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[求助]
微谱数据，求结构，多糖
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| 40.54, 60.07, 60.54, 60.69, 61.18, 61.29, 62.37, 63.02, 63.34, 63.82, 64.07, 67.48, 69.12, 69.16, 69.55, 69.58, 70.99, 71.03, 71.11, 71.38, 71.50, 71.84, 72.12, 72.34, 72.47, 72.68, 73.28, 73.61, 73.80, 73.95, 74.07, 74.33, 75.66, 75.87, 76.39, 80.04, 81.27, 92.02, 92.13 , 95.82, 98.03, 103.60, 162.70 , 171.12, 178.53, 179.35,179.93 |
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【答案】应助回帖
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感谢参与，应助指数 +1
nyl8791: 金币+20, ★★★★★最佳答案, 谢谢 2012-07-06 21:05:55
感谢参与，应助指数 +1
nyl8791: 金币+20, ★★★★★最佳答案, 谢谢 2012-07-06 21:05:55
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查询模式：模糊查询 碳谱数据输入： 按从小到大顺序输入，数字间用英文半角逗号(,)分隔例如： 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 40.54, 60.07, 60.54, 60.69, 61.18, 61.29, 62.37, 63.02, 63.34, 63.82, 64.07, 67.48, 69.12, 69.16, 69.55, 69.58, 70.99, 71.03, 71.11, 71.38, 71.50, 71.84, 72.12, 72.34, 72.47, 72.68, 73.28, 73.61, 73.80, 73.95, 74.07, 74.33, 75.66, 75.87, 76.39, 80.04, 81.27, 92.02, 92.13 , 95.82, 98.03, 103.60, 162.70 , 171.12, 178.53, 179.35,179.93 溶剂选项： 全部 CDCl3 CD3CD2OD CD2Cl2 C5D5N C3D7NO CD3SOCD3 C4D8O (CH3)4Si C4D8O2 CD3COOD C4D8O2 H2O D2O CF3COOD CD3OD ND3 CD3COCD3 C6D6 CD3CN 查询空值 匹配容差： (数字格式，可自行设定) 相似度： %(相似度>=50%) 查询结果：共查到26个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . compound 1b 相似度:61.7% Chemical & Pharmaceutical Bulletin 1998 46 1891-1900 Studies on the Constituents of Clematis Species. VII. Triterpenoid Saponins from the Roots of Clematis terniflora DC. var. robusta TAMURA Yukio KAWATA,Haruhisa KIZU and Tsuyoshi TOMIMORI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . compound 9a 相似度:59.5% Chemical & Pharmaceutical Bulletin 1998 46 1891-1900 Studies on the Constituents of Clematis Species. VII. Triterpenoid Saponins from the Roots of Clematis terniflora DC. var. robusta TAMURA Yukio KAWATA,Haruhisa KIZU and Tsuyoshi TOMIMORI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . Compound 2 相似度:59.5% Magnetic Resonance in Chmesitry 2001 39 288-293 Assignment of the 1H and 13C NMR spectra, sequence and conformation of the synthetic pentasaccharide SanOrg34006 and its precursors Judica Bootsma, Gerard Wagenaars, Erik Dreef, Floris Hout and Edwin Kellenbach Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . myricetin 3-O-β-D-galactoside-3'-O-α-D-glucoside C27H30O18 相似度:57.4% Natural Product Research 2010 24 920-925 Flavonol glycosides with α-D-aldohexoses from Rhododendron irroratum Ming Hua Yang; Jian Guang Luo; Xue Feng Huang; Ling Yi Kong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . 3-O-[β-D-galactopyranosyl-(1→2)-β-D-glucuronopyranosyl]quillaic acid-28-O-[α-L-arabinopyranosyl-(1→2)-α-L-arabinopyranosyl-(1→3)-β-D-xylopyranosyl-(1→4)-α-L-rhamnopyranosyl-(1→2)]-[6-O-acetyl-β-D-glucopyranosyl-(1→3)]-4-O-acetyl-β-D-fucopyranoside C78H118O44Na 相似度:57.1% Journal of Natural Products 2002 65 1568-1572 New Acylated Triterpene Saponins from Silene fortunei that Modulate Lymphocyte Proliferation Ghezala Gaidi, Tomofumi Miyamoto, Véronique Laurens, and Marie-Aleth Lacaille-Dubois Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . 