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[求助]
求助一化合物微谱数据结构
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化合物数据：15.9, 16.0, 17.2, 18.9, 20.7, 20.9, 21.5, 21.8, 22.0, 26.5, 27.6, 30.4, 33.9, 35.2, 36.6, 39.0, 41.1, 42.7, 47.5, 47.9, 49.7, 53.3, 53.7, 55.4, 57.3, 57.6, 58.6, 71.9, 87.4, 217.5 溶剂：CDCl3 谢谢 |
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kaola0916
铁杆木虫 (著名写手)
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【答案】应助回帖
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感谢参与，应助指数 +1
yjl2007: 金币+10 2012-06-11 21:03:05
感谢参与，应助指数 +1
yjl2007: 金币+10 2012-06-11 21:03:05
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????????????? ??????????? ????С??????????????????????????(,)??????磺 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 15.9, 16.0, 17.2, 18.9, 20.7, 20.9, 21.5, 21.8, 22.0, 26.5, 27.6, 30.4, 33.9, 35.2, 36.6, 39.0, 41.1, 42.7, 47.5, 47.9, 49.7, 53.3, 53.7, 55.4, 57.3, 57.6, 58.6, 71.9, 87.4, 217.5 ?????? ??? CDCl3 CD3CD2OD CD2Cl2 C5D5N C3D7NO CD3SOCD3 C4D8O (CH3)4Si C4D8O2 CD3COOD C4D8O2 H2O D2O CF3COOD CD3OD ND3 CD3COCD3 C6D6 CD3CN ?????? ?????? (???????????????趨) ?????? %(?????>=50%) ???????????鵽889????????(???????????ο?) -------------------------------------------------------------------------------- 1 . (20R)-hydroxydammarane-3,12-dione C30H50O3 ?????:73.3% Journal of Natural Products 1997 60 1236-1241 Microbial Transformation of Protopanaxadiol and Protopanaxatriol Derivatives with Mycobacterium sp. (NRRL B-3805) K. C. Wang, Perng-Haur Wang, and Shoei-Sheng Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 2 . 3??-hydroxygammaceran-21-one C30H50O2 ?????:73.3% Journal of Natural Products 1994 Vol 57 761 Saturated Gammaceranes from the Stem Bark of Abies mariesii Reiko Tanaka, Tomoshi Mizota, Shunyo Matsunaga Structure 13C NMR ??????? -------------------------------------------------------------------------------- 3 . 3-oxo-20S,24R-epoxy-dammarane-25??,26-dial C30H50O4 ?????:73.3% Phytochemistry 1993 32 469-471 3-oxo-20S,24R-epoxy-dammarane-25??,26-diol from Mangifera indica V. Anjaneyulu, J. Suresh Babu, M. Murali Krishna, J. D. Connolly Structure 13C NMR ??????? -------------------------------------------------------------------------------- 4 . 20R,21-epoxydammar-24-ene-3,23-dione C30H46O3 ?????:73.3% Magnetic Resonance in Chmesitry 2005 43 943-947 Two new dammarane triterpenoids from Kageneckia angustifolia D. Don Jos?? Luis L??pez-P??rez, Silvia Erazo, Carla Delporte, Rosa Negrete, Orlando Muñoz, Rub??n Garc??a, Nadine Backhouse and Arturo San Feliciano Structure 13C NMR ??????? -------------------------------------------------------------------------------- 5 . moretenone ?????:73.3% Chinese Traditional and Herbal Drugs 2003 34 13-15 Studies on chemical constituents of Sapium chihsinianum QI Shu hua; WU Shao hua; MA Yun bao; LUO Xiao dong; WU Da gang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 6 . 20R,24R-epoxy-3-oxo-dammarane-25??,26-diol C30H50O4 ?????:73.3% Phytochemistry Letters 2011 4 183-186 Dammarane triterpenes from the apical buds of Gardenia collinsae Thanesuan Nuanyai, Ruengrit Sappapan, Tirayut Vilaivan, Khanitha Pudhom Structure 13C NMR ??????? -------------------------------------------------------------------------------- 7 . 