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[求助]
求一化合物微谱查询
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生物碱类化合物 碳谱数据如下： 25.9，55.4，55.9，104.4，111.4，111.6，112.1，119.2，120.4，120.9，121.8，126.9，132.5，137.1，143.7，144.4，146.4，146.8，150.6 溶剂是DMSO，谢谢大侠的帮助。 |
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kaola0916
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cxgxb: 金币+20, ★★★很有帮助 2012-06-11 17:44:33
感谢参与，应助指数 +1
cxgxb: 金币+20, ★★★很有帮助 2012-06-11 17:44:33
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????????????? ??????????? ????С??????????????????????????(,)??????磺 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 25.9,55.4,55.9,104.4,111.4,111.6,112.1,119.2,120.4, 120.9,121.8,126.9,132.5,137.1,143.7,144.4,146.4,146.8,150.6 ?????? ??? CDCl3 CD3CD2OD CD2Cl2 C5D5N C3D7NO CD3SOCD3 C4D8O (CH3)4Si C4D8O2 CD3COOD C4D8O2 H2O D2O CF3COOD CD3OD ND3 CD3COCD3 C6D6 CD3CN ?????? ?????? (???????????????趨) ?????? %(?????>=50%) ???????????鵽556????????(???????????ο?) -------------------------------------------------------------------------------- 1 . Berberrabine ?????:89.4% Acta Bot. Boreal. -Occident. Sin. 2010 30 405-411 Isolation and Identification of Alkaloids fromMacleaya microcarpa (Maxim. ) Fedde YANG Xin-juan, MIAO Fang, ZHENG Feng, ZHOU Le , WANG Xin, GENG Hui-ling, SUN Wei Structure 13C NMR ??????? -------------------------------------------------------------------------------- 2 . epiberberine ?????:80% China Journal of Chinese Materia Medica 2009 34 1097-1100 A new flavonoid glucoside from Huanglian jiedutang decoction MA Zhaotang, YANG Xiuwei, ZHONG Guoyue Structure 13C NMR ??????? -------------------------------------------------------------------------------- 3 . epiberberine ?????:75% Natural Product Sciences 2008 14 68-72 Quantitative Determination of Protoberebrines from the Roots of Coptis chinensis Min, Byung-Sun; Cho, Jae-Sue Structure 13C NMR ??????? -------------------------------------------------------------------------------- 4 . jatrorrhizine ?????:75% Phytochemistry 1990 29 135-139 Degradation of reticuline in Berberis suspension cultures Stefan Jendrzejewski Structure 13C NMR ??????? -------------------------------------------------------------------------------- 5 . Epiberberine ?????:75% Archives of Pharmacal Research 2008 31 1405-1412 Inhibitory activities of the alkaloids from Coptidis Rhizoma against aldose reductase Hyun Ah Jung, Na Young Yoon, Hyun Ju Bae, Byung-Sun Min and Jae Sue Choi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 6 . groenlandicine ?????:73.6% China Journal of Chinese Materia Medica 2009 34 1097-1100 A new flavonoid glucoside from Huanglian jiedutang decoction MA Zhaotang, YANG Xiuwei, ZHONG Guoyue Structure 13C NMR ??????? -------------------------------------------------------------------------------- 7 . coptisine ?????:73.6% China Journal of Chinese Materia Medica 2005 30 1756-1757 Studies on the alkaloides from herb of Corydalis adunca ZHAO Dongbao, TANG Yanli, WANG Hanqiang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 8 . stepharanine C19H18NO4 ?????:73.6% China Journal of Chinese Materia Medica 2011 Vol 36,Issue 8 1024-1027 Study on chemical constituents from branches and leaves of Polyalthia nemoralis LU Ziming, Zhang Qing jian, CHEN Ruoyun, YU Dequan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 9 . columbamine ?????:70% China Journal of Chinese Materia Medica 2009 34 1097-1100 A new flavonoid glucoside from Huanglian jiedutang decoction MA Zhaotang, YANG Xiuwei, ZHONG Guoyue Structure 13C NMR ??????? -------------------------------------------------------------------------------- 10 . coptisine ?????:68.4% Korean Journal of Pharmacognosy 2000 31(4) 390-393 Alkaloidal Components of Chelidonii Fructus Kim, Min-Soo; Hwang, Bang-Yeon; Choe, Sang-Gil; Lee, Myung-Koo; Ro, Jai-Seup; Lee, Kyong-Soon Structure 13C NMR ??????? -------------------------------------------------------------------------------- 11 . coptisine ?????:68.4% Korean Journal of Pharmacognosy 1997 28(4) 257-263 Studies on the Constituents of Berberis amurensis Ruprecht Lee, Hyang-Yi; Kim, Chong-Won Structure 13C NMR ??????? -------------------------------------------------------------------------------- 12 . Groenlandicine ?????:68.4% Archives of Pharmacal Research 2008 31 1405-1412 Inhibitory activities of the alkaloids from Coptidis Rhizoma against aldose reductase Hyun Ah Jung, Na Young Yoon, Hyun Ju Bae, Byung-Sun Min and Jae Sue Choi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 13 . 2-Methoxy-4-(9H-pyrido [3,4-b] indol-1-yl)phenol C18H14N2O2 ?????:68.4% Natural Product Communications 2010 5 1591 - 1596 Synthesis and Bioactivity of -Carboline Derivatives Shengkun Li , Bing Yang, Qianliang Zhang, Jiwen Zhang*, JunruWang and Wenjun Wu Structure 13C NMR ??????? -------------------------------------------------------------------------------- 14 . dehydrothalictrifoline C21H20NO4 ?????:66.6% Chemistry of Natural Compounds 2007 43 214-215 CHEMICAL RESEARCH OF Caragana microphylla Seeds Yan Huo, Cheng Guo, Shan Lu,Qiao-Yan Zhang, and Lu-Ping Qin Structure 13C NMR ??????? -------------------------------------------------------------------------------- 15 . crinumaquine C20H18NO4 ?????:65% Chemistry & Biodiversity 2009 6 1751-1757 Chemical Constituents of Crinum asiaticum L. var. sinicum Baker and Their Cytotoxic Activities Qian Sun, Yun-Heng Shen, Jun-Mian Tian, Jian Tang, Juan Su, Run-Hui Liu, Hui-Liang Li, Xi-Ke Xu, and Wei-Dong Zhang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 16 . 5,3'-Dihydroxy-4,4'-dimethoxy-2,7'-cycloligna-7,7'-diene-9,9'-lactone C20H16O6 ?????:65% Natural Product Research 2010 24 1079-1085 New phenolic compounds from Liatris elegans Zhizhen Zhang; Stacy Ownby; Ping Wang; Wei Yuan; Wanli Zhang; Shiyou Li Structure 13C NMR ??????? -------------------------------------------------------------------------------- 17 . berberine ?????:65% Archives of Pharmacal Research 2005 28 1224-1227 Cytotoxic constituents from the whole plant of corydalis pallida Hyang Rim Kim, Hye -Young Min, Yeon Hee Jeong, Sang Kook Lee and Nam Sook Lee, et al. Structure 13C NMR ??????? -------------------------------------------------------------------------------- 18 . berberine ?????:65% Natural Product Research and Development 2008 20 1005-1007 Chemical Constituents from the Aerial Part of Medicago sativa L. XU Wen-yan; GAO Wei-wei*; HE Chun-nian; TONG Jian-ming Structure 13C NMR ??????? -------------------------------------------------------------------------------- 19 . Berberine hydrochloride ?????:65% Chemistry of Natural Compounds 2011 47 154-156 Alkaloids of Phellodendrone lavallei introduced to Western Georgia M. B. Meskheli, V. Yu. Vachnadze, N. S. Vachnadze and A. J. Bakuridze Structure 13C NMR ??????? -------------------------------------------------------------------------------- 20 . dehydrocorydaline C22H24NO4 ?????:63.6% Journal of the Chinese Chemical Society 1997 44 357-359 Cytotoxic Principles from Saussurea Lappa and Corydalis Turtshaninovii f. Yanhusuo ?????p(Tian-Shung Wu);?????Y(Yann-Lii Leuh);???L??(Chang-Sheng Kuoh);?????(Shwu-Duan Jiang);???鸦(Chieh-Fu Chen);?????