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[求助]
TiO2三种晶型的XRD特征峰及对应晶面
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目前只了解锐钛矿的XRD特征峰在各个2õ角处对应的晶面，即25.3°对应(101), 38°对应(004), 47.7°对应(105)，54.8°对应(204)， 想请教的是金红石和板钛矿的情况，谢谢！！ |
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yx_clouds
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【答案】应助回帖
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下面这个是板钛矿的： d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.512 100.0 92.0 1 2 0 25.339 12.670 0.1424 1.7891 3.465 80.0 74.0 1 1 1 25.689 12.844 0.1443 1.8133 2.900 90.0 100.0 1 2 1 30.807 15.403 0.1724 2.1666 2.729 4.0 5.0 2 0 0 32.790 16.395 0.1832 2.3024 2.476 25.0 33.0 0 1 2 36.251 18.125 0.2019 2.5376 2.409 18.0 24.0 2 0 1 37.296 18.648 0.2076 2.6082 2.370 6.0 8.0 1 3 1 37.933 18.966 0.2110 2.6511 2.344 4.0 5.0 2 2 0 38.370 19.185 0.2133 2.6805 2.332 4.0 6.0 2 1 1 38.575 19.288 0.2144 2.6943 2.296 5.0 7.0 0 4 0 39.204 19.602 0.2178 2.7366 2.254 8.0 11.0 1 1 2 39.966 19.983 0.2218 2.7876 2.244 18.0 26.0 0 2 2 40.151 20.076 0.2228 2.8000 2.133 16.0 24.0 2 2 1 42.339 21.169 0.2344 2.9457 1.968 16.0 26.0 0 3 2 46.071 23.036 0.2540 3.1919 1.893 30.0 51.0 2 3 1 48.011 24.005 0.2641 3.3185 1.851 18.0 31.0 1 3 2 49.171 24.586 0.2701 3.3937 1.833 3.0 5.0 2 1 2 49.692 24.846 0.2727 3.4274 1.756 3.0 6.0 2 4 0 52.011 26.005 0.2846 3.5765 1.690 20.0 38.0 3 2 0 54.203 27.102 0.2957 3.7161 1.661 30.0 58.0 2 4 1 55.233 27.616 0.3009 3.7812 1.648 5.0 10.0 1 5 1 55.710 27.855 0.3033 3.8112 1.609 13.0 26.0 1 1 3 57.174 28.587 0.3106 3.9031 1.596 2.0 4.0 2 3 2 57.683 28.842 0.3131 3.9349 1.540 7.0 15.0 1 2 3 59.990 29.995 0.3245 4.0779 1.494 10.0 22.0 0 5 2 62.064 31.032 0.3346 4.2050 1.472 4.0 9.0 1 6 0 63.063 31.532 0.3395 4.2659 1.465 9.0 20.0 3 1 2 63.414 31.707 0.3412 4.2871 1.460 12.0 26.0 2 5 1 63.642 31.821 0.3423 4.3009 1.451 12.0 27.0 2 0 3 64.103 32.051 0.3445 4.3288 1.441 6.0 13.0 1 3 3 64.601 32.301 0.3469 4.3588 1.433 10.0 22.0 2 1 3 65.001 32.500 0.3488 4.3828 1.416 9.0 20.0 1 6 1 65.874 32.937 0.3529 4.4351 1.364 5.0 12.0 4 0 0 68.766 34.383 0.3666 4.6064 1.335 8.0 19.0 3 3 2 70.430 35.215 0.3743 4.7037 1.318 3.0 7.0 4 0 1 71.488 35.744 0.3792 4.7650 1.311 2.0 5.0 2 3 3 71.929 35.964 0.3812 4.7905 1.285 2.0 5.0 0 0 4 73.646 36.823 0.3890 4.8889 1.238 10.0 26.0 0 2 4 76.946 38.473 0.4038 5.0749 1.210 2.0 5.0 4 3 1 79.022 39.511 0.4130 5.1897 1.207 1.0 3.0 1 2 4 79.281 39.640 0.4141 5.2039 1.155 4.0 11.0 3 3 3 83.640 41.820 0.4328 5.4390 1.148 2.0 6.0 0 8 0 84.285 42.142 0.4355 5.4732 1.143 2.0 6.0 4 4 1 84.721 42.360 0.4374 5.4961 1.121 4.0 11.0 0 4 4 86.740 43.370 0.4458 5.6015 1.039 3.0 9.0 5 2 1 95.586 47.793 0.4808 6.0421 1.039 3.0 9.0 4 2 3 95.586 47.793 0.4808 6.0421 1.036 2.0 6.0 2 8 1 95.989 47.995 0.4823 6.0613 1.023 4.0 13.0 3 2 4 97.606 48.803 0.4884 6.1377 0.987 2.0 7.0 1 2 5 102.556 51.278 0.5064 6.3640 0.982 4.0 13.0 2 5 4 103.198 51.599 0.5087 6.3925 0.982 4.0 13.0 3 7 2 103.198 51.599 0.5087 6.3925 |
19楼2011-06-16 20:30:06
2楼2011-06-15 13:30:20
nanohappyyou
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3楼2011-06-15 16:13:21
4楼2011-06-15 21:51:49