20R,24S-epoxy-3-oxo-dammarane-25??,26-diol C30H50O4 ?????:73.3% Phytochemistry Letters 2011 4 183-186 Dammarane triterpenes from the apical buds of Gardenia collinsae Thanesuan Nuanyai, Ruengrit Sappapan, Tirayut Vilaivan, Khanitha Pudhom Structure 13C NMR ??????? -------------------------------------------------------------------------------- 8 . compound 7 ?????:70.9% Phytochemistry 1994 35 739-743 24-methyl-25-ethyldammarane derivatives from Pilocarpus spicatus Manoel Andrade-Neto, Edilberto R. Silveira, Raimundo Braz-Filho, Maria Teresa P. Gambardela, Regina Helena A. Santos Structure 13C NMR ??????? -------------------------------------------------------------------------------- 9 . 12??,20R-dihydroxydammaran-3-one C30H52O3 ?????:70% Journal of Natural Products 1997 60 1236-1241 Microbial Transformation of Protopanaxadiol and Protopanaxatriol Derivatives with Mycobacterium sp. (NRRL B-3805) K. C. Wang, Perng-Haur Wang, and Shoei-Sheng Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 10 . gammacer-16-en-3-one C30H48O ?????:70% Chemical & Pharmaceutical Bulletin 1995 43 1634-1639 Composite Constituents : Forty-Two Triterpenoids Including Eight Novel Compounds Isolated from Picris hieracioides subsp. Japonica Kenji SHIOJIMA,Kazuo MASUDA,Hideki SUZUKI,Tokuhide LIN,Yuko OOISHI and Hiroyuki AGETA Structure 13C NMR ??????? -------------------------------------------------------------------------------- 11 . lupenone C30H48O ?????:70% Acta Botanica Sinica 2002 44 354-358 Triterpenoids from the Dai Medicinal Plant Winchia calophylla ZHU Wei-Ming, SHEN Yue-Mao, HONG Xin, ZUO Guo-Ying, YANG Xiao-Sheng, HAO Xiao-Jiang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 12 . Phyllanthone (13,27-cycloursan-3-one) C30H48O ?????:70% Phytochemistry Letters 2008 1 11-17 Triterpenoids from the African tree Phyllanthus polyanthus Vuyelwa J. Ndlebe, Neil R. Crouch, Dulcie A. Mulholland Structure 13C NMR ??????? -------------------------------------------------------------------------------- 13 . lupenone,lup-20(29)-en-3-one C38H48O ?????:70% Natural Product Research 1996 8 97-103 Triterpenes from Acacia Dealbata Florbela B. M. Pereira; Fernando M. J. Domingues; Artur M. S. Silva Structure 13C NMR ??????? -------------------------------------------------------------------------------- 14 . 11??-hydroxy-urs-12-en-3-one C30H48O2 ?????:70% Natural Product Research 1999 13 187-194 New Ursane Type Triterpenes From Salvia Mellifera Greene Javier G. Luis; Luc?? S. Andr??s Structure 13C NMR ??????? -------------------------------------------------------------------------------- 15 . lupeone ?????:70% China Journal of Chinese Materia Medica 2006 31 1168-1171 Compounds from marine mangrove plant Bruguiera sexangula var. rhynchopetala BAO Shuyun, LIN Wenhan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 16 . lupenone ?????:70% China Journal of Chinese Materia Medica 2006 31 1872-1875 Studies on constituents in herb of Senecio scandens CHENG Luxin, MA Hongyan, ZHANG Mian, ZHANG Chaofeng, WANG Zhengtao Structure 13C NMR ??????? -------------------------------------------------------------------------------- 17 . lupenone ?????:70% China Journal of Chinese Materia Medica 2006 31 1953-1955 Chemical constitutents of Bauhinia aurea SHANG Xiaoya, LI Shuai, WANG Yinghong, WANG Sujuan, YANG Yongchun, SHI Jiangong Structure 13C NMR ??????? -------------------------------------------------------------------------------- 18 . 3-oxo-20S-hydroxytaraxastane C30H52O2 ?????:70% Fitoterapia 2001 72 709-711 Triterpenes from the resin of Protium heptaphyllum G.S. Susunaga, A.C. Siania, M.G. Pizzolatti,R.A. Yunes, F. Delle Monache Structure 13C NMR ??????? -------------------------------------------------------------------------------- 19 . lup-20(29)-en-3-on-28-oic acid ?????:70% Acta Pharmaceutica Sinica 2005 Vol 40 935-939 Chemical constituents from the mangrove plant Ceriops tagal ZHANG Yan; DENG Zhi-wei; GAO Tian-xiang; FU Hong-zheng; LIN Wen-han Structure 13C NMR ??????? -------------------------------------------------------------------------------- 20 . 