(Kuo-Hsiung Lee) Structure 13C NMR ??????? -------------------------------------------------------------------------------- 21 . berberine ?????:63.1% China Journal of Chinese Materia Medica 2009 34 2895-2897 Water-soluble chemical constituents from fruits of Phellodendron chinense var. glabriusculum YAN Chen, WANG Ye, HAO Xiaojiang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 22 . (E)-3-Hydroxy-2',4,4'-trimethoxystilbene C17H18O4 ?????:63.1% Bioorganic & Medicinal Chemistry 2011 19 5155-5166 Synthesis and antimicrobial activity of (E) stilbene derivatives Sabrina Albert, Ralf Horbach, Holger B. Deising, Bianka Siewert, Ren?? Csuk Structure 13C NMR ??????? -------------------------------------------------------------------------------- 23 . tsugacetal C21H24O6 ?????:63.1% Phytochemistry 1985 24 1363-1365 (+)-Tsugacetal, a lignan acetal from Taiwan hemlock Jim-Min Fang, Kuo-Min Wei, Yu-Shia Cheng, Ming-Chu Cheng, Yu Wang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 24 . 5-(3-(tert-butyldimethylsilyloxy)-4-methoxyphenyl)-1-(3,4,5-trimethoxybenzyl)-1H-1,2,3-triazole C25H35N3O5Si ?????:63.1% Bioorganic & Medicinal Chemistry 2010 18 6874-6885 1, 2, 3-Triazole analogs of combretastatin A-4 as potential microtubule-binding agents Kristin Odlo, J??r??mie Fournier-Dit-Chabert, Sylvie Ducki, Osman A.B.S.M. Gani, Ingebrigt Sylte, Trond Vidar Hansen Structure 13C NMR ??????? -------------------------------------------------------------------------------- 25 . 5-(3-(tert-butyldimethylsilyloxy)-4-methoxy-phenyl)-1-(3,4,5-trimethoxyphenyl)-1H-1,2,3-triazole C24H33N3O5Si ?????:63.1% Bioorganic & Medicinal Chemistry 2008 16 4829-4838 1,5-Disubstituted 1,2,3-triazoles as cis-restricted analogues of combretastatin A-4: Synthesis, molecular modeling and evaluation as cytotoxic agents and inhibitors of tubulin Kristin Odlo, Jean Hentzen, J??r??mie Fournier dit Chabert, Sylvie Ducki, Osman A.B.S.M. Gani, Ingebrigt Sylte, Martina Skrede, Vivi Ann Flørenes, Trond Vidar Hansen Structure 13C NMR ??????? -------------------------------------------------------------------------------- 26 . tsugacetal C21H24O6 ?????:63.1% Journal of the Chinese Chemical Society 1985 32 75-80 A Study of the Constituents of the Heartwood of Tsuga Chinensis Pritz. Var. Formosana (Hay.) ??????(Jim-Min Fang);κ???(Kuo-Min Wei);?????(Yu-Shia Cheng) Structure 13C NMR ??????? -------------------------------------------------------------------------------- 27 . dehydrocavidine C21H20NO4 ?????:61.9% Chemistry & Biodiversity 2008 Vol. 5 1335 DNA Topoisomerase I Inhibitory Alkaloids from Corydalis saxicola Xuanxuan Cheng, Dongmei Wang, Lin Jiang, and Depo Yang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 28 . 10-(3,4-dimethoxyphenyl)-6-hydroxyfuro[3',4': 6,7]naphtho[1,2-d]-1,3-dioxol- 9(7H)-one (3) C21H16O7 ?????:61.9% Helvetica Chimica Acta 2008 Vol. 91 2316 Three New Arylnaphthalide Lignans from the Aerial Parts of Bupleurum marginatum Wall. ex DC. Ying Liu, Ting-Ting Zhang, Jin-Song Zhou, and Qiang Wang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 29 . palmatine ?????:61.9% Biochemical Systematics and Ecology 1991 19 433-437 Constituants chimiques de trois especes de Burasaia (Menispermacees) endemiques de Madagascar Ph. Rasoanaivo, S. Ratsimamanga-Urverg, A. Rakoto-Ratsimamanga, A. Raharisololalao Structure 13C NMR ??????? -------------------------------------------------------------------------------- 30 . palmatine C21H22NO4 ?????:61.9% China Journal of Chinese Materia Medica 2008 33 1669-1670 ????????????