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《离子液体电沉积》Electrodeposition from Ionic Liquids
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Contents Preface IX Foreword XIII List of Contributors XV List of Abbreviations XIX 1 Why use Ionic Liquids for Electrodeposition? 1 Andrew P. Abbott, Ian Dalrymple, Frank Endres, and Douglas R. MacFarlane 1.1 Non-aqueous Solutions 3 1.2 Ionic Fluids 3 1.3 What is an Ionic Liquid? 4 1.4 Technological Potential of Ionic Liquids 6 1.5 Concluding Remarks 12 References 12 2 Synthesis of Ionic Liquids 15 Tom Beyersdorff, Thomas J. S. Schubert, Urs Welz-Biermann, Will Pitner, Andrew P. Abbott, Katy J. McKenzie, and Karl S. Ryder 2.1 Synthesis of Chloroaluminate Ionic Liquids 15 2.2 Air- and Water-stable Ionic Liquids 21 2.3 Eutectic-based Ionic Liquids 31 References 42 3 Physical Properties of Ionic Liquids for Electrochemical Applications 47 Hiroyuki Ohno 3.1 Introduction 47 3.2 Thermal Properties 47 3.3 Viscosity 54 3.4 Density 55 3.5 Refractive Index 56 3.6 Polarity 58 3.7 Solubility of Metal Salts 64 3.8 Electrochemical Properties 66 3.9 Conclusion and Future Prospects 77 Acknowledgement 77 References 78 4 Electrodeposition of Metals 83 Thomas Schubert, Sherif Zein, El Abedin, Andrew P. Abbott, Katy J. McKenzie, Karl S. Ryder, and Frank Endres 4.1 Electrodeposition in AlCl3-based Ionic Liquids 84 4.2 Electrodeposition of Metals in Air- and Water-stable Ionic Liquids 92 4.3 Deposition of Metals from Non-chloroaluminate Eutectic Mixtures 103 4.4 Troublesome Aspects 114 References 120 5 Electrodeposition of Alloys 125 I.-Wen Sun, and Po-Yu Chen 5.1 Introduction 125 5.2 Electrodeposition of Al-containing Alloys from Chloroaluminate Ionic Liquids 126 5.3 Electrodeposition of Zn-containing Alloys from Chlorozincate Ionic Liquids 132 5.4 Fabrication of a Porous Metal Surface by Electrochemical Alloying and De-alloying 137 5.5 Nb–Sn 139 5.6 Air- and Water-stable Ionic Liquids 140 5.7 Summary 145 References 145 6 Electrodeposition of Semiconductors in Ionic Liquids 147 Natalia Borisenko, Sherif Zein El Abedin, and Frank Endres 6.1 Introduction 147 6.2 Gallium Arsenide 149 6.3 Indium Antimonide 149 6.4 Aluminum Antimonide 150 6.5 Zinc Telluride 150 6.6 Cadmium Telluride 151 6.7 Germanium 151 6.8 Silicon 155 6.9 Grey Selenium 160 6.10 Conclusions 164 References 164 7 Conducting Polymers 167 Jennifer M. Pringle, Maria Forsyth, and Douglas R. MacFarlane 7.1 Introduction 167 7.2 Electropolymerization – General Experimental Techniques 171 7.3 Synthesis of Conducting Polymers 177 7.4 Characterization 191 7.5 Future Directions 203 7.6 Conclusions 207 References 208 8 Nanostructured Metals and Alloys Deposited from Ionic Liquids 213 Rolf Hempelmann, and Harald Natter 8.1 Introduction 213 8.2 Pulsed Electrodeposition from Aqueous Electrolytes 215 8.3 Special Features of Ionic Liquids as Electrolytes 220 8.4 Nanocrystalline Metals and Alloys from Chlorometallate-based Ionic Liquids 222 8.5 Nanocrystalline Metals from Air- and Water-stable Ionic Liquids 227 8.6 Conclusion and Outlook 234 Acknowledgement 235 References 235 9 Electrodeposition on the Nanometer Scale: In Situ Scanning Tunneling Microscopy 239 Frank Endres, and Sherif Zein El Abedin 9.1 Introduction 239 9.2 In situ STM in [Py1,4] TFSA 241 9.3 Electrodeposition of Aluminum 245 9.4 Electrodeposition of Tantalum 250 9.5 Electrodeposition of Poly(p-phenylene) 252 9.6 Summary 256 References 256 10 Plasma Electrochemistry with Ionic Liquids 259 J¨urgen Janek, Marcus Rohnke, Manuel P¨olleth, and Sebastian A. Meiss 10.1 Introduction 259 10.2 Concepts and Principles 260 10.3 Early Studies 265 10.4 The Stability of Ionic Liquids in Plasma Experiments 269 10.5 Plasma Electrochemical Metal Deposition in Ionic Liquids 274 10.6 Conclusions and Outlook 282 Acknowledgement 283 References 283 11 Technical Aspects 287 Debbie S. Silvester, Emma I. Rogers, Richard G. Compton, Katy J. McKenzie, Karl S. Ryder, Frank Endres, Douglas MacFarlane, and Andrew P. Abbott 11.1 Metal Dissolution Processes/Counter Electrode Reactions 287 11.2 Reference Electrodes for Use in Room-temperature Ionic Liquids 296 11.3 Process Scale Up 310 11.4 Towards Regeneration and Reuse of Ionic Liquids in Electroplating 319 11.5 Impurities 334 Appendix: Protocol for the Deposition of Zinc from a Type III Ionic Liquid 344 References 345 12 Plating Protocols 353 Frank Endres, Sherif Zein El Abedin, Q. Liu, Douglas R. MacFarlane, Karl S. Ryder, and Andrew P. Abbott 12.1 Electrodeposition of Al from 1-Ethyl-3-methylimidazolium chloride/AlCl3 353 12.2 Electrodeposition of Al from 1-Butyl-3-methylimidazolium chloride–AlCl3 – Toluene 356 12.3 Electrodeposition of Al from 1-Ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)amide/AlCl3 358 12.4 Electrodeposition of Al from 1-Butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide/AlCl3 360 12.5 Electrodeposition of Li from 1-Butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide/Lithium bis(trifluoromethylsulfonyl)amide 362 12.6 Electrodeposition of Ta from 1-Butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide 364 12.7 Electrodeposition of Zinc Coatings from a Choline Chloride: Ethylene Glycol-based Deep Eutectic Solvent 365 References 367 13 Future Directions and Challenges 369 Frank Endres, Andrew P. Abbott, and Douglas MacFarlane 13.1 Impurities 369 13.2 Counter Electrodes/Compartments 370 13.3 Ionic Liquids for Reactive (Nano-)materials 371 13.4 Nanomaterials/Nanoparticles 372 13.5 Cation/Anion Effects 373 13.6 Polymers for Batteries and Solar Cells 373 13.7 Variable Temperature Studies 374 13.8 Intrinsic Process Safety 374 13.9 Economics (Price, Recycling) 375 13.10 Which Liquid to Start With? 375 13.11 Fundamental Knowledge Gaps 376  |
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