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Fluorous methods for synthesis and separation of organic molecules Abstract: Fluorous molecules partition out of an organic phase and into a fluorous(highly fluorinated) phase in a liquid–liquid extraction. New fluorous techniques allow simple yet substantive separations of organic reaction mixtures based on the presence or absence of a fluorous tag. Fluorous-tagged molecules can also be separated from nontagged molecules by solid phase extraction over fluorous reverse-phase silica gel. This technique is ideal for solu-tion-phase parallel synthesis because it allows simple yet substantive separations of organic reaction mixtures. |
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linmouhong
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