о? ????, ???? Structure 13C NMR ??????? -------------------------------------------------------------------------------- 31 . palmatine ?????:61.9% China Journal of Chinese Materia Medica 2010 35 1272-1275 Alkaloids in stems and leaves of Stephania cepharantha HE Li; ZHANG Yuanhu; TANG Lijia; SONG Shaohui; SUN Qianyun Structure 13C NMR ??????? -------------------------------------------------------------------------------- 32 . Compound 7a ?????:61.9% Bioorganic & Medicinal Chemistry Letters 2005 15 5053-5056 Synthesis and HIV-1 integrase inhibitory activities of caffeic acid dimers derived from Salvia officinalis Fabrice Bailly, Cl??mence Queffelec, Gladys Mbemba, Jean-François Mouscadet, Philippe Cotelle Structure 13C NMR ??????? -------------------------------------------------------------------------------- 33 . Compound 9 ?????:61.9% Bioorganic & Medicinal Chemistry Letters 2007 17 1755-1758 N-Caffeoylphenalkylamide derivatives as bacterial efflux pump inhibitors Serge Michalet, Gilbert Cartier, Bruno David, Anne-Marie Mariotte, Marie-Genevi??ve Dijoux-franca, Glenn W. Kaatz, Michael Stavri, Simon Gibbons Structure 13C NMR ??????? -------------------------------------------------------------------------------- 34 . 11-Hydroxypalmatine C21H22NO5I ?????:61.9% Journal of Asian Natural products Research 2010 12 99-105 Anti-hyperglycemic effect of 11-hydroxypalmatine, a palmatine derivative from Stephania glabra tubers Deepak Kumar Semwal; Usha Rawat; Ravindra Semwal; Randhir Singh; Gur Jas Preet Singh Structure 13C NMR ??????? -------------------------------------------------------------------------------- 35 . palmatine C21H23NO4 ?????:61.9% Chinese Journal of Natural Medicines 2007 5 31-34 Chemical Constituents of Corydalis saxicola WANG Qi-Zhi; LIANG Jing-Yu; YUAN Yue Structure 13C NMR ??????? -------------------------------------------------------------------------------- 36 . dehydroisoapocavidine C20H19NO5 ?????:60% Chemistry & Biodiversity 2008 Vol. 5 777 Alkaloids from Corydalis saxicola and Their Anti-Hepatitis B Virus Activity Hui-Liang Li, Ting Han, Run-Hui Liu, Chuan Zhang, Hai-Sheng Chen, and Wei-Dong Zhang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 37 . 10-(4-hydroxy-3-methoxyphenyl)furo[3',4': 6,7]naphtho[1,2-d]-1,3-dioxol- 9(7H)-one C20H14O6 ?????:60% Helvetica Chimica Acta 2008 Vol. 91 2316 Three New Arylnaphthalide Lignans from the Aerial Parts of Bupleurum marginatum Wall. ex DC. Ying Liu, Ting-Ting Zhang, Jin-Song Zhou, and Qiang Wang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 38 . arisantetralone A C20H22O5 ?????:60% Journal of Natural Products 2009 72 1663-1668 Oxygenated Lignans from the Fruits of Schisandra arisanensis Yuan-Bin Cheng, Meng-Ting Chang, Yi-Wen Lo, Ching-Jen Ho, Yuh-Chi Kuo, Ching-Te Chien, Shun-Ying Chen, Shorong-Shii Liou, Yao-Haur Kuo, and Ya-Ching Shen Structure 13C NMR ??????? -------------------------------------------------------------------------------- 39 . N-trans-feruloyl tryptamine ?????:60% Phytochemistry 2003 1381-1387 Cinnamic acid amides from Chenopodium album: effects on seeds germination and plant growth Francesca Cutillo, Brigida D??Abrosca, Marina DellaGreca, Cinzia Di Marino,Annunziata Golino, Lucio Previtera, Armando Zarrelli Structure 13C NMR ??????? -------------------------------------------------------------------------------- 40 . (-)-cis-isocorypalmine N-oxide C20H24O5N ?????:60% Planta Medica 2001 67 423-427 A New Tetrahydroprotoberberine N-Oxide Alkaloid and Anti-Platelet Aggregation Constituents of Corydalis tashiroi Jih-Jung Chen, Ya-Ling Chang, Che-Ming Teng, Wei-Yu Lin, Yu-Chang Chen, Ih-Sheng Chen Structure 13C NMR ??????? -------------------------------------------------------------------------------- 41 . berberine C18H18NO4 ?????:60% Chemistry of Natural Compounds 1996 32 216-334 ALKALOIDS. PLANTS, STRUCTURE, PROPERTIES R. Shakirov, M. V. Telezhenetskaya, I. A. Bessonova,S. F. Aripova, I. A. Israilov, M. N. Sultankhodzhaev,V. I. Vinogradova, V. I. Akhmedzhanova, T. S. Tulyaganov,B. T. Salimov, and V. A. Tel'nov Structure 13C NMR ??????? -------------------------------------------------------------------------------- 42 . 