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However, the yield dropped significantly when a bulky R group is present,which could be explained by the increased difficulty in the formation of enamine with bulky ketones. The condensations of cyclic diones also proceeded in lower yields and required longer time to complete, but with better diastereoselectivity. Compared to the reactions with D-glucosamine, the reactions with D-galactosamine generally proceeded with lower diastereoselectivity. |
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