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[求助]
审稿中的两个意见不知道怎么处理
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2. last sentence: the Cg...Cg distance and symmetry operations must be given. However, the two oxazole units have two five-membered and six six-membered rings. this implies a lot of work defining the centres of gravity (Cg's) for the rings and calculating the distances between Cg's and average perpendicular distances between the ring systems. Moreover, your Fig. 2 does not show the inversion related \p--\p interaction clearly, and the symmetry operators for molecule A and molecule B should also be provided in the caption of Figure 2. You need a programme like PLATON which can help analize this problem by using the "cal all" option. It will also be seen that the complexes are held together by a combination of different \p--\p interactions and a C---H...\p contact when PLATON is applied. (see point 9) The best was to delete the sentence in Abstract ... exhibits obvious intermolecular \p--\p interactions and also delete Fig. 2. Otherwise, details must be calculated, which needs time ... IMPORTANT: all numerical measured values need standard uncertainties (s.u.), which will be described for the Comment section. 6. Comment: please think of having two oxazol ligands, so the average deviation of Ir1 C18 C23 C24 N2 and the dihedral angles as for molecule 1(average is 0.0628 and 0.0719 (typo mol. 1, please check, and mol. 2) the s.u.'s for dihedral angles in parentheses: 6.5(2)\% (6.9(1)\% for mol.2), 9.2(1)\% (11.4(1)\% for mol. 2). please check with MPLA in SHELXL97. |
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