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smcg铜虫 (小有名气)
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我该如何回复审稿人 已有2人参与
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文章意见回来了 其中机理部分有两位审稿人都提出了问题： Reviewer #2: 2. A two step mechanism was proposed to explain the formation of Fe3O4 microparticles. The authors listed many literatures about the Fe3O4 secondary structures. However, they didn't give a detailed description about the formation process of their Fe3O4 microparticles. In the aggregation process, the effect of surfactant should be cleared. Is it in the aggregated particles? The author also mentioned that the Fe3O4 microparticles possible to be fabricated by oriented-assembly. Oriented means the aggregation should be along one or several special directions, but the obtained particles seem not to be like that. If possible, a sketch should be given out to describe the process. Reviewer #3: This manuscript synthesised ferromagnetic Fe3O4 microparticles via an one-step solvothermal method. > However, the mechanism that governs the transformation of FeCl3 to Fe3O4 with ethylene glycol as the reducing agent is debatable. Polyehtylene glycol has been used as a template for synthesis of nanoparticles, perhaps EG also acted as a template here. 因为机理部分我不是很熟悉， 而且这部分现在也有争议，很不好回答，修改。 虫虫们, 我现在能不能把这部分，同时补加其他实验内容了？或者有其他更好的回答吗？ 谢了 |
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