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linda_521@163

铜虫 (小有名气)

[交流] 【求助】薄层色谱

请教大家一个关于薄层的问题:
    我现在在做一项薄层鉴别实验,标准是这样的:
    取硝酸钾,用96%乙醇制成0.1mg/ml的溶液,作为对照品
    取样品,用96%乙醇制成0.1mg/ml的溶液,作为供试品
    展开剂:冰醋酸:丙酮:甲苯=15:30:60
       硅胶H板
    点样展开后,将板至于空气中使醋酸尽量挥发尽。喷洒新鲜配制的KI和淀粉溶液。在254nm紫外光下照射15分钟,取出,观察
    供试品中对应的硝酸钾斑点不得深于对照品中的斑点

    我按照此标准操作,没有见到任何斑点,请教大家,这是怎么回事呢?这项显色的原理是什么呢?急求答案啊,谢谢了
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