20,29-Epoxysalacianone C30H46O3 ?????:70% Phytochemistry 1996 42 789-794 20, 29-Epoxysalacianone and 6??-hydroxysalacianone, two lupane triterepenes from Salacia beddomei A. Hisham, G. Jaya Kumar, Y. Fujimoto, N. Hara Structure 13C NMR ??????? -------------------------------------------------------------------------------- 21 . Gammacer-16-ene-3-one C30H48O ?????:70% Phytochemistry 1996 41 1573-1577 Triterpenoids from Melilotus messanensis; soyasapogenol G, the first natural carbonate derivative Francisco A. Mac??as*, Ana M. Simonet, M. Dolores Esteban, Juan Carlos G. Galindo Structure 13C NMR ??????? -------------------------------------------------------------------------------- 22 . Lup-20(29)-en-3-one ?????:70% Phytochemistry 1995 40 1227-1231 Salacianone and salacianol, two triterpenes from Salacia beddomei A. Hisham, G. Jaya Kumar, Y. Fujimoto, N. Hara Structure 13C NMR ??????? -------------------------------------------------------------------------------- 23 . gammacerane-3,21-dione C30H48O2 ?????:70% Phytochemistry 1995 39 1403-1409 Steroids and terpenoids from the gum resin of Ailanthus grandis T. Hung, H. Stuppner, E. P. Ellmerer-M??ller, D. Scholz, D. Eigner, M. P. Manandhar Structure 13C NMR ??????? -------------------------------------------------------------------------------- 24 . compound 338 ?????:70% Phytochemistry 1994 37 1517-1575 13C NMR Spectra of pentacyclic triterpenoids??a compilation and some salient features Shashi B. Mahato, Asish P. Kundu Structure 13C NMR ??????? -------------------------------------------------------------------------------- 25 . compound 359 ?????:70% Phytochemistry 1994 37 1517-1575 13C NMR Spectra of pentacyclic triterpenoids??a compilation and some salient features Shashi B. Mahato, Asish P. Kundu Structure 13C NMR ??????? -------------------------------------------------------------------------------- 26 . hydroxyhopanone C30H50O2 ?????:70% Phytochemistry 1992 31 3535-3539 Saturated hopane and gammacerane triterpene-diols from the stem bark of Abies veitchii Reiko Tanaka, Shunyo Matsunaga Structure 13C NMR ??????? -------------------------------------------------------------------------------- 27 . limocinone C30H48O ?????:70% Phytochemistry 1991 30 1615-1619 Terpenoids from fruit coatings of Azadirachta indica Salimuzzaman Siddiqui, Bina Shaheen Siddiqui, Ghiasuddin, Shaheen Faizi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 28 . lupeone ?????:70% China Journal of Chinese Materia Medica 2010 35 3156-3160 Chemical constituents from roots of Pueraria lobata LI Guohui; ZHANG Qingwen; WANG Yitao Structure 13C NMR ??????? -------------------------------------------------------------------------------- 29 . ?????? C30H48O ?????:70% Chinese Traditional and Herbal Drugs 2005 36 982-983 ???????????????о? ??????,???,?????,???,???? Structure 13C NMR ??????? -------------------------------------------------------------------------------- 30 . ?????-20(29)-?-3-? C30H48O ?????:70% Chinese Traditional and Herbal Drugs 2005 36 1466-1467 ????????????о?(??) ????,?賿??,??С÷,????? Structure 13C NMR ??????? -------------------------------------------------------------------------------- 31 . Betulonic acid ?????:70% Archives of Pharmacal Research 2006 29 203-208 Cytotoxic terpenes and lignans from the roots of Ainsliaea acerifolia Sang Zin Choi, Min Cheol Yang, Sang Un Choi and Kang Ro Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 32 . 