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杨大松至尊木虫 (文坛精英)
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[求助]
求助微谱数据，谢谢
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碳谱数据如下： 17.5,24.9,28.4,29.0,32.1,35.0,49.4,49.9,79.2,85.3,178.8 辛苦各位了，谢谢。 |
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chzhbin
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
杨大松: 金币+10, ★★★★★最佳答案 2012-06-30 08:08:36
leecius: 金币+1, 谢谢参与！ 2012-06-30 09:10:05
感谢参与，应助指数 +1
杨大松: 金币+10, ★★★★★最佳答案 2012-06-30 08:08:36
leecius: 金币+1, 谢谢参与！ 2012-06-30 09:10:05
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1 . 4-Nonyl-3-methyloxetan-2-one 相似度:58.3% Bioorganic & Medicinal Chemistry 1998 6 1255-1272 Synthesis and inhibitory action on HMG-CoA synthase of racemic and optically active oxetan-2-ones (β-Lactones) Daniel Romo, Paul H.M. Harrison, Stephen I. Jenkins, R.William Riddoch, Kaapjoo Park, Hong Woon Yang, Cunxiang Zhao, Gerard D. Wright Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . 4-Octyl-3-methyloxetan-2-one 相似度:58.3% Bioorganic & Medicinal Chemistry 1998 6 1255-1272 Synthesis and inhibitory action on HMG-CoA synthase of racemic and optically active oxetan-2-ones (β-Lactones) Daniel Romo, Paul H.M. Harrison, Stephen I. Jenkins, R.William Riddoch, Kaapjoo Park, Hong Woon Yang, Cunxiang Zhao, Gerard D. Wright Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 4-Tridecyl-3-methyloxetan-2-one 相似度:58.3% Bioorganic & Medicinal Chemistry 1998 6 1255-1272 Synthesis and inhibitory action on HMG-CoA synthase of racemic and optically active oxetan-2-ones (β-Lactones) Daniel Romo, Paul H.M. Harrison, Stephen I. Jenkins, R.William Riddoch, Kaapjoo Park, Hong Woon Yang, Cunxiang Zhao, Gerard D. Wright Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . tert-butyl 4-methyl-3-oxo-5-oxa-4,11-diazatricyclo-[6.2.1.0(2,6)]undecane-11-carboxylate 相似度:58.3% Bioorganic & Medicinal Chemistry 2010 18 4498-4508 Novel tricyclic Δ2-isoxazoline and 3-oxo-2-methyl-isoxazolidine derivatives: Synthesis and binding affinity at neuronal nicotinic acetylcholine receptor subtypes Clelia Dallanoce, Fabio Frigerio, Giuliana Martelli, Giovanni Grazioso, Carlo Matera, Diego Yuri Pomè, Luca Pucci, Francesco Clementi, Cecilia Gotti, Marco De Amici Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . nephthediol C14H24O3 相似度:57.1% Natural Product Research 2008 22 1605-1609 New norsesquiterpene and sesquiterpene from a soft coral of the genus Nephthea Ruo-Lin Yang; Yun-Yan Kuang; Jing-Yu Su; Long-Mei Zeng Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . 6-hexyl-4-methoxy-3-methyl-(3R,3aS,4S,6R,6aR)-perhydrofuro[3,4-b]furan-2-one C14H24O4 相似度:57.1% Tetrahedron 2003 59 6521-6530 Radical cyclisation approach for the synthesis of (+)dihydrocanadensolide, (+)dihydrosporothriolide and their C-3 epimers from d-xylose G.V.M Sharma, T Gopinath Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 5-cyclohexyl-5-oxopentanoic acid 相似度:54.5% Phytochemistry 2002 61 669-673 Oxidative cleavage of the C–C bond of 3,6-dialkylcyclohexane-1,2-diones by cell suspension cultures of Marchantia polymorpha Yoshitomo Matsuura, Wen Chai, Etsuko Endoh, Jyumpei Suhara, Hiroki Hamada,C. Akira Horiuchi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . (5S)-decan-5-olide 相似度:54.5% Chemical & Pharmaceutical Bulletin 1990 38 2381-2389 Structure Elucidation of Glycosidic Antibiotics, Glykenins, from Basidiomycetes sp. II. : Absolute Structures of Unusual Polyhydroxylated C26-Fatty Acids, Aglycones of Glykenins Fumiko NISHIDA,Yuji MORI,Naoko ROKKAKU,Sayuri ISOBE,Takeyuki FURUSE,Makoto SUZUKI,Vithaya MEEVOOTISOM,Timothy W. FLEGEL,Yodhathai THEBTARANONTH and Suthum INTARARUANGSORN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . 1-(3'-cyclohexenyl)-4-penten-2-one 相似度:54.5% Helvetica Chimica Acta 1981 64 2193-2202 Fragmentation of Homoallylic Alkoxides. Thermolysis of potassium 2-substituted bicyclo [2.2.2]oct-5-en-2-alkoxides Roger L. Snowden, Karl H. Schulte-Elte Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . Palmicacid 相似度:54.5% Journal of Chinese Pharmaceutical Sciences 2006 15 127-129 Chemical Constituents of Roots of Ranunculus ternatus Thunb. HU Xiao-yan; DOU De-qiang; PEI Yu-ping; and FU Wen-wei Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . 6-Boc-amino-hexanoic acid C11H21NO4 相似度:54.5% Steroids 2012 77 403-412 Design of novel tyrosine-nitrogen mustard hybrid molecules active against uterine, ovarian and breast cancer cell lines Caroline Descôteaux, Kevin Brasseur, Valérie Leblanc, Sophie Parent, Éric Asselin, Gervais Bérubé Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . 9-Hydroxynonanoic Acid 相似度:54.5% Helvetica Chimica Acta 2012 95 428-447 Exaltone (=Cyclopentadecanone) from Isomuscone (=Cyclohexadecanone), a One-C-Atom Ring-Contraction Methodology via a Stereospecific Favorskii Rearrangement: Regioselective Application to (-)-(R)-Muscone Christian Chapuis, Fabrice Robvieux, Carole Cantatore, Christine Saint-Léger, and Laurent Maggi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . compound 12a 相似度:54.5% Tetrahedron Letters 2000 41 10075-10078 New synthesis of 5-amino-4-hydroxy-2,6-dimethylheptanoic acid, a hydroxyethylene isostere of the Val-Ala dipeptide Fabio Benedetti, Paolo Maman, Stefano Norbedo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . compound 15 相似度:54.5% Tetrahedron Letters 2001 42 5167-5170 A facile synthesis of cyclic enecarbamates using Dess–Martin periodinane Chengzhi Yu, Longqin Hu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 8-Acetoxyoctan-5-olide C10H16O4 相似度:54.5% Tetrahedron Letters 2002 43 1321-1324 A rearrangement of 1-hydroperoxy-2-oxabicycloalkanes into lactones of ω-acyloxy-(ω-3)-hydroxyalkanoic acids related to the Criegee reaction Yuri N Ogibin, Alexandre O Terent'ev, Alexandre V Kutkin, Gennady I Nikishin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . N-Benzyloxymonosuberoylamide 相似度:54.5% Archiv der Pharmazie 1999 332 353-357 Inhibitors of Histone Deacetylase Suppress the Growth of MCF-7 Breast Cancer Cells Kathrin Schmidt, Ronald Gust and Manfred Jung Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . (4S)-N,N-Dimethyl-4-tert-butyloxycarbonylamino-6-fluoro-5-hydroxy-hexanamide 相似度:54.5% Bioorganic & Medicinal Chemistry 1997 5 797-807 In vitro and ex vivo inhibition of hepatitis A virus 3C proteinase by a peptidyl monofluoromethyl ketone Tina S Morris, Sven Frormann, Shirley Shechosky, Christopher Lowe, Manjinder S Lall, Verena Gauss-Müller, Robert H Purcell, Suzanne U Emerson, John C Vederas, Bruce A Malcolm Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . 4-Heptyl-3-methyloxetan-2-one 相似度:54.5% Bioorganic & Medicinal Chemistry 1998 6 1255-1272 Synthesis and inhibitory action on HMG-CoA synthase of racemic and optically active oxetan-2-ones (β-Lactones) Daniel Romo, Paul H.M. Harrison, Stephen I. Jenkins, R.William Riddoch, Kaapjoo Park, Hong Woon Yang, Cunxiang Zhao, Gerard D. Wright Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . tert-butyl 6-(2,3-ihydroxypropylamino)hexanoate C13H28NO4 相似度:54.5% Tetrahedron 2012 68 499-506 Carboxyalkyl peptoid PNAs: synthesis and hybridization properties Chiara De Cola, Alex Manicardi, Roberto Corradini, Irene Izzo, Francesco De Riccardis Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . Undecan-5-olide C11H20O2 相似度:54.5% Journal of the Chemical Society, Perkin Transactions 1 1994 2537-2543 Biological Baeyer–Villiger oxidation of some monocyclic and bicyclic ketones using monooxygenases from Acinetobacter calcoaceticus NCIMB 9871 and Pseudomonas putida NCIMB 10007 Rene Gagnon, Gideon Grogan, Melissa S. Levitt, Stanley M. Roberts, Peter W. H. Wan and Andrew J. Willetts Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . (8E)-10-hydroxydec-8-enoic acid C10H16O2 相似度:54.5% Acta Chemica Scandinavica 1992 46 793-798 Tobacco Chemistry. 75. Two New Cembratrienetriols from Tobacco. Forsblom, Ingrid; Berg, Jan-Eric; Wahlberg, Inger Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . Methyl (-)-cis-2,2-Dimethyl-3-(3-oxobutyl)cyclopropanecarboxylate C11H18O3 相似度:54.5% Journal of the Chemical Society, Perkin Transactions 1 1980 1711-1717 Total synthesis of the macrocyclic diterpene (–)-casbene, the putative biogenetic precursor of lathyrane, tigliane, ingenane, and related terpenoid structures Leslie Crombie, Geoffrey Kneen, Gerald Pattenden and Derek Whybrow Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . 18-methyl-19-oxoicosanoic acid C21H40O3 相似度:54.5% Journal of the Chemical Society, Perkin Transactions 1 1982 1449-1453 Polyolefinic 18-methyl-19-oxoicosenoic acid pigments from the fungus Piptoporus australiensis(Wakefield) Cunningham Melvyn Gill Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . 11-hydroxyundecanoic acid C11H22O3 相似度:54.5% Bioorganic & Medicinal Chemistry 2010 18 6429-6441 Synthesis and characterization of mitoQ and idebenone analogues as mediators of oxygen consumption in mitochondria Damien Y. Duveau, Pablo M. Arce, Robert A. Schoenfeld, Nidhi Raghav, Gino A. Cortopassi, Sidney M. Hecht Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . 10-chloro-3-aminodecanoic acid C11H22NO2Cl 相似度:54.5% Tetrahedron 1998 54 13475-13484 Four new microginins, linear peptides from the cyanobacterium Microcystis aeruginosa Keishi Ishida, Hisashi Matsuda, Masahiro Murakami Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . compound 14b C10H18O4 相似度:54.5% Tetrahedron 2004 60 3273-3282 Total syntheses of (−  -vallesamidine and related Aspidosperma and Hunteria type indole alkaloids from the common intermediateHideo Tanino, Kazuhisa Fukuishi, Mina Ushiyama, Kunisuke Okada Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 27 . γ-Butyrolactone C14H28O3Si 相似度:54.5% Tetrahedron 2010 66 3353-3359 Isolation and total syntheses of two new alkaloids, dubiusamines-A, and -B, from Pandanus dubius Mario A. Tan, Mariko Kitajima, Noriyuki Kogure, Maribel G. Nonato, Hiromitsu Takayama Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 28 . N-cyclohexylidene-N'-(2-vinyloxyethyl)ethane-1,2-diamine C12H22N2O 相似度:54.5% Russian Journal of Organic Chemistry 2010 46 495-498 Condensation of N-(2-vinyloxyethyl)ethane-1,2-diamine with carbonyl compounds B. F. Kukharev, V. K. Stankevich, N. A. Lobanova, G. R. Klimenko and V. V. Stankevich, et al. Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 29 . palmitic acid C16H32O2 相似度:54.5% Zeitschrift für Naturforschung C 2003 58 505-516 Immunomodulatory Triterpenoids from the Oleogum Resin of Boswellia carterii Birdwood F. A. Badria, B. R. Mikhaeil, G. T. Maatooq, and M. M. A. Amer Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 30 . palmitic acid 相似度:54.5% Food Chemistry 2011 127 394-403 Chemical composition and biological activity of Citrus jambhiri Lush Dalia Hamdan, Mahmoud Zaki El-Readi, Ahmad Tahrani, Florian Herrmann, Dorothea Kaufmann, Nawal Farrag, Assem El-Shazly, Michael Wink Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 31 . dasycarpusacid C11H18O5 相似度:54.5% Journal of Asian Natural Products Research 2012 14 210-215 Three new compounds from Dictamnus dasycarpus Li-Na Guo, Yue-Hu Pei, Gang Chen, Xuan Lu, Hao Xu & Ji-Cheng Liu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 32 . (3S,3aS,6α,6aR)-dihydrosporothrioride C13H20O4 相似度:53.8% Journal of Natural Products 2010 73 683-687 Eremophilane-Type Sesquiterpenes from the Fungus Xylaria sp. BCC 21097 Masahiko Isaka, Panida Chinthanom, Tanapong Boonruangprapa, Nattawut Rungjindamai and Umpava Pinruan Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 33 . 4-Decyl-3-methyloxetan-2-one 相似度:53.8% Bioorganic & Medicinal Chemistry 1998 6 1255-1272 Synthesis and inhibitory action on HMG-CoA synthase of racemic and optically active oxetan-2-ones (β-Lactones) Daniel Romo, Paul H.M. Harrison, Stephen I. Jenkins, R.William Riddoch, Kaapjoo Park, Hong Woon Yang, Cunxiang Zhao, Gerard D. Wright Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 34 . 4-Undecyl-3-methyloxetan-2-one 相似度:53.8% Bioorganic & Medicinal Chemistry 1998 6 1255-1272 Synthesis and inhibitory action on HMG-CoA synthase of racemic and optically active oxetan-2-ones (β-Lactones) Daniel Romo, Paul H.M. Harrison, Stephen I. Jenkins, R.William Riddoch, Kaapjoo Park, Hong Woon Yang, Cunxiang Zhao, Gerard D. Wright Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 35 . 4-Heptadecyl-3-methyloxetan-2-one 相似度:53.8% Bioorganic & Medicinal Chemistry 1998 6 1255-1272 Synthesis and inhibitory action on HMG-CoA synthase of racemic and optically active oxetan-2-ones (β-Lactones) Daniel Romo, Paul H.M. Harrison, Stephen I. Jenkins, R.William Riddoch, Kaapjoo Park, Hong Woon Yang, Cunxiang Zhao, Gerard D. Wright Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 36 . N-[4-[(tert-butoxycarbonyl)amino]butyl]-N-[3-[(tert-butyldimethylsilyl)oxy]propyl]amine 相似度:53.8% The Journal of Organic Chemistry 1996 61 1023-1029 Enantioselective Total Synthesis of the Macrocyclic Spermidine Alkaloid (− -OncinotineHiroji Ina, Masayuki Ito, and Chihiro Kibayashi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 37 . compound 7a 相似度:53.3% Chemical & Pharmaceutical Bulletin 1989 37 2995-3000 Studies on the Constiutents of Atractylodes lancea Shoji YAHARA,Tomoko HIGASHI,Kazue IWAKI,Toshihiro NOHARA,Nobuhiro MARUBAYASHI,Ikuhiko UEDA,Hiroshi KOHDA,Katsumi GOTO,Hiromasa IZUMI,Mariko NUNO,Shigeki KATSUKI,Susumu ISODA and Motoyoshi SATAKE Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 38 . plucheol A 相似度:53.3% Phytochemistry 1991 30 655-657 Terpene and lignan glycosides from Pluchea indica Taketo Uchiyama, Toshio Miyase, Akira Ueno, Khan Usmanghani Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 39 . Crispatanolide C15H22O2 相似度:53.3% Chemical Communications 1980 1232-1233 X-Ray crystal structure of (+)-crispatanolide, a novel eudesmane-type sesquiterpene δ-lactone from Makinoa crispata(liverwort) Yoshinori Asakawa, Masao Toyota, Zenei Taira, Tsunematsu Takemoto, Masaru Kido and Yasuji Ichikawa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 40 . 