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quzhaojuan

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[交流] 高手帮忙分析下:这个氮掺杂的二氧化钛的制备加硫化钠的作用是什么 已有1人参与

看了一篇文献上制备N-doped TiO2
TiCl3加Na2S ,再加氨水沉淀反应为什么就会得到 N-doped TiO2 ,Na2S的作用是什么
原文的实验部分是这样写的
For the typical synthesis of the N-doped TiO2 powders, 50 mL
of 15% titanium trichloride(48.6 mmol) was mixed with 50 mL
of Na2S solution (51.2 mmol). The pH of this acidic solution was
adjusted to 8.5 by slow addition of diluted NH3 solution. The
precipitate formed at this pH was continuously stirred for 4 h. The
precipitate was filtered and washed with double distilled water until
the filtrate was free from chloride and sulfide ions. The oxide was
calcined at different temperatures, viz., 400, 500, and 600 °C, for
4 h in air. Pure TiO2 was also prepared by a similar procedure
without the addition of Na2S solution.
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yuran15137

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zhangwengui330(金币+2): 欢迎参与讨论! 2011-05-07 16:16:42
引用回帖:
Originally posted by quzhaojuan at 2011-05-06 15:28:47:
看了一篇文献上制备N-doped TiO2
TiCl3加Na2S ,再加氨水沉淀反应为什么就会得到 N-doped TiO2 ,Na2S的作用是什么
原文的实验部分是这样写的
For the typical synthesis of the N-doped TiO2 powders, 50 mL ...

这个反应我没做过,不过从你的描述看,TiCl3加Na2S 生成硫化钛沉淀,至于是二硫化钛还是三硫化钛我就不清楚了,然后通过焙烧的方式将硫化钛转化成氧化钛
2楼2011-05-06 17:34:51
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