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csgdaipanp银虫 (小有名气)
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[求助]
审稿意见
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文章投稿 Journal of Solid State Electrochemistry 审稿人提出了下面这个两个问题，实在是不知道怎么回答，知道的朋友，麻烦解释一下哦！感激不尽！ Also S/N = 3 was used to determine the LOD, but this technique is only applicable in homogeneous solution. For interfacial (heterogeneous) electrochemistry you cannot extrapolate using S/N = 3 due to the different activity of different sites on the electrode surface, especially at very low concentrations, and 3 times the standard deviation should be used instead. P10, amperometric response. The anodic (stripping) voltammetry of Pd(II) is reported. How was it reduced in the first place!? Significantly more detail regarding the experimental protocol needs to be included. |
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