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lgq101木虫 (小有名气)
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[求助]
求助翻译一实验过程，谢谢~~~
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Solid-phase synthesis and chemical space analysis of a 190-membered alkaloid/terpenoid-like library General Procedure for Pauson–Khand Reaction (5). Vacuum-dried enyne resin 3 (800 mg, 0.86 meq, 1.0 eq) was swollen with CH2Cl2 (20 mL) for 10 min, then Co2(CO)8 (1.18 g, 3.44 mmol, 4.0 eq) was added and the slurry was stirred at RT for 3 h. The solution was decanted from the flask under positive Ar pressure and the resin was washed with anhydrous CH3CN (2 × 25 mL). The resin was swollen with anhydrous CH3CN (20mL) and heated to 75 °C for 12 h, then allowed to cool to RT. The resin was washed and dried to afford cyclopentapyrrolidinones 5. |
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1986
铁杆木虫 (知名作家)
药童
- 翻译EPI: 26
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【答案】应助回帖
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sltmac(金币+1): 谢谢交流~ 2011-06-02 22:48:26
lgq101(金币+10, 翻译EPI+1): 谢谢~~~ 2011-06-03 09:04:42
sltmac(金币+1): 谢谢交流~ 2011-06-02 22:48:26
lgq101(金币+10, 翻译EPI+1): 谢谢~~~ 2011-06-03 09:04:42
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Solid-phase synthesis and chemical space analysis of a 190-membered alkaloid/terpenoid-like library 一个有190成员的萜类、生物碱化合物库的固定相合成和化学空间分析。 General Procedure for Pauson–Khand Reaction (5). Vacuum-dried enyne resin 3 (800 mg, 0.86 meq, 1.0 eq) was swollen with CH2Cl2 (20 mL) for 10 min, then Co2(CO)8 (1.18 g, 3.44 mmol, 4.0 eq) was added and the slurry was stirred at RT for 3 h. 对于Pauson–Khand Reaction (5). 反应的一般性实验步骤，真空干燥国的炔树脂3（800毫克，0.86mmol,1.0当量）在20毫升的二氯甲烷中搅拌溶解10分钟，然后加入Co2(CO)8 (1.18 g, 3.44 mmol, 4.0 eq)，形成的泥浆在室温下搅拌3小时。 |
2楼2011-06-02 13:26:03