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zhigang985银虫 (小有名气)
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[求助]
求助高手翻译一段话，谢谢！
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（1）x微米球的TEM(a, b)、HRTEM(c, d)图及x=0.1 mol/L时，120 ℃反应24 h制得产物x的TEM(e)、HRETEM(f)图 （2）根据实验的结果，我们提出了x空心微米球可能形成的形成机理：首先，乙二胺与x溶液混合形成配合物[x(en)2]2+，然后配合物离解生成的en与透过油膜的CS2发生反应(2)，(2)式中形成的中间体再发生缩聚反应(3)生成H2S，H2S作为反应的S2-源与x发生反应(4)生成xS纳米晶。可能的反应如下 |
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【答案】应助回帖
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zhigang985(金币+10, 翻译EPI+1): 2011-05-02 22:20:48
sltmac(金币+1): 谢谢交流，欢迎常来~~ 2011-05-03 12:36:19
zhigang985(金币+10, 翻译EPI+1): 2011-05-02 22:20:48
sltmac(金币+1): 谢谢交流，欢迎常来~~ 2011-05-03 12:36:19
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翻译不精，仅供参考。 The TEM (a, b) of X microns ball, HRTEM (c, d) chart and x = 0.1 mol/L, the TEM (e), HRETEM (f) chart of the production X were achieved under the conditions of 120 ℃, 24 h. According to the experimental results, we proposed the mechanism that x hollow microns ball might be formed: first, ethylenediamine and X solution were mixed to form complexes [x (en) 2] 2 +, then en generated by complexes dissociation reacted with CS2 penetrated through oil film, as reaction (2), polycondensation reaction (3) by intermediate generated in reaction (2) produced H2S,which reacted with X as the S2- source to generate XS nanocrystalline, as reaction (4). The possible reactions were as follows: |
2楼2011-05-02 21:18:36