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【求助】求LiFePO4标准PDF卡片
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求LiFePO4标准PDF卡片，谢谢 |
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2楼2010-11-29 16:40:25
3楼2010-11-29 17:00:09
lixg711(金币+5): 2010-11-29 21:00:56
lixg711(金币+5): 2010-11-30 10:29:48
lixg711(金币+5): 2010-11-30 10:29:48
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PDF#40-1499: QM=Star(+); d=Diffractometer; I=Diffractometer Triphylite Li Fe P O4 Radiation=CuKa1 Lambda=1.540598 Filter=Graph Calibration=Internal(Si) d-Cutoff= I/Ic(RIR)= Ref= Blanchard, F., Saligan, P. Powder Diffraction, 4 26 (1989) Orthorhombic - (Unknown), Pmnb (62) Z=4 mp= Cell=6.0189x10.347x4.7039 Pearson=oP28 (?) Density(c)=3.577 Density(m)=3.420 Mwt=157.76 Vol=292.95 F(30)=43.9(.0163,42) Ref= Yakubovich, O., Simmov, M., Belov, N. Sov. Phys. Dokl., 22 347 (1977) Strong Line: 3.01/X 2.53/8 4.28/8 3.49/7 5.18/3 2.78/3 3.92/3 2.46/3 1.50/3 1.74/2 NOTE: Specimen from Palermo, New Hampshire, USA. To replace 00-011-0456, 00-019-0721 and 00-027-1248 and validated by calculated pattern 00-042-0580. Optical data on specimen from Garutrask pegmatite, Skellestua, Sweden. Li ( Fe0.78 Mn0.22 ) P O4. d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 5.175 34.0 20.0 0 2 0 17.120 8.560 0.0966 1.2141 4.277 76.0 53.0 0 1 1 20.751 10.375 0.1169 1.4691 3.923 26.0 20.0 1 2 0 22.647 11.324 0.1275 1.6016 3.705 10.0 8.0 1 0 1 23.999 11.999 0.1350 1.6959 3.487 70.0 60.0 0 2 1 25.524 12.762 0.1434 1.8019 3.487 70.0 60.0 1 1 1 25.524 12.762 0.1434 1.8019 3.008 100.0 100.0 1 2 1 29.675 14.837 0.1662 2.0888 3.008 100.0 100.0 2 0 0 29.675 14.837 0.1662 2.0888 2.781 34.0 37.0 0 3 1 32.160 16.080 0.1798 2.2593 2.602 1.0 1.0 2 2 0 34.439 17.220 0.1922 2.4148 2.525 81.0 96.0 1 3 1 35.524 17.762 0.1980 2.4884 2.462 25.0 31.0 2 1 1 36.464 18.232 0.2031 2.5521 2.376 16.0 20.0 1 4 0 37.833 18.917 0.2104 2.6444 2.352 1.0 1.0 0 0 2 38.234 19.117 0.2126 2.6714 2.293 9.0 12.0 0 1 2 39.258 19.629 0.2181 2.7402 2.276 14.0 19.0 2 2 1 39.563 19.782 0.2197 2.7606 2.268 19.0 25.0 0 4 1 39.709 19.854 0.2205 2.7704 2.142 16.0 22.0 0 2 2 42.152 21.076 0.2334 2.9333 2.142 16.0 22.0 1 1 2 42.152 21.076 0.2334 2.9333 2.043 4.0 6.0 2 3 1 44.300 