| 查看: 879 | 回复: 1 | |||
| 本帖产生 1 个 翻译EPI ，点击这里进行查看 | |||
godevil6127银虫 (小有名气)
|
[求助]
急求翻译！万分感谢！-微波合成
|
||
|
化合物1、2、3、4分别是以水杨醛（2-羟基苯乙酮）、正丙胺（正丁胺）、硼酸为原料在乙腈中合成的，采用一锅法，在微波条件为（反应功率800 w，反应温度80℃）下短时间大量合成了上述化合物用于光谱性质的研究，由于化合物1-4N上和与N相连的C上的取代基不同，这些化合物在紫外光照射下，分别有蓝色、蓝紫色、蓝绿色的荧光产生。本论文经过相关的条件实验获得了针对此类化合物的微波合成的最佳反应条件。除化合物5、6外其余化合物的固体粉末在紫外光照射下均能发出较为明显的荧光；含有氟或氨基取代基的化合物对一价离子具有比较好的识别作用。 [ Last edited by godevil6127 on 2011-5-6 at 15:05 ] |
回复此楼» 猜你喜欢
情人节自我反思：在爱情中有过遗憾吗？
已经有6人回复
-
基金正文30页指的是报告正文还是整个申请书
已经有4人回复
-
今年春晚有几个节目很不错，点赞！
已经有6人回复
-
球磨粉体时遇到了大的问题，请指教！
已经有15人回复
-
过年走亲戚时感受到了所开私家车的鄙视链
已经有5人回复
-
江汉大学解明教授课题组招博士研究生/博士后
已经有3人回复
ziyoujisea
银虫 (小有名气)
- 翻译EPI: 6
- 应助: 2 (幼儿园)
- 金币: 485
- 散金: 10
- 帖子: 134
- 在线: 78.4小时
- 虫号: 823658
- 注册: 2009-08-07
- 性别: GG
- 专业: 环境化工
【答案】应助回帖
★ ★
godevil6127(金币+10, 翻译EPI+1): 2011-05-11 09:58:27
Mally89(金币+2): 感谢应助！~欢迎常来！~ 2011-05-17 21:46:11
godevil6127(金币+10, 翻译EPI+1): 2011-05-11 09:58:27
Mally89(金币+2): 感谢应助！~欢迎常来！~ 2011-05-17 21:46:11
| Using salicylaldehyde (2-hydroxyacetophenone), propylamine (n-butylamine), boric acid in the solution of acetonitrile as raw materials, compound 1, 2, 3 and 4 have been prepared by microwave-assisted one-pot method. In the microwave conditions of reaction power 800 w and reaction temperature 80 oC under a short reaction time, large amount of the compounds have been prepared and the spectral properties of these compounds have been studied. For the different of the substituent on C connected to N, there were blue, bluish violet, blue-green fluorescence on those compounds under the irradiation of ultraviolet light. This paper gives the best microwave synthesis conditions of for such compounds All the compounds except for 5,6 have obviously fluorescence effect under the irradiation of ultraviolet light. Compounds containing fluorine or amino substituents have relatively good recognition effect for monovalent ion. |
2楼2011-05-08 00:57:29