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【答案】应助回帖
juliezwj(金币+2, 翻译EPI+1): 谢谢,很完整很细心 2011-04-24 15:52:48
1.Then, to a 1.5 mL sample 2 mL of a 0.5 g'L-1 potassium ferricyan ide solution in 0.5 M sodium carbonate were added.
然后:在1.5ml的样品中加入2ml0.5 g'L-1 铁氰化钾的0.5 M 碳酸钠溶液(注:m是指摩尔每l,即0.5 mol·L-1碳酸钠溶液)
2.The supernatant was analyzed by HPLC in an Applied Biosystems Series 1100 chromatograph using a Hypersil APS-2 column (4.6 *250 mm; particle size, 5 lm). The analysis was carried out at 40 ℃ using a mobile phase of 3:2 MeCN–water 60:40 (v/v) and a flow rate of 0.8 mL min1, and the peaks were detected with a refractive index detector.
上清夜用(Biosystems Series 1100 色谱)高效液相色谱 (Biosystems Series 1100 色谱)-差示折射法测量吸收峰,Hypersil APS-2色谱柱(4.6 *250 mm; 粒径大小:5 lm),柱温:40℃,流动相:乙腈-水(3:2)60:40 (v/v),流速是0.8ml/min。 |
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