22.150 0.2447 3.0755 2.018 5.0 7.0 1 2 2 44.879 22.439 0.2478 3.1136 1.962 2.0 3.0 2 4 0 46.220 23.110 0.2548 3.2016 1.893 1.0 2.0 0 5 1 48.016 24.008 0.2641 3.3188 1.851 8.0 13.0 2 0 2 49.160 24.580 0.2700 3.3930 1.844 1.0 2.0 3 0 1 49.362 24.681 0.2710 3.4061 1.824 4.0 7.0 2 1 2 49.960 24.980 0.2741 3.4447 1.816 11.0 18.0 3 1 1 50.187 25.093 0.2753 3.4593 1.806 5.0 8.0 1 5 1 50.475 25.237 0.2768 3.4779 1.744 23.0 40.0 2 2 2 52.422 26.211 0.2867 3.6027 1.739 13.0 22.0 0 4 2 52.567 26.284 0.2874 3.6121 1.739 13.0 22.0 3 2 1 52.567 26.284 0.2874 3.6121 1.671 12.0 22.0 1 4 2 54.871 27.435 0.2991 3.7583 1.657 13.0 24.0 1 6 0 55.381 27.691 0.3016 3.7905 1.626 14.0 26.0 3 3 1 56.526 28.263 0.3074 3.8625 1.602 2.0 4.0 2 5 1 57.451 28.726 0.3120 3.9204 1.585 8.0 15.0 3 4 0 58.129 29.065 0.3153 3.9627 1.550 1.0 2.0 0 1 3 59.572 29.786 0.3225 4.0521 1.504 25.0 50.0 4 0 0 61.579 30.789 0.3323 4.1754 1.504 25.0 50.0 1 5 2 61.579 30.789 0.3323 4.1754 1.501 9.0 18.0 0 2 3 61.751 30.876 0.3331 4.1860 1.501 9.0 18.0 1 1 3 61.751 30.876 0.3331 4.1860 1.496 10.0 20.0 2 6 0 61.962 30.981 0.3341 4.1989 1.456 3.0 6.0 1 2 3 63.871 31.936 0.3434 4.3148 1.445 1.0 2.0 4 2 0 64.421 32.210 0.3460 4.3479 1.419 3.0 6.0 4 1 1 65.717 32.858 0.3522 4.4257 1.410 5.0 11.0 0 7 1 66.227 33.113 0.3546 4.4562 1.396 1.0 2.0 3 3 2 66.967 33.484 0.3581 4.5002 1.389 5.0 11.0 1 3 3 67.349 33.675 0.3599 4.5229 1.377 1.0 2.0 3 5 1 68.022 34.011 0.3631 4.5626 1.373 1.0 2.0 1 7 1 68.247 34.124 0.3641 4.5759 1.355 2.0 4.0 1 6 2 69.288 34.644 0.3690 4.6370 1.343 7.0 16.0 2 2 3 69.997 34.998 0.3723 4.6785 1.323 2.0 5.0 4 3 1 71.177 35.588 0.3778 4.7470 1.314 2.0 5.0 3 4 2 71.720 35.860 0.3803 4.7785 1.308 6.0 14.0 3 6 0 72.139 36.069 0.3822 4.8026 1.308 6.0 14.0 1 4 3 72.139 36.069 0.3822 4.8026 1.289 2.0 5.0 2 3 3 73.341 36.670 0.3877 4.8714 1.276 5.0 12.0 2 7 1 74.212 37.106 0.3916 4.9210 |
4楼2010-11-29 19:24:46
5楼2010-11-29 19:25:22
6楼2010-11-29 21:01:23
