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Brown-red block single crystals was afforded by slow evaporation of CH3CN-H2O solution of X in an open vial at room temperature The residual brown solid was washed Et2O (2 × 0.5 mL) and H2O (2 × 0.5 mL), and then re-dissolved in CH3CN/H2O (3 mL/0.5 mL). Slow evaporation of the solvent in an open vial at room temperature resulted in olive block crystals of x which were suitable for the X-ray diffraction study |
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