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经典Ebook：Modern Analytical Chemistry
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经典Ebook：Modern Analytical Chemistry ebook ： Modern Analytical Chemistry by McGraw-Hill 共８１６页，Chapter 1 Introduction 1 1A What is Analytical Chemistry? 2 1B The Analytical Perspective 5 1C Common Analytical Problems 8 1D Key Terms 9 1E Summary 9 1F Problems 9 1G Suggested Readings 10 1H References 10 Chapter 2 Basic Tools of Analytical Chemistry 11 2A Numbers in Analytical Chemistry 12 2A.1 Fundamental Units of Measure 12 2A.2 Significant Figures 13 2B Units for Expressing Concentration 15 2B.1 Molarity and Formality 15 2B.2 Normality 16 2B.3 Molality 18 2B.4 Weight, Volume, and Weight-to-Volume Ratios 18 2B.5 Converting Between Concentration Units 18 2B.6 p-Functions 19 2C Stoichiometric Calculations 20 2C.1 Conservation of Mass 22 2C.2 Conservation of Charge 22 2C.3 Conservation of Protons 22 2C.4 Conservation of Electron Pairs 23 2C.5 Conservation of Electrons 23 2C.6 Using Conservation Principles in Stoichiometry Problems 23 2D Basic Equipment and Instrumentation 25 2D.1 Instrumentation for Measuring Mass 25 2D.2 Equipment for Measuring Volume 26 2D.3 Equipment for Drying Samples 29 2E Preparing Solutions 30 2E.1 Preparing Stock Solutions 30 2E.2 Preparing Solutions by Dilution 31 2F The Laboratory Notebook 32 2G Key Terms 32 2H Summary 33 2I Problems 33 2J Suggested Readings 34 2K References 34 Chapter 3 The Language of Analytical Chemistry 35 3A Analysis, Determination, and Measurement 36 3B Techniques, Methods, Procedures, and Protocols 36 3C Classifying Analytical Techniques 37 3D Selecting an Analytical Method 38 3D.1 Accuracy 38 3D.2 Precision 39 3D.3 Sensitivity 39 3D.4 Selectivity 40 3D.5 Robustness and Ruggedness 42 3D.6 Scale of Operation 42 3D.7 Equipment, Time, and Cost 44 3D.8 Making the Final Choice 443E Developing the Procedure 45 3E.1 Compensating for Interferences 45 3E.2 Calibration and Standardization 47 3E.3 Sampling 47 3E.4 Validation 47 3F Protocols 48 3G The Importance of Analytical Methodology 48 3H Key Terms 50 3I Summary 50 3J Problems 51 3K Suggested Readings 52 3L References 52 Chapter 4 Evaluating Analytical Data 53 4A Characterizing Measurements and Results 54 4A.1 Measures of Central Tendency 54 4A.2 Measures of Spread 55 4B Characterizing Experimental Errors 57 4B.1 Accuracy 57 4B.2 Precision 62 4B.3 Error and Uncertainty 64 4C Propagation of Uncertainty 64 4C.1 A Few Symbols 65 4C.2 Uncertainty When Adding or Subtracting 65 4C.3 Uncertainty When Multiplying or Dividing 66 4C.4 Uncertainty for Mixed Operations 66 4C.5 Uncertainty for Other Mathematical Functions 67 4C.6 Is Calculating Uncertainty Actually Useful? 68 4D The Distribution of Measurements and Results 70 4D.1 Populations and Samples 71 4D.2 Probability Distributions for Populations 71 4D.3 Confidence Intervals for Populations 75 4D.4 Probability Distributions for Samples 77 4D.5 Confidence Intervals for Samples 80 4D.6 A Cautionary Statement 81 4E Statistical Analysis of Data 82 4E.1 Significance Testing 82 4E.2 Constructing a Significance Test 83 4E.3 One-Tailed and Two-Tailed Signif http://files.rushim.ru/books/analitika/ModernAnalyticChemistry.pdf [ Last edited by darliu on 2007-5-20 at 00:03 ] |
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