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【请教】求教如何制备粒径小于10纳米的纳米二氧化硅？？
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如题求教如何制备粒径小于10纳米的纳米二氧化硅？？ 最好能够制备得到粒径较为均一的纳米材料~~~谢谢 找不到类似的文献，帮忙找找吧，谢谢 |
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再推荐一篇ASAP paper Two-Phase Synthesis of Monodisperse Silica Nanospheres with Amines or Ammonia Catalyst and Their Controlled Self-Assembly http://pubs.acs.org/doi/abs/10.1021/am200104m |
4楼2011-04-22 11:43:39
2楼2010-12-10 10:54:05
naomitina(金币+2): 2011-03-17 10:16:18
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看看下边推荐的文献就知道怎么合成了。 (1) Yokoi, T.; Sakamoto, Y.; Terasaki O.; Kubota, Y.; Okubo, T.; Tatsumi, T. J. Am. Chem. Soc. 2006, 128, 13664–13665. (2) Yokoi, T.; Wakabayashi, J.; Otsuka, Y.; Fan, W.; Iwama, M.; Watanabe, R.; Aramaki, K.; Shimojima, A.; Tatsumi, T.; Okubo, T. Chem. Mater. 2009, 21, 3719–3729. (3) Davis, T. M.; Snyder, M. A.; Krohn, J. E.; Tsapatsis, M. Chem. Mater. 2006, 18, 5814–5816. (4) Hartlen, K. D.; Athanasopoulos, A. P. T.; Kitaev, V. Langmuir 2008, 24, 1714–1720. (5) Snyder, M. A.; Lee, J. A.; Davis, T. M.; Scriven, L. E.; Tsapatsis, M. Langmuir 2007, 23, 9924–9928. (6) Yamauchi Y, Imasu J, Kuroda Y, Kuroda K, Sakka Y. J. Mater. Chem. 2009, 19, 1964–1967. (7)Junzheng Wang, Ayae Sugawara, Atsushi Shimojima, and Tatsuya Okubo, Langmuir, 2010, 26 (23), 18491–18498 (8) Watanabe, R.; Yokoi, T.; Kobayashi, E.; Otsuka, Y.; Shimojima, A.; Okubo, T.; Tatsumi, T. J. Colloid Interface Sci., in press. |
3楼2010-12-20 16:58:01
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