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小兰花

银虫 (著名写手)

[交流] 【求助】请教 Al-Ag合金 TEM 图片 衍射斑点 的问题,非常感谢! (急)

附图1为 Al-Ag合金 TEM 图片:

   图中,黑色棒 为  γ相(Ag溶质富积区);白色带 区域为 Ag-depleted regions (贫Ag溶质的消耗区)

其他区域为 Guinier-Preston区(GPZ)。

附图1说明:
BF TEM image of an edge-on g plate in a sample aged at 400 ℃ for 120 s and 160 ℃ for 48 h, with a matrix containing GP zones

已知:Al 和Ag 都是   面心立方(fcc)结构, Al-Ag合金在时效时的析出相 为 密排六方(hcp)结构。

注解:
The precipitates are hexagonal-shaped within the (0001)//(111) habit plane, with edges parallel to the close-packed [11-20]//[1-10] directions. Thus, when the precipitates are oriented edge-on in a [11-20]//[1-10] zone axis, their edges are parallel to the electron beam and the exact length of the plates (facet-to-facet) can be measured without any effects of geometry or truncation in the foil.


问题:
  附图1中左上角的衍射斑点(即附图2)起到了什么作用?是哪个相的斑点?

  附图1


附图2


实验说明





[ Last edited by 小兰花 on 2010-8-30 at 13:50 ]
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小兰花

银虫 (著名写手)

多谢关注和帮忙!
因为对 TEM不了解,所以请大家帮帮忙!
引用回帖:
Originally posted by wsq_7710 at 2010-08-29 21:51:34:
说明文字呢??

附图文字说明:

BF TEM image of an edge-on g plate in a sample aged at 400 ℃ for 120 s and 160 ℃ for 48 h, with a matrix containing GP zones


一些注解:
The precipitates are hexagonal-shaped within the (0001)//(111) habit plane, with edges parallel to the close-packed [11-20]//[1-10] directions. Thus, when the precipitates are oriented edge-on in a [11-20]//[1-10] zone axis, their edges are parallel to the electron beam and the exact length of the plates (facet-to-facet) can be measured without any effects of geometry or truncation in the foil.
3楼2010-08-29 22:43:06
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wsq_7710

木虫 (职业作家)

还真不知道斑点作用,不知道它打在哪里,不过注解的我到时看明白了,我怀疑斑点是用来佐证电子束的入射方向的,但是是打的哪个合金,不清楚
4楼2010-08-30 09:06:26
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sourbing

木虫 (正式写手)

小兰花(金币+3):谢谢指点!我对TEM不了解,真在学习中! 2010-08-30 13:45:31
电子衍射斑点是析出物的衍射斑,目的就是说明析出物的析出方向(与基体方向的关系)
5楼2010-08-30 09:09:52
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wsq_7710

木虫 (职业作家)

小兰花(金币+4):谢谢您的关注和帮忙! 现在附上 实验过程的部分解说,比较长! 有时间的话,再指点一下我! 谢谢 2010-08-30 13:44:19
如果斑点打在析出相上,也太牛了,这么清楚,我没用过那么好的设备
6楼2010-08-30 11:40:52
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