[交流] Need help for purification of LiClO4 and tetramethyl ammonium perchlorate

Originally posted by ulanhot at 2006-6-27 22:17:
anhydrous lithium perchlorate is prepared by heating the commercially available anhydrous material or its trihydrate at 160 °C for 48 h under high vacuum (P2O5 trap).

Originally posted by miniearth at 2006-7-1 19:23:
你提到的两个化合物目前都是电解质。你如果需要提纯到4个9以上的纯度，那是技术机密，估计很难找到答案。一般可以从生产电解质的公司得到纯度很高的物质。