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a strategy of steric hindrance has been successfully applied to the design of a series of novel chiral diamines fromamino acids, and a series of robust and tunable bulky chiral primaryamine catalysts have been developed and applied in the direct diastereo- and enantioselective Michael addition of substituted rhodanines to R,β-unsaturated ketones. The reactions proceeded well, and a variety of different enones were well tolerated, providing access to a wide range of enantioenriched rhodanine derivatives, which were proven to be valuable scaffolds in biochemistry and medicinal chemistry |
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2楼2012-04-17 09:04:17