做负载贵金属催化剂,看了点文献都说先在氢气中还原若干小时,然后就是passivated几个小时,不知道这个方法是怎么操作的,具体目的是什么?
文献一:……reduced in H2-N2 flow at 450℃ for 4h,and finally passivated in a flowing of CO2-N2 gas for 12h and stored.(载体 是SiO2)
文献二:the samples with different Ru content were reduced in an H2 ?ow at 450 ?C for 8 h, followed by cooling to room temperature in hydrogen and then passivation.(载体是GNF)