10β-Hydroxyginsenol C15H26O2 相似度:53.3% Journal of the Chemical Society, Perkin Transactions 1 1999 727-730 Biotransformation of the fungistatic sesquiterpenoid ginsenol by Botrytis cinerea Josefina Aleu, Rosario Hernández-Galán, James R. Hanson, Peter B. Hitchcock and Isidro G. Collado Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 41 . compound 7 C15H24O3 相似度:53.3% Tetrahedron 2001 57 8481-8493 Structure elucidation of arteannuin O, a novel cadinane diol from Artemisia annua, and the synthesis of arteannuins K, L, M and O Lai-King Sy, Kung-Kai Cheung, Nian-Yong Zhu, Geoffrey D Brown Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 42 . compound 7 相似度:50% Journal of Natural Products 2003 66 655-661 Plakortides M and N, Bioactive Polyketide Endoperoxides from the Caribbean Marine Sponge Plakortis halichondrioides Mara del Sol Jimnez, Sandra P. Garzn, and Abimael D. Rodrguez Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 43 . compound 17 C15H20O3 相似度:50% Journal of Natural Products 1999 62 726-729 Microbial Transformation of Sesquiterpene Lactones by the Fungi Cunninghamella echinulata and Rhizopus oryzae Alejandro F. Barrero, J. Enrique Oltra, Délio S. Raslan, and Dênia A. Saúde Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 44 . 1',2.2-Trimethyl-spiro[cyclopentan-1,2'-(6'-oxabicyclo[3.2.0]heptan)] C13H22O 相似度:50% Helvetica Chimica Acta 1980 63 154-190 Photochemische Reaktionen. 106. Mitteilung. Zur Photochemie tetraalkylsubstituierter γ-Keto-olefine Jacob Berger, Michikazu Yoshioka, Markus P. Zink, Hans R. Wolf, Oskar Jeger Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 45 . trans-3-dodecenedioic acid 相似度:50% Chemical & Pharmaceutical Bulletin 1998 46 1008-1014 Medicinal Foodstuffs. XIV. On the Bioactive Constituents of Moroheiya. (2) : New Fatty Acids, Corchorifatty Acids A, B, C, D, E, and F, from the Leaves of Corchorus olitorius L. (Tiliaceae) : Structures and Inhibitory Effect on NO Production in Mouse Peri Masayuki YOSHIKAWA,Toshiyuki MURAKAMI,Hiromi SHIMADA,Satoshi YOSHIZUMI,Masami SAKA,Johji YAMAHARA and Hisashi MATSUDA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 46 . compound 13 相似度:50% Canadian Journal of Chemistry 2006 84 1388-1396 Synthesis and Lewis acid induced isomerization of mono-, di-, and tri-spiro -keto tetrahydro-furans and -pyrans1 David G. Hilmey, Peter R. Selvaraj, and Leo A. Paquette Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 47 . Chabranol C14H24O3 相似度:50% Organic Letters 2009 Vol.11,No.21 4830-4833 New Terpenoids from the Soft Corals Sinularia capillosa and Nephthea chabroli Shi-Yie Cheng, Ki-Jhih Huang, Shang-Kwei Wang, Zhi-Horng Wen,Chi-Hsin Hsu, Chang-Feng Dai, and Chang-Yih Duh Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 48 . all-endo-tert-Butyl-N-[5-(hydroxy-3-hydroxymethyl)bicyclo[2.2.2]octan-2-yl] carbamate C14H25NO4 相似度:50% Molecules 2011 16 7691-7705 Synthesis and Transformations of di-endo-3-Aminobicyclo-[2.2.2]oct-5-ene-2-carboxylic Acid Derivatives Márta Palkó, Pál Sohár and Ferenc Fülöp Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 49 . compound 22 相似度:50% Phytochemistry 1990 29 757-763 Rearranged caryophyllenes by biotransformation with Chaetomium cochliodes Wolf-Rainer Abraham,Ludger Ernst,Hans-Adolf Arfmann Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 50 . compound 8 相似度:50% Phytochemistry 1982 21 2355-2358 Structural elucidation of 13-acetoxylichesterinic and 13-acetoxyprotolichesterinic acids, two aliphatic lichen metabolites from Neuropogon trachycarpus Raphaël Tih Ghogomu, Bernard Bodo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- |
2楼2012-06-30 08:04:19
杨大松
至尊木虫 (文坛精英)
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3楼2012-06-30 08:09:09