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SWB888

至尊木虫 (著名写手)

[交流] 急切请教一个化学问题

请问:以下粗体字的意思?


H2PtCl6.6H2O- Catalyzed Reactions of 1-Pentene and
Styrene. As given in Table 1, the arachno-6,8-C2B7H13 and either H2-
PtCl6.6H2Owere added to a 100 mL Schlenk tube, equipped
with a magnetic stirbar, under a N2 purge. Either 1-pentene or styrene
was added via syringe, and then the reaction vessel was degassed on
the high-vacuum line. The chloroplatinic acid-catalyzed reactions were
stirred in a 60 °C oil bath. In the chloroplatinic acid-catalyzed reaction
with styrene, toluene (3 mL) was added to prevent gelling of the
solution.
The reaction products were isolated and purified by passing the
product mixture through a 1/1 mixture of Celite 545/activated charcoal
followed by flash column chromatography to yield analytically pure
samples (Table 1).Sample TextSample Text



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[ Last edited by SWB888 on 2006-5-19 at 07:46 ]

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yhyh96

木虫 (著名写手)


★ ★
SWB888(金币+1):xie xie
zhaoyusnow(金币+1):谢谢参与。
Schlenk tube-施兰克试管(施兰克是一个德国公司)
Celite 545-是一种助滤剂
flash column chromatography -快速柱色谱
2楼2006-05-19 08:17:05
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tanduanming

捐助贵宾 (职业作家)

在google的图片中搜索Schlenk tube,出来的图片全是它。是由1913年Walter Schlenk 发明的。
红日初升,其道大光;河出伏流,一泻汪洋;潜龙腾渊,鳞爪飞扬;乳虎啸谷,百兽震惶;鹰隼试翼,风尘吸张;奇花初胎,矞矞皇皇;干将发硎,有作其芒;天戴其苍,
3楼2006-05-19 10:41:19
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