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汕头大学海洋科学接受调剂
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dgf2008

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[交流] 【求助】这段话谁知道是哪篇文献的,请提供全文,谢谢 已有4人参与

The tetraethoxysilane (TEOS, 22.0 ml) was added into a solution containing ethanol (27 ml), deionized water (3.7 ml) and aqueous ammonia (30 wt.%, 7.0 ml) at 303 K with vigorous stirring. The mixture was stirred continuously for 1 h to get uniform silica spheres. A mixture solution containing of TEOS (14.5 ml) and octadecyltrimethoxysilane (C18TMS, 5.8 ml) was added into above colloidal solution and stirred for 1 h. The resulting products were dried in atmosphere at 363 K for 12 h and calcined at 873 K for 5 h under atmosphere to obtain final products.

Typically, SCMSS templates (1.0 g), glucose (0.5 g) and deionized water (100 ml) were mixed in a small flask and stirred dramatically with a magnetic stirrer in 343 K water bath until the mixture turned into a dry solid cake. Subsequently, the cake was heated in tube furnace with different heating rates from 373 K to 523 K in nitrogen atmosphere to make glucose melted and flow down along the mesopores of the templates. The cake was then heated to 1123 K and held at that temperature for 3 h to carbonize the glucose. The silica templates were removed by etching in 10% HF and washed by deionized water to obtain HCHs.
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bachier

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这个

dgf2008(金币+5):谢谢 2010-08-12 11:35:22
Electrochemistry Communications,Volume 12, Issue 5, May 2010, Pages 689-692。去下载吧
2楼2010-08-12 09:03:46
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lizzy1221

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楼上的好厉害啊
3楼2010-08-12 11:10:28
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fxwjg

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★ ★
dgf2008(金币+2):谢谢 2010-08-12 15:05:23
mhwu514(金币+2):谢谢讨论 2010-08-12 16:16:13
引用回帖:
Originally posted by dgf2008 at 2010-08-12 08:46:01:
The tetraethoxysilane (TEOS, 22.0 ml) was added into a solution containing ethanol (27 ml), deionized water (3.7 ml) and aqueous ammonia (30 wt.%, 7.0 ml) at 303 K with vigorous stirring. The mixtu ...

直接粘到google,OK
4楼2010-08-12 11:29:47
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sciencemaji

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厉害
5楼2010-08-24 18:06:04
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temedx

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赞二楼,太强悍了。
Everybodyissobusymindingotherppl'sbusiness,thattheyforgettofindtheirownhappiness.
6楼2010-08-24 19:28:10
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wsq_7710

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悲剧,google能告诉你几乎你所想知道的一切,当然正确与否得自己判断!!!
7楼2010-08-24 23:49:12
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雨中孤亭

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佩服一下二楼
男人是社会的主体,不管你信或不信,所以男人应该有种责任感!
8楼2010-10-15 10:51:11
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