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PDF#81-1173: QM=Calculated; d=Calculated; I=Calculated Triphylite, syn Li Fe ( P O4 ) Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= d-Cutoff=17.7 I/Ic(RIR)=1.35 Ref= Calculated from ICSD using POWD-12++ (1997) Orthorhombic - (Unknown), Pnma (62) Z=4 mp= Cell=10.332x6.01x4.692 Pearson=oP28 (?) Density(c)=3.596 Density(m)=3.38A Mwt=157.76 Vol=291.35 F(30)=138.1(.0062,35) Ref= Streltsov, V.A., Belokoneva, E.L., Tsirel'son, V.G., Hansen, N.K. Acta Crystallogr., Sec. B: Structural Science, 49 147 (1993) Strong Line: 2.52/X 3.48/8 3.01/8 4.27/8 5.17/4 2.46/3 2.78/3 1.74/3 3.92/2 2.37/2 FIZ=072545: ATF REM TEM 25 C. DEN. See PDF 01-083-2092. Multipole analysis of the electron density in triphylite, LiFePO4, using X-ray diffraction data d c4 a (PNMA) ABCX4 d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 5.166 38.0 18.5 2 0 0 17.150 8.575 0.0968 1.2163 4.272 76.1 44.8 1 0 1 20.775 10.387 0.1170 1.4707 3.917 24.2 15.6 2 1 0 22.679 11.339 0.1276 1.6038 3.698 9.0 6.1 0 1 1 24.042 12.021 0.1352 1.6989 3.482 82.3 59.6 2 0 1 25.561 12.780 0.1436 1.8045 3.482 82.3 59.6 1 1 1 25.561 12.780 0.1436 1.8045 3.005 78.9 66.2 2 1 1 29.705 14.853 0.1664 2.0909 3.005 78.9 66.2 0 2 0 29.705 14.853 0.1664 2.0909 2.776 30.8 28.0 3 0 1 32.215 16.108 0.1801 2.2631 2.597 2.2 2.1 2 2 0 34.500 17.250 0.1925 2.4189 2.583 0.5 0.5 4 0 0 34.700 17.350 0.1936 2.4325 2.520 100.0 100.0 3 1 1 35.590 17.795 0.1984 2.4929 2.457 31.5 32.3 1 2 1 36.528 18.264 0.2034 2.5564 2.373 21.3 22.6 4 1 0 37.881 18.941 0.2107 2.6477 2.346 1.4 1.5 0 0 2 38.336 19.168 0.2131 2.6783 2.287 12.8 14.1 1 0 2 39.351 19.676 0.2186 2.7464 2.272 12.9 14.3 2 2 1 39.626 19.813 0.2200 2.7649 2.262 17.2 19.2 4 0 1 39.804 19.902 0.2210 2.7768 2.136 15.4 18.2 2 0 2 42.275 21.138 0.2341 2.9415 2.136 15.4 18.2 1 1 2 42.275 21.138 0.2341 2.9415 2.039 6.0 7.4 3 2 1 44.386 22.193 0.2452 3.0812 2.012 4.1 5.1 2 1 2 45.003 22.502 0.2484 3.1218 1.958 1.9 2.4 4 2 0 46.312 23.156 0.2553 3.2077 1.938 0.1 0.1 3 0 2 46.816 23.408 0.2579 3.2406 1.891 1.5 2.0 5 0 1 48.072 24.036 0.2644 3.3225 1.867 0.3 0.4 2 3 0 48.711 24.356 0.2677 3.3639 1.849 12.2 16.6 0 2 2 49.234 24.617 0.2704 3.3978 1.842 7.2 9.8 0 3 1 49.427 24.713 0.2714 3.4103 1.842 7.2 9.8 3 1 2 49.427 24.713 0.2714 3.4103 1.820 3.2 4.4 1 2 2 50.070 25.035 0.2747 3.4518 1.813 13.2 18.3 1 3 1 50.260 25.130 0.2757 3.4641 1.807 7.2 10.0 4 2 1 50.445 25.222 0.2766 3.4760 1.803 6.3 8.8 5 1 1 50.555 25.278 0.2772 3.4831 1.741 30.7 44.4 2 2 2 52.518 