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lgq101木虫 (小有名气)
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[求助]
求一段有机合成翻译~~~谢谢
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| General Procedure for Enyne Metathesis (8). Vacuum-dried resin 3 (800 mg, 0.86 meq, 1.0 eq) was swollen with degassed toluene (200 mL) for 10 min, then a stock solution of Grubbs’ second-generation catalyst (0.1 M in degassed toluene, 5.1 mL, 0.51 mmol, 0.6 eq) was added via syringe and the mixture was stirred at 60 °C overnight. The resin was cooled, washed, and dried to afford vinylpyrrolines 8. |
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zou-yanhua
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liubencai
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