1-(4-hydroxy-3-methoxyphenyl)-2-[4-(3-hydroxypropyl)-2-methoxyphenoxy]-propane-1,3-diol C20H26O7 ?????:60% Molecules 2008 13 1219-1229 Identification of Minor Secondary Metabolites from the Latex of Croton lechleri (Muell-Arg) and Evaluation of Their Antioxidant Activity Simona De Marino, Fulvio Gala, Franco Zollo, Sara Vitalini, Gelsomina Fico, Francesco Visioli and Maria Iorizzi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 43 . Spicatolignan B C20H20O7 ?????:60% Journal of Asian Natural Products Research 2007 9 445-449 Two new lignans from Mentha spicata L JIAN ZHENG, GUANG-TONG CHEN, HUI-YUAN GAO, BIN WU and LI-JUN WU Structure 13C NMR ??????? -------------------------------------------------------------------------------- 44 . cis-moschamin C20H20N2O4 ?????:60% Natural Product Research 1997 9 189-199 Moschamine, CIS-Moschamine, Moschamindole and Moschamindolol: Four Novel Indole Alkaloids from Centaurea Moschata Satyajit D. Sarker; Tamara Savchenko; Pensri Whiting; Vladimir Šik; Laurence N. Dinan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 45 . cleomiscosin B ?????:60% China Journal of Chinese Materia Medica 2008 33 1708-1710 Coumarins from branch of Fraxinus sieboldiana and their antioxidative activity LIN Sheng, LIU Mingtao, WANG Sujuan, LI Shuai, YANG Yongchun, SHI Jiangong Structure 13C NMR ??????? -------------------------------------------------------------------------------- 46 . 4,4',9-trihydroxy-3,3'-dimethoxy-9,9'-epoxylignan ?????:60% Journal of Natural Products 1994 Vol 57 713 Lignans from the Wood of Abies pinsapo Alejandro F. Barrero, Ali Haïdour, M. Muñoz Dorado, Dolores G. Gr??valos, Teresa G. Quesada Structure 13C NMR ??????? -------------------------------------------------------------------------------- 47 . compound 1e ?????:60% Phytochemistry 1994 36 785-788 Lignans and an aromatic acid from Cinnamomum philippinense Tian-Shung Wu, Yann-Lii Leu, Yu-Yi Chan, Sheu-Meei Yu, Che-Ming Teng, Jeng-De Su Structure 13C NMR ??????? -------------------------------------------------------------------------------- 48 . 7S,8S-threo-4,7,9,9'-Tetrahydroxy-3,3'-dimethoxy-8-O-4'-neolignan ?????:60% Archives of Pharmacal Research 2011 Vol 34, No 8 1289-1296 Phenolic Constituents of Acorus gramineus Cheol Hyeong Park, Ki Hyun Kim, Il Kyun Lee, Seung Young Lee, Sang Un Choi, Jei Hyun Lee, and Kang Ro Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 49 . 7S,8R-erythro-4,7,9,9'-Tetrahydroxy-3,3'-dimethoxy-8-O-4'-neolignan ?????:60% Archives of Pharmacal Research 2011 Vol 34, No 8 1289-1296 Phenolic Constituents of Acorus gramineus Cheol Hyeong Park, Ki Hyun Kim, Il Kyun Lee, Seung Young Lee, Sang Un Choi, Jei Hyun Lee, and Kang Ro Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 50 . threo-2-(4''-allyl-2''-methoxyphenoxy)-1-(4'-hydroxy-3'-methoxyphenyl)propan-1-ol C20H24O5 ?????:60% Phytochemistry 1988 27 563-568 New neolignans and lignans from the aril of Myristica fragrans Sumitra Hada,Masao Hattori,Yasuhiro Tezuka,Tohru Kikuchi,Tsuneo Namba Structure 13C NMR ??????? |
2楼2012-06-11 12:21:39