26.259 0.2872 3.6089 1.736 25.2 36.6 2 3 1 52.661 26.331 0.2879 3.6180 1.736 25.2 36.6 4 0 2 52.661 26.331 0.2879 3.6180 1.722 1.3 1.9 6 0 0 53.143 26.572 0.2904 3.6488 1.668 15.1 22.8 4 1 2 54.993 27.497 0.2997 3.7661 1.655 17.1 26.0 6 1 0 55.461 27.731 0.3020 3.7956 1.624 20.3 31.5 3 3 1 56.608 28.304 0.3078 3.8676 1.600 2.1 3.3 5 2 1 57.535 28.768 0.3124 3.9256 1.583 11.1 17.7 4 3 0 58.233 29.117 0.3159 3.9691 1.561 0.3 0.5 6 1 1 59.132 29.566 0.3203 4.0249 1.550 0.1 0.2 5 0 2 59.570 29.785 0.3224 4.0520 1.546 0.4 0.7 1 0 3 59.751 29.876 0.3233 4.0632 1.513 0.3 0.5 0 1 3 61.182 30.591 0.3303 4.1512 1.507 2.0 3.3 1 3 2 61.472 30.736 0.3317 4.1689 1.502 15.6 26.2 0 4 0 61.683 30.842 0.3328 4.1818 1.502 15.6 26.2 5 1 2 61.683 30.842 0.3328 4.1818 1.497 14.6 24.6 2 0 3 61.907 30.954 0.3339 4.1955 1.497 14.6 24.6 1 1 3 61.907 30.954 0.3339 4.1955 1.494 16.3 27.5 6 2 0 62.070 31.035 0.3347 4.2054 1.461 0.2 0.3 2 3 2 63.625 31.813 0.3422 4.2999 1.452 3.2 5.6 2 1 3 64.052 32.026 0.3442 4.3257 1.442 0.8 1.4 2 4 0 64.540 32.270 0.3466 4.3551 1.424 0.7 1.2 3 0 3 65.491 32.746 0.3511 4.4122 1.424 0.7 1.2 6 2 1 65.491 32.746 0.3511 4.4122 1.417 2.8 5.0 1 4 1 65.838 32.919 0.3528 4.4329 1.408 5.8 10.4 7 0 1 66.334 33.167 0.3551 4.4626 1.393 0.8 1.4 3 3 2 67.129 33.564 0.3589 4.5098 1.388 2.2 4.0 6 0 2 67.406 33.703 0.3602 4.5262 1.385 5.0 9.1 3 1 3 67.544 33.772 0.3608 4.5344 1.378 0.7 1.3 2 4 1 67.971 33.986 0.3628 4.5596 1.378 0.7 1.3 5 2 2 67.971 33.986 0.3628 4.5596 1.375 1.8 3.3 1 2 3 68.130 34.065 0.3636 4.5690 1.375 1.8 3.3 5 3 1 68.130 34.065 0.3636 4.5690 1.370 1.2 2.2 7 1 1 68.374 34.187 0.3647 4.5834 1.352 3.0 5.6 6 1 2 69.430 34.715 0.3697 4.6454 1.339 9.6 18.1 2 2 3 70.184 35.092 0.3732 4.6894 1.337 5.3 10.0 4 0 3 70.305 35.153 0.3737 4.6964 1.321 3.0 5.7 3 4 1 71.313 35.656 0.3784 4.7549 1.312 2.3 4.4 4 3 2 71.890 35.945 0.3810 4.7882 1.305 10.2 19.7 6 3 0 72.294 36.147 0.3829 4.8115 1.305 10.2 19.7 4 1 3 72.294 36.147 0.3829 4.8115 1.291 0.2 0.4 8 0 0 73.228 36.614 0.3871 4.8650 1.286 2.7 5.3 3 2 3 73.536 36.768 0.3885 4.8826 1.275 6.7 13.2 7 2 1 74.336 37.168 0.3922 4.9281 1.265 1.4 2.8 0 4 2 75.005 37.503 0.3952 4.9660 1.262 0.8 1.6 8 1 0 75.185 37.592 0.3960 4.9761 1.260 0.3 0.6 6 2 2 