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北京石油化工学院2026年研究生招生接收调剂公告

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platomzb

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[交流] 【求助】关于晶体结构的两个问题

请问各位高人
本人测定了一次XRD
样品是硅的氧化物，在21.9 有最强的峰，很高。36.1 处有峰次之。31.2 和57.0 弱的吸收峰请问这个可能是什么种类的结晶啊。
另外，晶体结构中。d1/In, d2/In, d3/In 代表什么意义啊
谢谢

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1楼 2010-03-14 14:45:13

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

pztchina

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专业: 无机材料化学

★ ★
platomzb(金币+1):谢谢参与
platomzb(金币+1): 2010-03-15 19:42
化学小工(金币+1):鼓励交流 2010-03-15 20:31

你的是老式的查卡片对晶体结构那些东东比如d1 d2 d3 为最强峰次强峰第三强峰 d1/In d2/In d3/In 解释为测试出来的峰和标准JCPDS卡片上的峰比较详细内容请看下各种XRD书

你的晶体结构类型最好把XRD数据发上来我帮你看下

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2楼2010-03-15 06:26:50

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platomzb

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非常感谢我的材料是一种硅藻土其二氧化硅可能是方石英但是其在25.5处的那个是什么东西的峰啊应该不是硅的硅藻土中有时会含有铝和铁的麻烦您给我看看谢谢了！！！

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3楼2010-03-15 20:03:07

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

platomzb

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5.49E+01 23
5.50E+01 23

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4楼2010-03-15 20:06:59

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

platomzb

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注册: 2005-08-28
性别: GG
专业: lcp0802@yahoo.com.cn

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7.47E+01 8
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7.59E+01 14
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7.61E+01 27
7.62E+01 21
7.62E+01 25
7.63E+01 26
7.63E+01 19
7.64E+01 26
7.64E+01 20
7.65E+01 18
7.65E+01 22
7.66E+01 24
7.66E+01 17
7.67E+01 24
7.67E+01 22
7.68E+01 27
7.68E+01 26
7.69E+01 32
7.69E+01 25
7.70E+01 30
7.70E+01 18
7.71E+01 20
7.71E+01 22
7.72E+01 28
7.72E+01 16
7.73E+01 23
7.73E+01 19
7.74E+01 32
7.74E+01 21
7.75E+01 15
7.75E+01 26
7.76E+01 24
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7.78E+01 28
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7.79E+01 32
7.79E+01 28
7.80E+01 32
7.80E+01 29
7.81E+01 23
7.81E+01 21
7.82E+01 24
7.82E+01 25
7.83E+01 21
7.83E+01 27
7.84E+01 10
7.84E+01 27
7.85E+01 18
7.85E+01 23
7.86E+01 25
7.86E+01 27
7.87E+01 24
7.87E+01 23
7.88E+01 22
7.88E+01 29
7.89E+01 23
7.89E+01 17
7.90E+01 23
7.90E+01 29
7.91E+01 27
7.91E+01 25
7.92E+01 17
7.92E+01 30
7.93E+01 27
7.93E+01 25
7.94E+01 20
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7.95E+01 26
7.95E+01 27
7.96E+01 24
7.96E+01 26
7.97E+01 28
7.97E+01 21
7.98E+01 18
7.98E+01 17
7.99E+01 18
7.99E+01 25
8.00E+01 24
由于数据比较大我分两部分了是连在一起的

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5楼2010-03-15 20:09:09

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

platomzb

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谢谢啊

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6楼2010-03-15 20:20:52

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pztchina

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专业: 无机材料化学

★
化学小工(金币+1):鼓励交流 2010-03-16 01:19

应该和 JCPDS卡片 39-1425 非常对了
属于SiO2的Cristobalite

本身Cristobalite 在25.5左右有个小峰的
你这个有点杂项主要表现在19度左右的峰
Cristobalite在这个位置没有峰的

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7楼2010-03-15 21:06:47

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pztchina

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★
化学小工(金币+1):鼓励交流 2010-03-16 01:19

如果杂项含有少量铁铝什么的有不知道具体属于什么化合物还是金属那么比较麻烦
需要花费大量时间对JCPDS卡片而且不一定有正确结果

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8楼2010-03-15 21:10:12

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platomzb

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谢谢!
我用浓盐酸处理了几个小时, 好像那个位置的峰明显变小了.说明这些氧化物可能溶解了
不过上次测试的酸处理样品测的结果不怎么好过两天去重新测定一下看看.

赞一下

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9楼2010-03-16 16:16:22

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