22-hydroxyhopan-3-one ?????:70% Chinese Journal of Medicinal Chemistry 2009 19 195-199 Triterpenoidal constituents of Pericampylus glaucus and their antitumor activity in vitro ZHAO We i-quan, CUI Cheng-bin Structure 13C NMR ??????? -------------------------------------------------------------------------------- 33 . lupeone ?????:70% Journal of Shenyang Pharmaceutical University 2010 27 113-115 Isolation and identification of chemical constituents from stems and leaves of Quercus variabilis Blume XIN Yan, LI Qian, JIA Ling-yun, YUAN Jiu-zhi, SUN Qi-shi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 34 . ?????? C30H48O ?????:70% Journal of China Pharmaceutical University 2001 32 336-338 Study on the Liposoluble Components of the Caulis spatholobi YAN Qi Xin; LI Ping; WANG Di Structure 13C NMR ??????? -------------------------------------------------------------------------------- 35 . compound C30H48O ?????:70% Bulletin of the Korean Chemical Society 2001 22 59-62 Purification, Structure Determination and Biological Activities of 20(29)-lupen-3-one from Daedaleopsis tricolor (Bull. ex Fr.) Bond. et Sing. Eun-Mi Kim, Hae-Ryong Jung, Tae-Jin Min Structure 13C NMR ??????? -------------------------------------------------------------------------------- 36 . 3-O-methylbetulinic aldehyde C31H50O2 ?????:70% Bioorganic & Medicinal Chemistry 2010 18 2549-2558 Synthesis and biological evaluation of antitumor-active ??-butyrolactone substituted betulin derivatives Ren?? Csuk, Alexander Barthel, Stefan Schwarz, Harish Kommera, Reinhard Paschke Structure 13C NMR ??????? -------------------------------------------------------------------------------- 37 . 17,24-epoxy-25-hydroxy-3-oxobaccharan-21-oic acid C30H48O5 ?????:70% The Journal of Organic Chemistry 2004 69 3350-3358 Silvestrol and Episilvestrol, Potential Anticancer Rocaglate Derivatives from Aglaia silvestris Bang Yeon Hwang, Bao-Ning Su, Heebyung Chai, Qiuwen Mi, Leonardus B. S. Kardono, Johar J. Afriastini, Soedarsono Riswan, Bernard D. Santarsiero, Andrew D. Mesecar, Robert Wild, Craig R. Fairchild, Gregory D. Vite, William C. Rose, Norman R. Farnsworth, Ge Structure 13C NMR ??????? -------------------------------------------------------------------------------- 38 . lupenone ?????:70% Journal of the Chinese Chemical Society 1998 45 103-110 Chemical Constituents of Neolitsea parvigemma and Neolitsea Konishii ????B(Keh-Shaw Chen);?????s(Fang-Rong Chang);?Z???(Yi-Chen Chia);?????p(Tian-Shung Wu);??????(Yang-Chang Wu) Structure 13C NMR ??????? -------------------------------------------------------------------------------- 39 . Lupenone ?????:70% Journal of Chinese Pharmaceutical Sciences 2010 19 387-392 Assignment of the absolute stereochemistry of an unusual diterpenoid from the mangrove plant Excoecaria agallocha L. Zhen Liu; Wei Jiang; Zhi-Wei Deng; Wen-Han Lin* Structure 13C NMR ??????? -------------------------------------------------------------------------------- 40 . (20S,25S)-20,25-epoxy-25-methoxy-24,24-dimethyl-26,27-inordammaran-3-one C31H52O3 ?????:67.7% Helvetica Chimica Acta 2008 Vol. 91 333 Two Novel abeo-Dammaranes with a Six-Membered Acetal Moiety from Aglaia perviridis Hiern Shu-Min Yang, Chang-Heng Tan, Hong-Feng Luo, Dong-Xiao Wang, and Da-Yuan Zhu Structure 13C NMR ??????? -------------------------------------------------------------------------------- 41 . 13??,14??-epoxy-21??