75.357 37.679 0.3968 4.9858 1.258 0.7 1.4 6 3 1 75.509 37.754 0.3974 4.9943 1.255 1.7 3.4 1 4 2 75.663 37.832 0.3981 5.0031 1.251 1.0 2.0 4 4 1 75.961 37.980 0.3995 5.0198 1.249 0.6 1.2 7 0 2 76.131 38.066 0.4002 5.0293 1.247 0.7 1.4 5 0 3 76.293 38.146 0.4009 5.0384 1.232 0.6 1.2 0 3 3 77.338 38.669 0.4056 5.0967 1.228 2.9 5.9 2 4 2 77.627 38.814 0.4069 5.1127 1.226 3.7 7.6 5 3 2 77.830 38.915 0.4078 5.1240 1.224 2.2 4.5 7 1 2 77.990 38.995 0.4085 5.1328 1.224 2.2 4.5 1 3 3 77.990 38.995 0.4085 5.1328 1.221 1.2 2.5 5 1 3 78.223 39.111 0.4095 5.1457 1.219 0.4 0.8 8 1 1 78.357 39.179 0.4101 5.1531 1.199 0.7 1.5 2 3 3 79.937 39.968 0.4170 5.2398 1.187 0.1 0.2 3 4 2 80.869 40.435 0.4210 5.2905 1.187 0.1 0.2 8 2 0 80.869 40.435 0.4210 5.2905 1.176 0.3 0.6 5 4 1 81.806 40.903 0.4250 5.3410 1.173 1.2 2.6 0 0 4 82.094 41.047 0.4263 5.3565 1.170 1.0 2.2 2 5 0 82.287 41.144 0.4271 5.3669 1.165 0.8 1.7 1 0 4 82.736 41.368 0.4290 5.3909 1.164 0.7 1.5 0 5 1 82.833 41.416 0.4294 5.3961 1.160 2.2 4.8 3 3 3 83.157 41.578 0.4308 5.4134 1.157 1.7 3.7 6 0 3 83.475 41.737 0.4321 5.4303 1.157 1.7 3.7 1 5 1 83.475 41.737 0.4321 5.4303 1.153 2.1 4.6 7 2 2 83.784 41.892 0.4334 5.4467 1.151 3.4 7.4 5 2 3 83.940 41.970 0.4341 5.4550 1.151 3.4 7.4 7 3 1 83.940 41.970 0.4341 5.4550 1.150 2.7 5.9 8 2 1 84.074 42.037 0.4347 5.4620 1.143 0.9 2.0 2 0 4 84.659 42.329 0.4371 5.4929 1.143 0.9 2.0 1 1 4 84.659 42.329 0.4371 5.4929 1.141 2.0 4.4 6 3 2 84.922 42.461 0.4382 5.5067 1.136 2.1 4.7 6 1 3 85.306 42.653 0.4398 5.5268 1.136 2.1 4.7 4 4 2 85.306 42.653 0.4398 5.5268 1.132 1.2 2.7 8 0 2 85.747 42.873 0.4416 5.5499 1.132 1.2 2.7 6 4 0 85.747 42.873 0.4416 5.5499 1.123 0.4 0.9 2 1 4 86.547 43.273 0.4450 5.5915 1.115 1.6 3.6 9 0 1 87.382 43.691 0.4484 5.6346 1.112 4.6 10.4 8 1 2 87.631 43.815 0.4494 5.6474 1.112 4.6 10.4 4 3 3 87.631 43.815 0.4494 5.6474 1.110 2.2 5.0 3 0 4 87.851 43.925 0.4503 5.6587 1.103 4.1 9.4 3 5 1 88.583 44.292 0.4533 5.6961 1.100 2.1 4.8 6 4 1 88.839 44.419 0.4543 5.7091 1.096 0.2 0.5 9 1 1 89.265 44.632 0.4560 5.7307 1.092 0.4 0.9 3 1 4 89.648 44.824 0.4576 5.7501 1.092 0.4 0.9 0 2 4 89.648 44.824 0.4576 5.7501 1.089 0.8 1.9 4 5 0 89.954 44.977 0.4588 5.7656 |
7楼2010-11-29 23:02:06
8楼2010-11-29 23:02:44