3-O-(β-D-glucopyranosyl-(1 →3)-β-Dglucopyranosyl)-28-O-(α-L-rhamnopyranosyl-(1 →3)-β-Dxylopyranosyl-(1 →4)-α-L-rhamnopyranosyl-(1 →2)-α-Larabinopyranosyl)-16α-hydroxyprotobassic acid C64H104O33 相似度:55.1% Phytochemistry 2006 67 1793-1799 Saponins from the seeds of Mimusops laurifolia Jacqueline Eskander, Catherine Lavaud, Isabelle Pouny, Hesham S.M. Soliman,S.M. Abdel-Khalik, I.I. Mahmoud Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . compound 3 相似度:54.1% Chemical & Pharmaceutical Bulletin 2006 54(3) 287-291 Biologically Active Glycosides from Asteroidea, 42.1) Isolation and Structure of a New Biologically Active Ganglioside Molecular Species from the Starfish Asterina pectinifera Ryuichi HIGUCHI,Shinichi INOUE,Kouji INAGAKI,Maki SAKAI,Tomofumi MIYAMOTO,Tetsuya KOMORI,Masanori INAGAKI,and Ryuichi ISOBE Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 3-O-(β-D-apiofuranosyl(1 →3)-β-D-glucuronopyranosyl)-28-O-(α-L-rhamnopyranosyl-(1 →3)-β-D-xylopyranosyl-(1→4)-α-L-rhamnopyranosyl-(1→2)-α-L-arabinopyranosyl)-16α-hydroxyprotobassic acid C63H100O33 相似度:54.1% Phytochemistry 2006 67 1793-1799 Saponins from the seeds of Mimusops laurifolia Jacqueline Eskander, Catherine Lavaud, Isabelle Pouny, Hesham S.M. Soliman,S.M. Abdel-Khalik, I.I. Mahmoud Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . epibreynin G C46H66O27S 相似度:53.1% Journal of Natural Products 2007 70 824-829 Sulfur-Containing Spiroketal Glycosides from Breynia fruticosa Dahai Meng, Wenliang Chen, and Weimin Zhao Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . eucalbanin B 相似度:53.1% Chemical & Pharmaceutical Bulletin 1992 40 1750-1754 Eucalbanins A, B and C, Monomeric and Dimeric Hydrolyzable Tannins from Eucalyptus alba REINW. Takashi YOSHIDA,Tetsuhiro MARUYAMA,Aya NITTA and Takuo OKUDA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . compound XII C71H116O36 相似度:53.1% Acta Pharmaceutica Sinica 1993 28 358-363 STRUCTURE DETERMINATION OF SAPONIN Ⅺ, Ⅻ AND ⅩⅢ FROM DIPSACUS ASPER WALL YW Zhang and Z Xue Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . Raddeanoside R21 (sugar moieties) C83H136O44 相似度:53.1% Phytochemistry Letters 2012 5 258-261 Triterpenoid saponins from Anemone raddeana Fu Li, Cui-Rong Sun, Bin Chen, Li-Sheng Ding, Ming-Kui Wang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . methyl 2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1→3)-2-O-acetyl-4,6-O-benzylidene-α-D-mannopyranosyl-(1→3)-6-O-benzyl-4-O-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-α-D-mannopyranosyl-(1→4)-[2-(trimethylsilyl)ethyl 2,3-di-O-benzyl-β-D-glucopyranosid]uronate C108H124O26Si 相似度:53.1% Indian Journal of Chemistry 2005 44B 1058-1063 Revised synthesis of the pentasaccharide related to the repeating unit of the O-antigen from Shigella dysenteriae type-4 in the form of its methyl ester 2-(trimethylsilyl)ethyl glycoside Sarkar,Sujit Kumar; Mukhopadhyay,Balaram; Roy,Nirmolendu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . saponin C 相似度:53.1% Archives of Pharmacal Research 1991 14 124-129 Triterpenoidal saponins from the leaves of Kalopanax pictum var. chinense Min-Won Lee and Dug-Ryong Hahn Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . compound 9 相似度:53.1% Tetrahedron 1997 53 9007-9022 Isolation and structural characterization of new glyclipid ester type dimers from the resin of Ipomoea tricolor (Convolvulaceae) Moustapha Bah, Rogelio Pereda-Miranda Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . compound 10 相似度:53.1% Tetrahedron 1997 53 9007-9022 Isolation and structural characterization of new glyclipid ester type dimers from the resin of Ipomoea tricolor (Convolvulaceae) Moustapha Bah, Rogelio Pereda-Miranda Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . compound X 相似度:52.9% Acta Pharmaceutica Sinica 1993 28 358-363 STRUCTURE DETERMINATION OF SAPONIN Ⅺ, Ⅻ AND ⅩⅢ FROM DIPSACUS ASPER WALL YW Zhang and Z Xue Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . 28-(O-β-D-galactopyranosyl-(1→4)-O-[β-D-glucopyranosyl-(1→3)]-O-β-D-xylopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1→2)-{4-O-[(E)-4-methoxycinnamoyl]}-β-D-fucopyranosyl) ester C75H112O36 相似度:51.0% Helvetica Chimica Acta 2003 Vol. 86 2404 New Acylated Triterpene Saponins from Polygala arenaria Anne-Claire Mitaine-Offer, Tomofumi Miyamoto, Véronique Laurens, Clément Delaude, and Marie-Aleth Lacaille-Dubois Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 28-(O-β-D-galactopyranosyl-(1→4)-O-[β-D-glucopyranosyl-(1→3)]-O-β-D-xylopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1→2)-{4-O-[(Z)-4-methoxycinnamoyl]}-β-D-fucopyranosyl) ester C75H112O36 相似度:51.0% Helvetica Chimica Acta 2003 Vol. 86 2404 New Acylated Triterpene Saponins from Polygala arenaria Anne-Claire Mitaine-Offer, Tomofumi Miyamoto, Véronique Laurens, Clément Delaude, and Marie-Aleth Lacaille-Dubois Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . 3-O-(β-D-glucopyranosyl)presenegenin 28-(O-β-D-galactopyranosyl-(1→4)-O-[β-D-glucopyranosyl-(1→3)]-O-β-D-xylopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1→2)-{4-O-[(E)-3,4-dimethoxycinnamoyl]}-β-D-fucopyranosyl) ester C76H114O37 相似度:51.0% Helvetica Chimica Acta 2003 Vol. 86 2404 New Acylated Triterpene Saponins from Polygala arenaria Anne-Claire Mitaine-Offer, Tomofumi Miyamoto, Véronique Laurens, Clément Delaude, and Marie-Aleth Lacaille-Dubois Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . 3-O-(β-D-glucopyranosyl)presenegenin 28-(O-β-D-galactopyranosyl-(1→4)-O-[β-D-glucopyranosyl-(1 3)]-O-β-D-xylopyranosyl-(1→4)-O-α-L-rhamnopyranosyl-(1 2)-{4-O-[(Z)-3,4-dimethoxycinnamoyl]}-β-D-fucopyranosyl) ester C76H114O37 相似度:51.0% Helvetica Chimica Acta 2003 Vol. 86 2404 New Acylated Triterpene Saponins from Polygala arenaria Anne-Claire Mitaine-Offer, Tomofumi Miyamoto, Véronique Laurens, Clément Delaude, and Marie-Aleth Lacaille-Dubois Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . cordylasin A C45H61O28 相似度:51.0% Phytochemistry 2008 69 2329-2335 Flavonol pentaglycosides of Cordyla (Leguminosae: Papilionoideae: Swartzieae): Distribution and taxonomic implications Nigel C. Veitch ,Geoffrey C. Kite,Gwilym P. Lewis Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . cordylasin B C45H61O27 相似度:51.0% Phytochemistry 2008 69 2329-2335 Flavonol pentaglycosides of Cordyla (Leguminosae: Papilionoideae: Swartzieae): Distribution and taxonomic implications Nigel C. Veitch ,Geoffrey C. Kite,Gwilym P. Lewis Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . tenuifoliosde F C68H86O39 相似度:51.0% Chemical & Pharmaceutical Bulletin 1991 39 3055-3056 Marine Terpenes and Terpenoids. XIII. Isolation of a New Dihydrofuranocembranoid, Sarcophytonin E, from the Sarcophyton sp. Soft Coral of Okinawa Masaru KOBAYASHI and Takumi HIRASE Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . quamoclinic acids E C56H98O34 相似度:51.0% Chemical & Pharmaceutical Bulletin 2010 58 666-672 Components of Ether-Insoluble Resin Glycoside (Convolvulin) from Seeds of Quamoclit pennata Masateru Ono, Yoko Takagi-Taki, Fumiko Honda-Yamada, Naoki Noda and Kazumoto Miyahara Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . mycaloside F C52H84O24 相似度:50% Journal of Natural Products 2003 66 1082-1088 Mycalosides B-I, Eight New Spermostatic Steroid Oligoglycosides from the Sponge Mycale laxissima Alexandr S. Antonov, Shamil Sh. Afiyatullov, Anatoly I. Kalinovsky, Ludmila P. Ponomarenko,Pavel S. Dmitrenok, Dmitry L. Aminin, Irina G. Agafonova, and Valentin A. Stonik Structure 13C NMR 碳谱模拟图 |
2楼2012-07-06 10:12:51