of the chemical constituents from Mangrove plant Acrostichum a ureurm MEI Wen-li, ZENG Yan-bo, DING Zhong-tao, DAI Hao-fu Structure 13C NMR 碳谱模拟图 38 . 20β-hydroxy-ecdysone-2-O-β-D-glucopyranoside 相似度:77.7% Natural Product Research and Development 2005 17 125-127 Chemical Constituents of Tinospora craveniana LI Hong-bo; HU Jun; CHEN Jian-chao; QIU Ming-hua Structure 13C NMR 碳谱模拟图 39 . 20-hydroxylecdysono-20,22-phosphonic acid C27H43O9P 相似度:77.7% Journal of Asian Natural Products Research 2011 13 297-303 Synthesis of a novel phosphate analog of 20-hydroxylecdysone with potent hypoglycemic activity Dan Zhang; Min Zhang; Bao Ding; Xiao-Lin Wang; Zong-Yin Qiu; Yong Qin Structure 13C NMR 碳谱模拟图 40 . sodium 20-hydroxylecdysono-20,22-phosphate C27H42NaO9P 相似度:77.7% Journal of Asian Natural Products Research 2011 13 297-303 Synthesis of a novel phosphate analog of 20-hydroxylecdysone with potent hypoglycemic activity Dan Zhang; Min Zhang; Bao Ding; Xiao-Lin Wang; Zong-Yin Qiu; Yong Qin Structure 13C NMR 碳谱模拟图 41 . (20R,22R)-2β,3β,14,20,22,25-Hexahydroxy-53-cholest-7-en-6-one ecdysterone C27H44O7 相似度:77.7% Organic Magnetic Resonance 1977 9 439-464 13C N.m.r. Spectra of steroids—A Survey and Commentary J.W.Blunt and J.B.Stothers Structure 13C NMR 碳谱模拟图 42 . malacosterone C27H44O8 相似度:76.9% Phytochemistry 1998 49 2109-2114 Ecdysteroid constituents of the mushroom Tapinella panuoides Karel Voká, Milo Budnsky, Juraj Harmathα, Jitka Kohoutová Structure 13C NMR 碳谱模拟图 43 . turkesterone C27H44O8 相似度:76.9% Phytochemistry 1998 49 2109-2114 Ecdysteroid constituents of the mushroom Tapinella panuoides Karel Voká, Milo Budnsky, Juraj Harmathα, Jitka Kohoutová Structure 13C NMR 碳谱模拟图 44 . 20-hydroxyecdysone C27H44O7 相似度:76% Chemical & Pharmaceutical Bulletin 1990 38 1927-1930 The Constituents of Cistanche tubulosa (SCHRENK) HOOK. f. II. : Isolation and Structures of a New Phenylethanoid Glycoside and a New Neolignan Glycoside Fumio YOSHIZAWA,Takeshi DEYAMA,Nobuo TAKIZAWA,Khan USMANGHANI and Mansoor AHMAD Structure 13C NMR 碳谱模拟图 45 . β-蜕皮激素 C27H44O7 相似度:76% Chinese Traditional and Herbal Drugs 2002 33 598-599 蒸茧液的化学成分研究 沈云修,孙祥洪,马丽英,赵永德,赵铭山 Structure 13C NMR 碳谱模拟图 46 . 20-hydroxyecdysone 20,22-monoacetonide 相似度:75.8% Phytochemistry 1994 37 707-711 Ecdysteroids from the roots of Leuzea carthamoides Jaroslav Pí?, Milo? Budě?ínsky?, Karel Voká?, Věra Laudová, Juraj Harmatha Structure 13C NMR 碳谱模拟图 47 . makisterone A 相似度:75% Chemistry & Biodiversity 2008 Vol. 5 707 Ecdysteroids from Vitex Species: Distribution and Compilation of Their 36C-NMR Spectral Data José G. Sena Filho, Jennifer Duringer, Gabriela L. A. Maia, Josean F. Tavares, Haroudo S. Xavier, Marcelo Sobral da Silva, Em.dio V. L. da-Cunha, and José M. Barbosa-Filho Structure 13C NMR 碳谱模拟图 48 . makisterone A 相似度:75% Planta Medica 1985 51 40-42 Phytoecdysteroids of Diploclisia glaucescens Seed R. W. Miller, J. C1ardy, J. Kozlowski, K. L. Mikolajczak, R. D. Plattner, R. G. Powell, C. R. Smith, D. Weisleder and Zheng Qi-Tai Structure 13C NMR 碳谱模拟图 49 . Carthamoleusterone C28H44O8 相似度:75% Steroids 2008 73 502-514 Additional minor ecdysteroid components of Leuzea carthamoides Milo? Budě?ínsky, Karel Voká?, Juraj Harmatha, Josef Cva?ka Structure 13C NMR 碳谱模拟图 50 . 20-hydroxyecdysone 相似度:74.0% Chemistry & Biodiversity 2008 Vol. 5 707 Ecdysteroids from Vitex Species: Distribution and Compilation of Their 13C-NMR Spectral Data José G. Sena Filho, Jennifer Duringer, Gabriela L. A. Maia, Josean F. Tavares, Haroudo S. Xavier, Marcelo Sobral da Silva, Em.dio V. L. da-Cunha, and José M. Barbosa-Filho Structure 13C NMR 碳谱模拟图 51 . 20-hydroxyecdysone 相似度:74.0% Journal of Natural Products 2002 65 1194-1197 Ecdysteroids from a Zoanthus sp. Apichart Suksamrarn,Aroon Jankam, Bongkoch Tarnchompoo, and Sumaitt Putchakarn Structure 13C NMR 碳谱模拟图 52 . 20-hydroxyecdysone 相似度:74.0% Journal of Natural Products 2002 65 1690-1692 Ecdysteroids of Vitex scabra Stem Bark Apichart Suksamrarn, Saowanee Kumpun, and Boon-ek Yingyongnarongkul Structure 13C NMR 碳谱模拟图 |
2楼2012-07-07 20:36:35
杨大松
至尊木虫 (文坛精英)
- 应助: 243 (大学生)
- 金币: 23878.3
- 散金: 3
- 红花: 46
- 帖子: 10466
- 在线: 831.8小时
- 虫号: 1190374
- 注册: 2011-01-15
- 专业: 化学生物学与生物有机化学
3楼2012-07-07 20:49:33