-methoxyserratan-3-one C31H50O3 ?????:67.7% Journal of Natural Products 2001 64 1044-1047 Structure and Stereochemistry of Epoxyserratanes from the Cuticle of Picea jezoensis var. jezoensis Reiko Tanaka, Kazuhiro Tsujimoto, Yasuko In,Toshimasa Ishida, Shunyo Matsunaga, and Yukimasa Terada Structure 13C NMR ??????? -------------------------------------------------------------------------------- 42 . 21??-methoxyserrat-13-ene-3,15-dione C31H48O3 ?????:67.7% Journal of Natural Products 1997 60 319-322 New Methoxytriterpene Dione from the Cuticle of Picea jezoensis var. jezoensis Reiko Tanaka, Kazuhiro Tsujimoto, Yasuko In, and Shunyo Matsunaga Structure 13C NMR ??????? -------------------------------------------------------------------------------- 43 . 3-Oxo-11??-methoxyurs-12-ene C31H50O2 ?????:67.7% Phytochemistry 2010 71 1741-1748 Antiproliferative terpenoids and alkaloids from the roots of Maytenus vitis-idaea and Maytenus spinosa Mar??a Tereza Rojo de Almeida, Carla R??os-Luci, Jos?? M. Padr??n, Jorge A. Palermo Structure 13C NMR ??????? -------------------------------------------------------------------------------- 44 . methyl 3-oxolupan-28-oate C31H50O3 ?????:67.7% Russian Journal of Organic Chemistry 2009 45 1464-1467 First examples of hydroxycyclopropanation in the series of lupane triterpenoids V. N. Odinokov, E. R. Shakurova, L. M. Khalilov and U. M. Dzhemilev Structure 13C NMR ??????? -------------------------------------------------------------------------------- 45 . 3-Oxo-28-nor-18??(H)-lupan-17??-yl acetate C31H50O3 ?????:67.7% Natural Product Communications 2008 3 1569-1574 Oxidative Decarboxylation of Triterpene C-28 Acids ofLupane Series Nataliya G. ??omissarova, Nataliya G. Belenkova, Olga V. Shitikova, Leonid V. Spirikhin andMarat S. Yunusov Structure 13C NMR ??????? -------------------------------------------------------------------------------- 46 . foliasalaci B1 C30H50O2 ?????:66.6% Chemical & Pharmaceutical Bulletin 2008 56(7) 915-920 Hnew Triterpene Constituents, Foliasalacins A1??A4, B1??B3, and C, from the Leaves of Salacia chinensis Masayuki YOSHIKAWA,Yi ZHANG, Tao WANG, Seikou NAKAMURA, and Hisashi MATSUDA Structure 13C NMR ??????? -------------------------------------------------------------------------------- 47 . foliasalaci B2 C30H50O2 ?????:66.6% Chemical & Pharmaceutical Bulletin 2008 56(7) 915-920 Hnew Triterpene Constituents, Foliasalacins A1??A4, B1??B3, and C, from the Leaves of Salacia chinensis Masayuki YOSHIKAWA,Yi ZHANG, Tao WANG, Seikou NAKAMURA, and Hisashi MATSUDA Structure 13C NMR ??????? -------------------------------------------------------------------------------- 48 . 3-oxo-15??-hydroxylup-20(29)-en-28-oic C30H46O4 ?????:66.6% Phytochemistry 2007 68 834-839 Biotransformation of betulinic and betulonic acids by fungi Denise Z.L. Bastos,Ida C. Pimentel, Daniel A. de Jesus,Br??s H. de Oliveira Structure 13C NMR ??????? -------------------------------------------------------------------------------- 49 . 17??,21??-epoxyhopan-3-one C30H48O2 ?????:66.6% Phytochemistry 2002 59 791-794 Triterpenoids from Gentiana scabra Rie Kakuda, Takeyoshi Iijima, Yasunori Yaoita, Koichi Machida, Masao Kikuchi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 50 . compound 4b ?????:66.6% Journal of Natural Products 2002 65 1838-1842 New Scalarane Class Sesterterpenes from an Indonesian Sponge, Phyllospongia sp. Michael C. Roy, Junichi Tanaka,Nicole de Voogd, and Tatsuo Higa Structure 13C NMR ??????? |
2楼2012-06-11 12:28:30
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您好！可以帮忙查一下下面这个化合物的微谱数据结构吗？ http://muchong.com/bbs/viewthread.php?tid=5159104 老板催着要结构，实在没办法，谢谢啊！ |
3楼2012-11-09 10:33:54